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Despite the polymeric nature of dendrimers, the present work has arguably more parallels to the multiazobenzene-containing macrocycles and catenanes reported by Vögtle and Shinkai: (a) Losensky, H.-W.; Spelthann, H.; Ehlen, A.; Vögtle, F.; Bargon, J. Angew. Chem., Int. Ed. Engl. 1988, 27, 1189.
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While not conclusive, the slight differences between [G2] and [G4] may be an indication of the polarity of the environment of the azobenzene: Bortolus, P.; Monti, S. J. Phys. Chem. 1979, 83, 648.
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46
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0345606351
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Repeated attempts at separating the isomers of 5 and 6 by size-exclusion chromatography were unsuccessful
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Repeated attempts at separating the isomers of 5 and 6 by size-exclusion chromatography were unsuccessful.
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