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84920312063
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note
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4 resonances. Si:Al ratios were determined by ICP/AES after digestion of the host in HF.
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22
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84920312062
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4OH (aq), and the nile red/zeolite inclusion was washed with EtOH. Soxhlet-extracted with EtOH, and collected.
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23
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84920312061
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note
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Visible and diffuse reflectance spectra were recorded on a Hitachi U-3501 spectrophotometer with an integrating sphere. X-ray diffractograms were taken on a Scintag XDS 2000 diffractometer with Cu Kα radiation. Mass spectral analysis was carried out on a Hewlett-Packard APCI 59987A electrospray and 5989B mass spectrometer. IR spectra were recorded on a Mattson Polaris spectrometer.
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24
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84920312060
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note
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Two side products were observed in the extracted siliceous sample 1 (M + H = 207 and 341, 15% total), while about 10 products were detected in the solution synthesis.
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