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+ ions and the quartz tube during laser ablation. Thus, we could still obtain a similar result using a target without SiO powder. We also found that the result is not sensitive to the concentration of carbon in the target.
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34
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Microscopic observation was performed with a high-resolution transmission electron microscope (Topcon 002B) working at 200 kV
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Microscopic observation was performed with a high-resolution transmission electron microscope (Topcon 002B) working at 200 kV.
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35
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3542998844
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note
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Although the diameter is homogeneous throughout a wire, the size distribution is diverse among different wires. The core has a lateral dimension in the same order with the thickness of the amorphous layer, which varies from 3 to 20 nm, depending on the diameter of the wire. The outer graphitic sheath usually contains 4 to 15 shells, which are 1.4 to 5.1 nm in thickness, independent of the wire diameter.
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37
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0002088267
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A scanning transmission electron microscope [VG-HB501 (VG Microscopes, Sussex, England)] working at 100 kV equipped with a parallel energy-loss spectrometer [Gatan (Warrendale, PA) PEELS 666] was used. The spatial resolution was about 0.5 nm. See C. Colliex, J. Electron Microsc. 45, 44 (1996).
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A slight disaccord between the B and N profiles at the center point is due to the quantification problem of the B K edge spectra. The long tail of L edge from Si present at the center of tubes overlaps the B K edge and affects the background subtraction there.
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40
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3542997615
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The reference spectra were provided by D. Imhoff and N. Brun.
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The reference spectra were provided by D. Imhoff and N. Brun.
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41
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3543016909
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2 and BN tubes are insulating, and carbon nanotubes are metallic or semiconducting (7)
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2 and BN tubes are insulating, and carbon nanotubes are metallic or semiconducting (7).
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note
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This work was partially supported by the Special Coordination Funds of the Science and Technology Agency of the Japanese Government and a New Energy and Industrial Technology Development Organization international research grant. The Sumitomo Foundation is acknowledged by K.S.
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