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Volumn 39, Issue 33, 1998, Pages 6099-6102

Synthetic studies towards phorboxazole A. A convergent synthesis of the C31-C46 polyene oxane-hemiacetal side chain

Author keywords

[No Author keywords available]

Indexed keywords

PHORBOL DERIVATIVE; PHORBOXAZOLE A; UNCLASSIFIED DRUG;

EID: 0032514515     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)01258-1     Document Type: Article
Times cited : (62)

References (23)
  • 8
    • 0010486984 scopus 로고    scopus 로고
    • note
    • 4. During the completion stages of our work, Ahmed and Forsyth described an alternative synthesis of a derivative of 2 using a conceptually different approach; see ref. 2c.
  • 9
    • 0002645715 scopus 로고    scopus 로고
    • 5. For oxazole ring forming reactions applicable to this study see: Chattopadhyay, S.K. and Pattenden, G., Synlett, 1997, 12, 1342-1343 and references therein.
    • (1997) Synlett , vol.12 , pp. 1342-1343
    • Chattopadhyay, S.K.1    Pattenden, G.2
  • 14
    • 0010518653 scopus 로고    scopus 로고
    • note
    • H (360MHz) 6,19 (d, J 16.0, 1H), 6.21-6.17 (m, 1H), 6.10 (d, J 13.6, 1H), 5.45 (dd, J 15.7, 7.9, 1H), 5.39 (d, J 9.2, 1H), 4.42 (d, J 9.1, 7.0, 1H), 4.18-4.13 (m, 2H), 3.67-3.54 (m, 2H), 3.48 (ddd, J 12.0, 7.1, 1.7, 1H), 3.33 (s, 3H), 3.27 (2xS, 6H), 2.83 (d, J 14.0, 1H), 2.57 (d, J 14.0, 1H), 2.45-2.41 (m, 1H), 2.37-2.23 (m, 2H), 1.92-1.89 (m, 1H), 1.78 (s, 3H), 1.44 (dd, J 12.7, 11.1, 1H), 1.28 (t, J 7.2, 3H), 1.05 (dd, J 13.6, 11.9, 1H), 0.88 (s, 9H), 0.07 (s, 3H), 0.02 (s, 3H).
  • 22
    • 0010493399 scopus 로고    scopus 로고
    • note
    • vic 15.7Hz); <5% of the Z-olefination product was detected by spectroscopy.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.