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2742566087
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note
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Stereochemistry assigned via independent synthesis of (R)-2-(1,1 -dimethylethyl)tetrahydrofuran.
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33847085176
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Russell, C.G.6
Singh, A.7
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53
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0028325136
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 70°C, rate: 0.5°C/min. Spectroscopic data see: D. Guijarro, G. Guillena, B. Mancheno, M. Yus, Tetrahedron 1994, 50, 3427-3436. Assignment of the absolute stereochemistry by comparison of the optical rotations see ref.[10]
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Guijarro, D.1
Guillena, G.2
Mancheno, B.3
Yus, M.4
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54
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2742535432
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 40°C. Spectroscopic data see: E. Lukevits, L. M. Ignatovich, Z. G. Yuskovets, M. V. Shimanskaya, J. Gen. Chem. USSR (Engl. Transl.) 1985, 55, 1839- 1843; Zh. Obshch. Khim. 1985, 55, 2072-2074. Assignment of the absolute configuration by independent synthesis of (R)-2-(1,1-dimethylethyl)tetrahydrofuran: H. C. Brown, S. V. Kulkarni, U. S. Racherla, J. Org. Chem. 1994, 59, 365-369. U. S. Racherla, H. C. Brown, J. Org. Chem. 1991, 56, 401-404.
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Lukevits, E.1
Ignatovich, L.M.2
Yuskovets, Z.G.3
Shimanskaya, M.V.4
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55
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2742557383
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 40°C. Spectroscopic data see: E. Lukevits, L. M. Ignatovich, Z. G. Yuskovets, M. V. Shimanskaya, J. Gen. Chem. USSR (Engl. Transl.) 1985, 55, 1839- 1843; Zh. Obshch. Khim. 1985, 55, 2072-2074. Assignment of the absolute configuration by independent synthesis of (R)-2-(1,1-dimethylethyl)tetrahydrofuran: H. C. Brown, S. V. Kulkarni, U. S. Racherla, J. Org. Chem. 1994, 59, 365-369. U. S. Racherla, H. C. Brown, J. Org. Chem. 1991, 56, 401-404.
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Zh. Obshch. Khim.
, vol.55
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56
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0028210619
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 40°C. Spectroscopic data see: E. Lukevits, L. M. Ignatovich, Z. G. Yuskovets, M. V. Shimanskaya, J. Gen. Chem. USSR (Engl. Transl.) 1985, 55, 1839- 1843; Zh. Obshch. Khim. 1985, 55, 2072-2074. Assignment of the absolute configuration by independent synthesis of (R)-2-(1,1-dimethylethyl)tetrahydrofuran: H. C. Brown, S. V. Kulkarni, U. S. Racherla, J. Org. Chem. 1994, 59, 365-369. U. S. Racherla, H. C. Brown, J. Org. Chem. 1991, 56, 401-404.
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J. Org. Chem.
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Brown, H.C.1
Kulkarni, S.V.2
Racherla, U.S.3
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57
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0001646391
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 40°C. Spectroscopic data see: E. Lukevits, L. M. Ignatovich, Z. G. Yuskovets, M. V. Shimanskaya, J. Gen. Chem. USSR (Engl. Transl.) 1985, 55, 1839- 1843; Zh. Obshch. Khim. 1985, 55, 2072-2074. Assignment of the absolute configuration by independent synthesis of (R)-2-(1,1-dimethylethyl)tetrahydrofuran: H. C. Brown, S. V. Kulkarni, U. S. Racherla, J. Org. Chem. 1994, 59, 365-369. U. S. Racherla, H. C. Brown, J. Org. Chem. 1991, 56, 401-404.
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J. Org. Chem.
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Racherla, U.S.1
Brown, H.C.2
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58
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0028114621
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 70°C. Spectroscopic data and assignment of the stereochemistry by comparison of the optical rotations see: Y. Kurihara, M. Sodcoka, M. Shibasaki, Chem. Pharm. Bull. 1994, 42, 2357-2359.
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Chem. Pharm. Bull.
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Kurihara, Y.1
Sodcoka, M.2
Shibasaki, M.3
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59
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37049066360
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 150°C. Spectroscopic data see: S. Fukuzawa, A. Nakanishi, T. Fujinami, S. Sakai, J. Chem. Soc., Perkin Trans. 1 1988, 1669-1676.
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J. Chem. Soc., Perkin Trans. 1
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Fukuzawa, S.1
Nakanishi, A.2
Fujinami, T.3
Sakai, S.4
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60
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0030605912
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Assignment of the absolute stereochemistry by comparison of the optical rotations: P. Compain, J. Gore, J. Vatele, Tetrahedron 1996, 52, 10405-10416.
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Tetrahedron
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Compain, P.1
Gore, J.2
Vatele, J.3
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61
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0013030399
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 140 °C. Spectroscopic data and assignment of the stereochemistry by comparison of the optical rotations see: A. Albinati, P. Bravo, F. Ganazzoli, G. Resnati, F. Viani, J. Chem. Soc., Perkin Trans, 1 1986, 1405-1416.
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(1986)
J. Chem. Soc., Perkin Trans, 1
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Albinati, A.1
Bravo, P.2
Ganazzoli, F.3
Resnati, G.4
Viani, F.5
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62
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2742584773
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note
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1H-NMR signals by heteronuclear multiple bond (HMBC) experiment.
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63
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0000110756
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Separation of enantiomers: GC Chrompack, β-CD-permethylated, 25 m, 75 °C, rate 0.5°C/min. Spectroscopic data see: E. P. Lodge, C. H. Hcathcock, J. Am. Chem. Soc. 1987, 109, 3353-3361. Assignment of the absolute configuration by independent synthesis see ref.[16]
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J. Am. Chem. Soc.
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Lodge, E.P.1
Hcathcock, C.H.2
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