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+, 239.1651; found, 239.1654.
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13
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85033180203
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note
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+, 379.2673; found, 379.2674. Full characterizations of other minor isomeric products are in progress.
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85033184826
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note
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Reaction was carried out in the same manner as the reaction of 1a with 2a, except that chlorodimethylethylsilane instead of chlorotrimethylsilane was used as an activator. The ratio of products, 5a/3a, decreased from 2.5 at 15 min to 1.5 at 25 min of reaction time.
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submitted for publication
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Choi, G. M.; Yeon, S. H.; Jin, J.; Yoo, B. R.; Jung, I. N. Organometallics, submitted for publication.
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Organometallics
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Choi, G.M.1
Yeon, S.H.2
Jin, J.3
Yoo, B.R.4
Jung, I.N.5
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