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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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0032503512
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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and pertinent references therein
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For lead references, see the following, (a) Fe: Enders, D.; Jandeleit, B.; Raabe, G. Angew. Chem., Int. Ed. Engl. 1994, 33, 1949. (b) Co: Bhatia, B.; Reddy, M. M.; Iqbal, J. Tetrahedron Lett. 1993, 34, 6301. (c) Ni: Bricout, H.; Carpentier, J.-F.; Mortreux, A. J. Chem. Soc., Chem. Commun. 1998, 1863. (d) Rh: Evans, P. A.; Nelson, J. D. J. Am. Chem. Soc. 1998, 120, 5581. (e) Ir: Takeuchi, R.; Kashio, M. J. Am. Chem. Soc. 1998, 120, 8647. (f) Pt: Brown, J. M.; MacIntyre, J. E. J. Chem. Soc., Perkin Trans. 2 1985, 961. (g) Mo: Trost, B. M.; Hachiya, I. J. Am. Chem. Soc. 1998, 120, 1104. (h) W: Lloyd-Jones, G. C.; Pfaltz, A. Angew. Chem., Int. Ed. Engl. 1995, 34, 462 and pertinent references therein.
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For a recent example, see: (a) Kondo, T.; Suzuki, N.; Okada, T.; Mitsudo, T. J. Am. Chem. Soc. 1997, 119, 6187. (b) Suzuki, N.; Kondo, T.; Mitsudo, T. Organometallics 1998, 17, 766. (c) Kondo, T.; Uenoyama, S.; Fujita, K.; Mitsudo, T. J. Am. Chem. Soc. 1999, 121, 482. (d) Mitsudo, T.; Suzuki, T.; Zhang, S.-W.; Imai, D.; Fujita, K.; Manabe, T.; Shiotsuki, M.; Watanabe, Y.; Wada, K.; Kondo, T. J. Am. Chem. Soc. 1999, 121, 1839 and references therein. For a review, see: Naota, T.; Takaya, H.; Murahashi, S. Chem. Rev. 1998, 98, 2599.
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For a recent example, see: (a) Kondo, T.; Suzuki, N.; Okada, T.; Mitsudo, T. J. Am. Chem. Soc. 1997, 119, 6187. (b) Suzuki, N.; Kondo, T.; Mitsudo, T. Organometallics 1998, 17, 766. (c) Kondo, T.; Uenoyama, S.; Fujita, K.; Mitsudo, T. J. Am. Chem. Soc. 1999, 121, 482. (d) Mitsudo, T.; Suzuki, T.; Zhang, S.-W.; Imai, D.; Fujita, K.; Manabe, T.; Shiotsuki, M.; Watanabe, Y.; Wada, K.; Kondo, T. J. Am. Chem. Soc. 1999, 121, 1839 and references therein. For a review, see: Naota, T.; Takaya, H.; Murahashi, S. Chem. Rev. 1998, 98, 2599.
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For a recent example, see: (a) Kondo, T.; Suzuki, N.; Okada, T.; Mitsudo, T. J. Am. Chem. Soc. 1997, 119, 6187. (b) Suzuki, N.; Kondo, T.; Mitsudo, T. Organometallics 1998, 17, 766. (c) Kondo, T.; Uenoyama, S.; Fujita, K.; Mitsudo, T. J. Am. Chem. Soc. 1999, 121, 482. (d) Mitsudo, T.; Suzuki, T.; Zhang, S.-W.; Imai, D.; Fujita, K.; Manabe, T.; Shiotsuki, M.; Watanabe, Y.; Wada, K.; Kondo, T. J. Am. Chem. Soc. 1999, 121, 1839 and references therein. For a review, see: Naota, T.; Takaya, H.; Murahashi, S. Chem. Rev. 1998, 98, 2599.
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35
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For a recent example, see: (a) Kondo, T.; Suzuki, N.; Okada, T.; Mitsudo, T. J. Am. Chem. Soc. 1997, 119, 6187. (b) Suzuki, N.; Kondo, T.; Mitsudo, T. Organometallics 1998, 17, 766. (c) Kondo, T.; Uenoyama, S.; Fujita, K.; Mitsudo, T. J. Am. Chem. Soc. 1999, 121, 482. (d) Mitsudo, T.; Suzuki, T.; Zhang, S.-W.; Imai, D.; Fujita, K.; Manabe, T.; Shiotsuki, M.; Watanabe, Y.; Wada, K.; Kondo, T. J. Am. Chem. Soc. 1999, 121, 1839 and references therein. For a review, see: Naota, T.; Takaya, H.; Murahashi, S. Chem. Rev. 1998, 98, 2599.
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36
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For a recent example, see: (a) Kondo, T.; Suzuki, N.; Okada, T.; Mitsudo, T. J. Am. Chem. Soc. 1997, 119, 6187. (b) Suzuki, N.; Kondo, T.; Mitsudo, T. Organometallics 1998, 17, 766. (c) Kondo, T.; Uenoyama, S.; Fujita, K.; Mitsudo, T. J. Am. Chem. Soc. 1999, 121, 482. (d) Mitsudo, T.; Suzuki, T.; Zhang, S.-W.; Imai, D.; Fujita, K.; Manabe, T.; Shiotsuki, M.; Watanabe, Y.; Wada, K.; Kondo, T. J. Am. Chem. Soc. 1999, 121, 1839 and references therein. For a review, see: Naota, T.; Takaya, H.; Murahashi, S. Chem. Rev. 1998, 98, 2599.
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For example, see: (a) Kondo, T.; Hiraishi, N.; Morisaki, Y.; Wada, K.; Watanabe, Y.; Mitaudo, T. Organometallics 1998, 17, 2131. (b) Kondo, T.; Kodoi, K.; Nishinaga, E.; Okada, T.; Morisaki, Y.; Watanabe, Y.; Mitsudo, T. J. Am. Chem. Soc. 1998, 120, 5587.
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18244427166
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For example, see: (a) Kondo, T.; Hiraishi, N.; Morisaki, Y.; Wada, K.; Watanabe, Y.; Mitaudo, T. Organometallics 1998, 17, 2131. (b) Kondo, T.; Kodoi, K.; Nishinaga, E.; Okada, T.; Morisaki, Y.; Watanabe, Y.; Mitsudo, T. J. Am. Chem. Soc. 1998, 120, 5587.
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The effect of the concentration of CpRuCl(cod) catalyst (5, 10, 25, and 50 mol %) was also examined in the reaction of cis-1e with 2a The beat stereoselectivity of product 3g was observed in eq 2 (5 mol % CpRuCl(cod), cis-3g/trans-3g = 95/5). While the increase of the concentration of CpRuCl(cod) catalyst slightly decreased the stereoselectivity of 3g, the stereoselectivity was constant in the range from 10 mol % to 50 mol % CpRuCl(cod) catalyst (10 mol %, cis-3g/trans-3g = 86/14; 25 mol %, cis-3g/trans-3g = 88/12; 50 mol %, cis-3g/trans-3g = 87/13). For a related reference, see: Ward, Y. D.; Villanueva, L. A.; Allred, G. D.; Liebeskind, L. S. J. Am. Chem. Soc. 1996, 118, 897.
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85034542879
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Since no reaction occurred between Cp*RuCl(cod) and an allylic carbonate, trans-1e, under the stoichiometric reaction conditions, the reaction with a more reactive allylic halide, trans-6a, was examined.
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47
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85034541766
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w = 0.060, GOF = 1.04.
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