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85034281136
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3 ligand is essential and should attach to Ru during the reaction. Efforts are currently underway to prepare the more efficient modified catalysts.
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Careful analysis of the byproducts by GC-MS showed the formation of undec-1-ene (obtained by decarbonylation/β-hydride elimination, 4% yield), undecane (obtained by decarbonylation, 2% yield), and 1-dodecanol (obtained by reduction, 9% yield). Other high-boiling byproducts may contain the aldol-type condensation products but cannot be characterized fully.
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