Preliminary Investigation on the Characterization of Durum Wheat Flours Coming from Some Areas of South Italy by Means of 1H High-Resolution Magic Angle Spinning Nuclear Magnetic Resonance

Journal of Agricultural and Food Chemistry

Volumn 46, Issue 10, 1998, Pages 4242-4249

  Sacco, Antonio ^a   Bolsi, Igor Neri ^a   Massini, Roberto ^b   Spraul, Manfred ^c   Humpfer, Eberhard ^c   Ghelli, Stefano ^d  

^a UNIVERSITY OF BARI   (Italy)

^b UNIVERSITY OF FOGGIA   (Italy)

^c Bruker Analytik GmbH   (Germany)

^d UNIVERSITY OF MODENA AND REGGIO EMILIA   (Italy)

Author keywords

Analysis; Durum wheat flours; NMR

Indexed keywords

TRITICUM AESTIVUM; TRITICUM TURGIDUM SUBSP. DURUM;

EID: 0000581962     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf971113d     Document Type: Article

References (34)

1. Armanino, C.; Forina, M.; Castino, M.; Piracci, A.; Ubigli, M. Chemometrical investigation on four red wines from a single cultivar grown in the Piedmont region. Analyst 1990, 115, 907-910.
2. Aue, W. P.; Karhan, J.; Ernst, R. R. Homonuclear broad band decoupling and two-dimensional J-resolved NMR spectroscopy. J. Chem. Phys. 1976, 64, 4226-4227.
3. Bax, A.; Griffey, R. H.; Hawkins, B. L. Correlation of proton and nitrogen-15 chemical shifted by multiple quantum NMR. J. Magn. Reson. 1983, 55, 301-315.
4. Belton, P. S.; Colquhoun, I. J.; Hills, B. P. Application of NMR to food science. Annu. Rep. NMR Spectrosc. 1993, 26, 1-53.
5. Belton, P. S., Delgadillo, I., Gil, A. M., Webb, G. A., Eds. Magnetic Resonance in Food Science; The Royal Society of Chemistry: Cambridge, U.K., 1995.
6. Belton, P. S.; Delgadillo, I.; Holmes, E.; Nicholls, A.; Nicholson J. K.; Spraul, M. Use of high-field 1H NMR spectroscopy for Analysis of liquid foods. J. Agric. Food Chem. 1996, 44, 1483-1487.
7. Braunschweiler, L.; Bodenhausen, G.; Ernst, R. R. Coherence transfer by isotropic mixing: application to proton correlation spectroscopy. J. Magn. Res. 1983, 53, 521-528.
8. Caselli, M.; De Giglio, A.; Mangone A.; Traini, A. Characterisation of mineral waters by pattern recognition methods. J. Sci. Food Agric. 1998, 76, 533-536.
9. Day, M. P.; Zhang, B.; Martin, G. J. Determination of the geographical origin of wine using joint analysis of elemental and isotopic composition. II-Differentiation of the principal production zones in France for the 1990 vintage. J. Sci. Food Agric. 1995, 67, 113-123.
10. Dunlop, P. J.; Bignell, C. M.; Jackson, J. F.; Hibbert, D. Chemometric analysis of gas Chromatographic data of oils from Eucalyptus species. Chemom. Intell. Lab. Syst. 1995, 30, 59-67.
11. Gabriel, N. E.; Roberts, M. F. Short-Chain lecithin/long-chain phospholipid unilammelar vesicle: asymmetry, dynamics and enzymatic hydrolysis of the short-chain component. Biochemistry 1987, 26, 2432-2440.
12. Gruppen, H.; Hoffmann, R. A.; Kormelink, F. J. M.; Voragen, A. G. J.; Kamerling J. P.; Vliegenthart, J. F. G. Characterisation by 1H NMR spectroscopy of enzymically derived oligosaccharides from alkali-extractable wheat-flour arabinoxylan. Carbohydr. Res. 1992, 233, 45-64.
13. 13C nuclear magnetic resonance spectroscopy. J. Am. Oil Chem. Soc. 1993, 70, 1139-1144.
14. Gutierrez, A. M.; Farrell, H. M., Jr.; Kumosinski, T. F. Comparison of hydration behaviour of bovine and caprine caseins as determined by oxigen-17 nuclear magnetic resonance: temperature dependence of colloidal stability. J. Agric. Food Chem. 1996, 44, 48-53.
15. 13C NMR of dell walls in wheat bran. J. Agric. Food Chem. 1997, 45, 117-119.
16. 13C nuclear magnetic resonance spectroscopy. J. Am. Oil Chem. Soc. 1993, 70, 1251-1254.
17. Jeener, J.; Meier, B. H.; Bachmann, P.; Ernst, R. R. Investigation of exchange processes by two-dimensional NMR spectroscopy. J. Chem. Phys. 1979, 71, 4546-4553.
18. Jengrasiak, G. L.; Smith, R.; Ribeiro, A. The interaction of pseudohalides with the phospholipids headgroup: a Nuclear Magnetic Resonance study. Physiol. Chem. Phys. Med. NMR 1991, 23, 1-11.
19. Jonas, J.; Winter, R.; Grandinetti, P. J.; Driscoll, D. High-pressure 2D NOESY experiments on Phospholipids vesicles. J. Magn. Reson. 1990, 87, 536-547.
20. Martin, G. J.; Martin, M. L. Stable isotope analysis of food and beverages by nuclear magnetic resonance. Annu. Rep. NMR Spectrosc. 1995, 31, 81-104.
21. Martin, G. J.; Danho, D.; Vallet, C. Natural isotope fractionation in the discrimination of sugar origins. J. Sci. Food Agric. 1991a, 56, 419-434.
22. Martin, M. L.; Martin, G. J.; Guillou, C. A site-specific and multi-element isotopic approach to origin inference of sugars in foods and beverages. Mikrochim. Acta [Vienna] 1991b, 2, 81-91.
23. Mine, Y. Phosphorous-31 nuclear magnetic resonance study on adsorption behaviour of caseinate in triacylglycerol-water emulsion. J. Agric. Food Chem. 1997, 45, 68-73.
24. Nicholson, J. K.; Foxall, P. J. D.; Spraul, M.; Farrant, R. D.; Lindon, J. C. 750 MHz 1H-13C NMR spectroscopy of human blood plasma. Anal. Chem. 1995, 67, 793-811.
25. Redfield, A. G.; Kunz, S. D. Quadrature Fourier NMR detection: simple multiplex for dual detection and discussion. J. Magn. Reson. 1975, 19, 250-254.
26. Renou, J. P. NMR studies in meat. Annu. Rep. NMR Spectrosc. 1995, 31, 313-343.
27. 1H Nuclear Magnetic Resonance Study of the minor components in virgin olive oils. J. Am. Oil Chem. Soc. 1996, 73, 747-758.
28. Shaka, A. J.; Barker, P. B.; Fremann, R. Computer-optimized decoupling scheme for wideband applications and low-level operation. J. Magn. Reson. 1980, 64, 547-552.
29. 1H NMR. Anal. Biochem. 1989, 178, 67-76.
30. Vogels, J. T. W. E.; Terwel, L.; Tas, A. C.; van den Berg, F.; Dukel, F.; van der Greef, J. Detection of Adulteration in Orange Juices by a new screening method using proton NMR Spectroscopy in combination with Pattern Recognition Techniques. J. Agric. Food Chem. 1996, 44, 175-180.
31. Wahlgren, N. M.; Drakenberg, T. Milk. Annu. Rep. NMR Spectrosc. 1995, 31, 275-312.
32. Wold, S.; Esbensen, K.; Geladi, P. Principal Component Analysis, Intell. Lab. Syst. 1987, 2, 37.
33. 13C nuclear magnetic resonance of the olefinic and carbonyl carbons of edible vegetable oils. J. Am. Oil Chem. Soc. 1990, 67, 487-494.
34. 13C nuclear magnetic resonance. J. Am. Oil Chem. Soc. 1994, 71, 361-364.