Gallophosphonates Containing Alkali Metal Ions. 2.1 Synthesis and Structure of Gallophosphonates Incorporating Na+ and K+ Ions

Inorganic Chemistry

Volumn 37, Issue 3, 1998, Pages 473-478

  Walawalkar, Mrinalini G ^a   Murugavel, Ramaswamy ^a,b   Roesky, Herbert W ^a   Usón, Isabel ^a   Kraetzner, Ralph ^a  

^a UNIVERSITY OF GÖTTINGEN   (Germany)

^b INDIAN INSTITUTE OF TECHNOLOGY BOMBAY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000165654     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic971441v     Document Type: Article

References (47)

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4. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
5. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
6. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
7. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
8. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
9. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
10. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
11. Group 13 phosphonates/phosphates: (a) Estermann, M.; McCusker, L. B.; Baerlocher, C.; Merrouche, A.; Kessler, H. Nature 1991, 352, 320. (b) Chippindale, A. M.; Walton, R. I. J. Chem. Soc., Chem. Commun. 1994, 2453. (c) Jones, R. H.; Thomas, J. M.; Huo, Q.; Xu, R.; Hursthouse, M. B.; Chen, J. J. Chem. Soc., Chem. Commun. 1991, 1520. (d) Chippindale, A. M.; Brech, S. J.; Cowley, A. R.; Simpson, W. M. Chem. Mater. 1996, 8, 2259. (e) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Chem. Mater. 1996, 8, 2391. (f) Jones, R. H.; Chippindale, A. M.; Natarajan, S.; Thomas, J. M. J. Chem. Soc., Chem. Commun. 1994, 565. (g) Yin, X.; Nazar, L. F. J. Chem. Soc., Chem. Commun. 1994, 2349. (h) Oliver, S.; Kuperman, A.; Lough, A.; Ozin, G. A. Inorg. Chem. 1996, 35, 6373.
12. Recent reviews on metal phosphates and phosphonates: (a) Zubieta, J. Comments Inorg. Chem. 1994, 16, 153. (b) Cao, G.; Hong, H.-G.; Mallouk, T. E. Acc. Chem. Res. 1992, 25, 420, (c) Clearfieid, A. Comments Inorg. Chem. 1990, 10, 89. (d) Alberti, G.; Constantino, U. In Inclusion Compounds 5; Atwood, J. L., Davis, J. E. D., MacNicol, D. D., Eds.; Oxford University Press: Oxford, U.K., 1996; p 136.
13. Recent reviews on metal phosphates and phosphonates: (a) Zubieta, J. Comments Inorg. Chem. 1994, 16, 153. (b) Cao, G.; Hong, H.-G.; Mallouk, T. E. Acc. Chem. Res. 1992, 25, 420, (c) Clearfieid, A. Comments Inorg. Chem. 1990, 10, 89. (d) Alberti, G.; Constantino, U. In Inclusion Compounds 5; Atwood, J. L., Davis, J. E. D., MacNicol, D. D., Eds.; Oxford University Press: Oxford, U.K., 1996; p 136.
14. Recent reviews on metal phosphates and phosphonates: (a) Zubieta, J. Comments Inorg. Chem. 1994, 16, 153. (b) Cao, G.; Hong, H.-G.; Mallouk, T. E. Acc. Chem. Res. 1992, 25, 420, (c) Clearfieid, A. Comments Inorg. Chem. 1990, 10, 89. (d) Alberti, G.; Constantino, U. In Inclusion Compounds 5; Atwood, J. L., Davis, J. E. D., MacNicol, D. D., Eds.; Oxford University Press: Oxford, U.K., 1996; p 136.
15. Recent reviews on metal phosphates and phosphonates: (a) Zubieta, J. Comments Inorg. Chem. 1994, 16, 153. (b) Cao, G.; Hong, H.-G.; Mallouk, T. E. Acc. Chem. Res. 1992, 25, 420, (c) Clearfieid, A. Comments Inorg. Chem. 1990, 10, 89. (d) Alberti, G.; Constantino, U. In Inclusion Compounds 5; Atwood, J. L., Davis, J. E. D., MacNicol, D. D., Eds.; Oxford University Press: Oxford, U.K., 1996; p 136.
16. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
17. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
18. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
19. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
20. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
21. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
22. Recent work on phosphonates and phosphates: (a) Byrd, H.; Clearfield, A.; Poojary, D.; Reis, K. P.; Thompson, M. E. Chem. Mater. 1996, 8, 2239. (b) Song, P.; Xu, J.; Zhao, Y.; Yue, Y.; Xu, Y.; Xu, R.; Hu, N.; Wie, G.; Jia, H. J. Chem. Soc., Chem. Commun. 1994, 1171. (c) Gendraud, P.; de Roy, M. E.; Besse, J. P. Inorg. Chem. 1996, 35, 6108. (d) Bonavia, G.; Haushalter, R. C.; O'Connor, C. J.; Zubieta, J. Inorg. Chem, 1996, 35, 5603. (e) Soghomonian, V.; Haushalter, R. C.; Zubieta, J. Chem. Mater, 1995, 7, 1648. (f) Roca, M.; Marcos, M. D.; Amorós, P.; Beltrán-Porter, A.; Edwards, A. J.; Beltrán-Porter, D. Inorg. Chem. 1996, 35, 5613. (g) Bellito, C.; Federici, F.; Ibrahim, S. A. J. Chem. Soc., Chem. Commun. 1996, 759.
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33. Owing to the low isolated yields of 3, the mother liquor was examined by 3lP NMR spectroscopy after removing the crops of crystals. The observed spectrum showed the presence of several phosphorus-containing species in solution. However, to date, we are not able to identify or crystallize of any of these products.
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38. Owing to the low isolated yields of 3, the mother liquor was examined by 3lP NMR spectroscopy after removing the crops of crystals. The observed spectrum showed the presence of several phosphorus-containing species in solution. However, to date, we are not able to identify or crystallize of any of these products.
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