Organic-Soluble Cyclic and Cage Alkylaluminophosphates: X-ray Crystal Structure of [(tBu)2Al(μ2-O)2P(OSiMe 3)2]2

Inorganic Chemistry

Volumn 35, Issue 20, 1996, Pages 5756-5757

  Mason, Mark R ^a   Matthews, R Mark ^a   Mashuta, Mark S ^a   Richardson, John F ^a  

^a UNIVERSITY OF LOUISVILLE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001586778     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic960619v     Document Type: Article

References (33)

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13. Mason, M. R.; Matthews, R. M.; Perkins, A. M.; Mashuta, M. S.; Richardson, J. F. Manuscript in preparation.
14. 28 (2.04 g, 11.6 mmol) in 30 mL of THF. The resulting clear and colorless solution was heated under reflux for 2 h. The volume of the solution was reduced in vacuo, and the concentrate was cooled at -20 °C overnight to produce clear colorless crystals. Yield of 1: 2.47 g, 3.23 mmol, 56%.
15. 8: C, 43.95: H, 9.49; Al, 7.05; P, 8.09. Found: C, 43.59; H, 9.88; AI, 6.99; P, 7.94.
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22. w = 5.5%.
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24. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
25. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
26. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
27. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
28. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
29. For examples, see: (a) Cheetham, G.; Harding, M. M. Zeolites 1996, 16, 245. (b) Bennett, J. M.; Kirchner, R. M. Zeolites 1992, 12, 338. (c) Wright, P. A.; Natarajan, S.; Thomas, J. M.; Bell, R. G.; Gai-Boyes, P. L.; Jones, R. H.; Chen, J. Angew. Chem., Int. Ed. Engl. 1992, 31, 1472. (d) Simmen, A.; McCusker, L. B.; Baerlocher, Ch.; Meier, W. M. Zeolites 1991, 11, 654. (e) Richardson, J. W., Jr.; Smith, J. V.; Pluth, J. J. J. Phys. Chem. 1989, 93, 8212. (f) Richardson, J. W., Jr.; Pluth, J. J.; Smith, J. V. Acta Crystallogr. 1988, B44, 367.
30. 28 (1.58 g, 10.2 mmol) in 25 mL of THF. The resulting clear and colorless solution was heated under reflux for 2 h. The volume of the solution was reduced in vacua, and the concentrate was cooled at -20 °C overnight to produce clear and colorless crystals. Yield of 2: 1.45 g, l .44 mmol, 56%.
31. 16: C, 33.32; H, 7.19; Al, 10.70; P, 12.28. Found: C, 32.92; H, 7.13; Al, 10.93; P, 12.15.
32. Mason, M. R.; Mashuta, M. S.; Richardson, J. F. Manuscript submitted.
33. Lehmkuhl, H.; Olbrysch, O.; Nehl, H. Liebigs Ann. Chem. 1973. 708.