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2Zn, see:, the β-elimination had been observed by us previously
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85028267913
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I-catalyzed carbo- and hydrozincation of ynamides, was engaged in Negishi cross-coupling reactions by Lam and co-workers
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I-catalyzed carbo- and hydrozincation of ynamides, was engaged in Negishi cross-coupling reactions by Lam and co-workers:
-
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45
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85028254041
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CCDC 1009934 (Z- 13), 1009935 (Z- 27) and 1009936 (E- 30) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via.
-
CCDC 1009934 (Z- 13), 1009935 (Z- 27) and 1009936 (E- 30) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
-
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46
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42749092334
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2 as an additive:, These reaction conditions were not compatible with our enamides and led to protodesilylation.
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2 as an additive:, Z. Wang, J.-P. Pitteloud, L. Montes, M. Rapp, D. Derane, S. F. Wnuk, Tetrahedron 2008, 64, 5322-5327. These reaction conditions were not compatible with our enamides and led to protodesilylation.
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47
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85028241309
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The reasons for this inversion are not clear but may be the result of a participating effect of the Lewis basic bromine atom introduced in allylic position prior to the bromodesilylation reaction.
-
The reasons for this inversion are not clear but may be the result of a participating effect of the Lewis basic bromine atom introduced in allylic position prior to the bromodesilylation reaction.
-
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48
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85028234212
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For recent applications of α-carbonyl β-substituted enamides, see
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For recent applications of α-carbonyl β-substituted enamides, see:
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