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Volumn 1454, Issue , 2016, Pages 86-92

Experimental evidence of the kinetic performance achievable with columns packed with new 1.9 μm fully porous particles of narrow particle size distribution

Author keywords

Column efficiency; Narrow particle size distribution (nPSD); Sub 2 m fully porous particles; Ultra high performance liquid chromatography (UHPLC)

Indexed keywords

COLUMN CHROMATOGRAPHY; EFFICIENCY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIGHT TRANSMISSION; PARTICLE SIZE ANALYSIS; PORE SIZE; POROUS MATERIALS; SIZE DISTRIBUTION;

EID: 84969695664     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2016.05.038     Document Type: Article
Times cited : (37)

References (42)
  • 2
    • 84875455212 scopus 로고    scopus 로고
    • Perspectives on the evolution of the column efficiency in liquid chromatography
    • [2] Gritti, F., Guiochon, G., Perspectives on the evolution of the column efficiency in liquid chromatography. Anal. Chem. 85 (2013), 3017–3035.
    • (2013) Anal. Chem. , vol.85 , pp. 3017-3035
    • Gritti, F.1    Guiochon, G.2
  • 3
    • 84912033978 scopus 로고    scopus 로고
    • The future of UHPLC: towards higher pressure and/or smaller particles?
    • [3] Broeckhoven, K., Desmet, G., The future of UHPLC: towards higher pressure and/or smaller particles?. Trends Anal. Chem. 63 (2014), 65–75.
    • (2014) Trends Anal. Chem. , vol.63 , pp. 65-75
    • Broeckhoven, K.1    Desmet, G.2
  • 4
    • 33748803913 scopus 로고    scopus 로고
    • The art and science of forming packed analytical high-performance liquid chromatography columns
    • [4] Kirkland, J., DeStefano, J., The art and science of forming packed analytical high-performance liquid chromatography columns. J. Chromatogr. A 1126 (2006), 50–57.
    • (2006) J. Chromatogr. A , vol.1126 , pp. 50-57
    • Kirkland, J.1    DeStefano, J.2
  • 5
    • 84983161302 scopus 로고    scopus 로고
    • Larger voids in mechanically stable, loose packings of 1.3 μm frictional, cohesive particles: their reconstruction, statistical analysis, and impact on separation efficiency
    • [5] Reising, A.E., Godinho, J.M., Hormann, K., Jorgenson, J.W., Tallarek, U., Larger voids in mechanically stable, loose packings of 1.3 μm frictional, cohesive particles: their reconstruction, statistical analysis, and impact on separation efficiency. J. Chromatogr. A 1436 (2016), 118–132.
    • (2016) J. Chromatogr. A , vol.1436 , pp. 118-132
    • Reising, A.E.1    Godinho, J.M.2    Hormann, K.3    Jorgenson, J.W.4    Tallarek, U.5
  • 6
    • 84975492248 scopus 로고    scopus 로고
    • Development of a New Monodisperse Porous Silica for UHPLC, Poster presented at 38th International Symposium on High Performance Liquid Phase Separations and Related Technique, (HPLC 2012), June 16–21, Anaheim, CA, USA.
    • [6] Development of a New Monodisperse Porous Silica for UHPLC, Poster presented at 38th International Symposium on High Performance Liquid Phase Separations and Related Technique, (HPLC 2012), June 16–21, 2012, Anaheim, CA, USA.
    • (2012)
  • 7
    • 84975509889 scopus 로고    scopus 로고
    • Advances in liquid chromatography particle technology: perspectives on the development and future of monodispersed silica supports
    • [7] Bell, D.S., Henry, R.A., Betz, W., Ross, P., Advances in liquid chromatography particle technology: perspectives on the development and future of monodispersed silica supports. Chromatogr. today(May/June), 2015, 34–37.
    • (2015) Chromatogr. today , Issue.May/June , pp. 34-37
    • Bell, D.S.1    Henry, R.A.2    Betz, W.3    Ross, P.4
  • 8
    • 84855453726 scopus 로고    scopus 로고
    • Mass transfer kinetics, band broadening and column efficiency
    • [8] Gritti, F., Guiochon, G., Mass transfer kinetics, band broadening and column efficiency. J. Chromatogr. A 1221 (2012), 2–40.
    • (2012) J. Chromatogr. A , vol.1221 , pp. 2-40
    • Gritti, F.1    Guiochon, G.2
  • 9
    • 4243237020 scopus 로고
    • Column efficiency in liquid–solid adsorption chromatography. H.E.T.P. (height equivalent to a theoretical plate) values as a function of separation conditions
    • [9] Snyder, L.R., Column efficiency in liquid–solid adsorption chromatography. H.E.T.P. (height equivalent to a theoretical plate) values as a function of separation conditions. Anal. Chem. 39 (1967), 698–704.
    • (1967) Anal. Chem. , vol.39 , pp. 698-704
    • Snyder, L.R.1
  • 10
    • 84963108088 scopus 로고
    • The performance of packings in high speed liquid chromatography II. ZIPAX®. The effect of particle size
    • [10] Done, J.N., Knox, J.H., The performance of packings in high speed liquid chromatography II. ZIPAX®. The effect of particle size. J. Chromatogr. Sci. 10 (1972), 606–612.
    • (1972) J. Chromatogr. Sci. , vol.10 , pp. 606-612
    • Done, J.N.1    Knox, J.H.2
  • 11
    • 33748439062 scopus 로고
    • Influence of column parameters on peak broadening in high-pressure liquid chromatography
    • [11] Halász, I., Naefe, M., Influence of column parameters on peak broadening in high-pressure liquid chromatography. Anal. Chem. 44 (1972), 76–84.
    • (1972) Anal. Chem. , vol.44 , pp. 76-84
    • Halász, I.1    Naefe, M.2
  • 12
    • 0000995948 scopus 로고
    • Influence of the particle size (5–35 μm) of spherical silica on column efficiency in HPLC
    • [12] Endele, R., Halász, I., Unger, K., Influence of the particle size (5–35 μm) of spherical silica on column efficiency in HPLC. J. Chromatogr. A 99 (1974), 377–393.
    • (1974) J. Chromatogr. A , vol.99 , pp. 377-393
    • Endele, R.1    Halász, I.2    Unger, K.3
  • 13
    • 0344316792 scopus 로고
    • Influence of the particle size distribution of the packing material in reversed-phase high-performance liquid chromatography
    • [13] Dewaele, C., Verzele, M., Influence of the particle size distribution of the packing material in reversed-phase high-performance liquid chromatography. J. Chromatogr. A 260 (1983), 13–21.
    • (1983) J. Chromatogr. A , vol.260 , pp. 13-21
    • Dewaele, C.1    Verzele, M.2
  • 14
    • 34547832128 scopus 로고    scopus 로고
    • Fused-core particles for HPLC columns
    • [14] Kirkland, J.J., DeStefano, J.J., Langlois, T.J., Fused-core particles for HPLC columns. Am. Lab.(February (39)), 2007, 18–21.
    • (2007) Am. Lab. , Issue.February (39) , pp. 18-21
    • Kirkland, J.J.1    DeStefano, J.J.2    Langlois, T.J.3
  • 15
    • 34547736886 scopus 로고    scopus 로고
    • Mass-transfer kinetics in a shell packing material for chromatography
    • [15] Cavazzini, A., Gritti, F., Kaczmarski, K., Marchetti, N., Guiochon, G., Mass-transfer kinetics in a shell packing material for chromatography. Anal. Chem. 79 (2007), 5972–5979.
    • (2007) Anal. Chem. , vol.79 , pp. 5972-5979
    • Cavazzini, A.1    Gritti, F.2    Kaczmarski, K.3    Marchetti, N.4    Guiochon, G.5
  • 16
    • 34250742009 scopus 로고    scopus 로고
    • Comparison between the efficiencies of columns packed with fully and partially porous C18-bonded silica materials
    • [16] Gritti, F., Cavazzini, A., Marchetti, N., Guiochon, G., Comparison between the efficiencies of columns packed with fully and partially porous C18-bonded silica materials. J. Chromatogr. A 1157 (2007), 289–303.
    • (2007) J. Chromatogr. A , vol.1157 , pp. 289-303
    • Gritti, F.1    Cavazzini, A.2    Marchetti, N.3    Guiochon, G.4
  • 17
    • 34547828159 scopus 로고    scopus 로고
    • Gradient elution separation and peak capacity of columns packed with porous shell particles
    • [17] Marchetti, N., Cavazzini, A., Gritti, F., Guiochon, G., Gradient elution separation and peak capacity of columns packed with porous shell particles. J. Chromatogr. A 1163 (2007), 203–211.
    • (2007) J. Chromatogr. A , vol.1163 , pp. 203-211
    • Marchetti, N.1    Cavazzini, A.2    Gritti, F.3    Guiochon, G.4
  • 18
    • 77953806581 scopus 로고    scopus 로고
    • Statistical analysis of packed beds, the origin of short-range disorder, and its impact on eddy dispersion
    • [18] Khirevich, S., Daneyko, A., Höltzel, A., Seidel-Morgenstern, A., Tallarek, U., Statistical analysis of packed beds, the origin of short-range disorder, and its impact on eddy dispersion. J. Chromatogr. A 1217 (2010), 4713–4722.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 4713-4722
    • Khirevich, S.1    Daneyko, A.2    Höltzel, A.3    Seidel-Morgenstern, A.4    Tallarek, U.5
  • 19
    • 80051864716 scopus 로고    scopus 로고
    • Structure-transport correlation for the diffusive tortuosity of bulk, monodisperse, random sphere packings
    • [19] Khirevich, K., Höltzel, A., Daneyko, A., Tallarek, U., Structure-transport correlation for the diffusive tortuosity of bulk, monodisperse, random sphere packings. J. Chromatogr. A 1218 (2011), 6489–6497.
    • (2011) J. Chromatogr. A , vol.1218 , pp. 6489-6497
    • Khirevich, K.1    Höltzel, A.2    Daneyko, A.3    Tallarek, U.4
  • 20
    • 79956127236 scopus 로고    scopus 로고
    • Influence of the particle size distribution on hydraulic permeability and eddy dispersion in bulk packings
    • [20] Daneyko, A., Höltzel, A., Khirevich, K., Tallarek, U., Influence of the particle size distribution on hydraulic permeability and eddy dispersion in bulk packings. Anal. Chem. 83 (2011), 3903–3910.
    • (2011) Anal. Chem. , vol.83 , pp. 3903-3910
    • Daneyko, A.1    Höltzel, A.2    Khirevich, K.3    Tallarek, U.4
  • 22
    • 84865628911 scopus 로고    scopus 로고
    • From random sphere packings to regular pillar arrays: analysis of transverse dispersion
    • [22] Daneyko, A., Hlushkou, D., Khirevich, S., Tallarek, U., From random sphere packings to regular pillar arrays: analysis of transverse dispersion. J. Chromatogr. A 1257 (2012), 98–115.
    • (2012) J. Chromatogr. A , vol.1257 , pp. 98-115
    • Daneyko, A.1    Hlushkou, D.2    Khirevich, S.3    Tallarek, U.4
  • 23
    • 84869877725 scopus 로고    scopus 로고
    • Influence of particle properties on the wall region in packed capillaries
    • [23] Bruns, S., Stoeckel, D., Smarsly, B.M., Tallarek, U., Influence of particle properties on the wall region in packed capillaries. J. Chromatogr. A 1268 (2012), 53–63.
    • (2012) J. Chromatogr. A , vol.1268 , pp. 53-63
    • Bruns, S.1    Stoeckel, D.2    Smarsly, B.M.3    Tallarek, U.4
  • 24
    • 84887169153 scopus 로고    scopus 로고
    • Slurry concentration effects on the bed morphology and separation efficiency of capillaries packed with sub-2 μm particles
    • [24] Bruns, S., Franklin, E.G., Grinias, J.P., Godinho, J.M., Jorgenson, J.W., Tallarek, U., Slurry concentration effects on the bed morphology and separation efficiency of capillaries packed with sub-2 μm particles. J. Chromatogr. A 1318 (2013), 189–197.
    • (2013) J. Chromatogr. A , vol.1318 , pp. 189-197
    • Bruns, S.1    Franklin, E.G.2    Grinias, J.P.3    Godinho, J.M.4    Jorgenson, J.W.5    Tallarek, U.6
  • 26
    • 84904368909 scopus 로고    scopus 로고
    • 18 particles. A detailed investigation of the intra-particle diffusivity
    • 18 particles. A detailed investigation of the intra-particle diffusivity. J. Chromatogr. A 1355 (2014), 164–178.
    • (2014) J. Chromatogr. A , vol.1355 , pp. 164-178
    • Gritti, F.1    Guiochon, G.2
  • 27
    • 70349823141 scopus 로고    scopus 로고
    • Hydrodynamic chromatography for the size classification of micron and sub-micron sized packing materials
    • [27] Thompson, J.W., Lieberman, R.A., Jorgenson, J.W., Hydrodynamic chromatography for the size classification of micron and sub-micron sized packing materials. J. Chromatogr. A 1216 (2009), 7732–7738.
    • (2009) J. Chromatogr. A , vol.1216 , pp. 7732-7738
    • Thompson, J.W.1    Lieberman, R.A.2    Jorgenson, J.W.3
  • 28
    • 84966889224 scopus 로고    scopus 로고
    • HPLC Columns: Theory, Technology and Practice
    • Wiley-VCH
    • [28] Neue, U.D., HPLC Columns: Theory, Technology and Practice. 1997, Wiley-VCH.
    • (1997)
    • Neue, U.D.1
  • 29
    • 0004221934 scopus 로고
    • Dynamics of Chromatography
    • Marcel Dekker New York
    • [29] Giddings, J.C., Dynamics of Chromatography. 1965, Marcel Dekker, New York.
    • (1965)
    • Giddings, J.C.1
  • 30
    • 33645975885 scopus 로고    scopus 로고
    • Influence of frictional heating on temperature gradients in ultra-high-pressure liquid chromatography on 2.1 mm i.d. columns
    • [30] de Villiers, A., Lauer, H., Szucs, R., Goodall, S., Sandra, P., Influence of frictional heating on temperature gradients in ultra-high-pressure liquid chromatography on 2.1 mm i.d. columns. J. Chromatogr. A 1113 (2006), 84–91.
    • (2006) J. Chromatogr. A , vol.1113 , pp. 84-91
    • de Villiers, A.1    Lauer, H.2    Szucs, R.3    Goodall, S.4    Sandra, P.5
  • 31
    • 84930276042 scopus 로고    scopus 로고
    • Method transfer from high-pressure liquid chromatography to ultra-high-pressure liquid chromatography. II. Temperature and pressure effects
    • [31] Åsberg, D., Samuelsson, J., Lesko, M., Cavazzini, A., Kaczmarski, K., Fornstedt, T., Method transfer from high-pressure liquid chromatography to ultra-high-pressure liquid chromatography. II. Temperature and pressure effects. J. Chromatogr. A 1401 (2015), 52–59.
    • (2015) J. Chromatogr. A , vol.1401 , pp. 52-59
    • Åsberg, D.1    Samuelsson, J.2    Lesko, M.3    Cavazzini, A.4    Kaczmarski, K.5    Fornstedt, T.6
  • 33
    • 77954758997 scopus 로고    scopus 로고
    • A protocol for the measurement of all the parameters of the mass transfer kinetics in columns used in liquid chromatography
    • [33] Gritti, F., Guiochon, G., A protocol for the measurement of all the parameters of the mass transfer kinetics in columns used in liquid chromatography. J. Chromatogr. A 1217 (2010), 5137–5151.
    • (2010) J. Chromatogr. A , vol.1217 , pp. 5137-5151
    • Gritti, F.1    Guiochon, G.2
  • 34
    • 37549043110 scopus 로고    scopus 로고
    • Detailed characterisation of the flow resistance of commercial sub-2 μm reversed-phase columns
    • [34] Cabooter, D., Billen, J., Terryn, H., Lynen, F., Sandra, P., Desmet, G., Detailed characterisation of the flow resistance of commercial sub-2 μm reversed-phase columns. J. Chromatogr. A 1178 (2008), 108–117.
    • (2008) J. Chromatogr. A , vol.1178 , pp. 108-117
    • Cabooter, D.1    Billen, J.2    Terryn, H.3    Lynen, F.4    Sandra, P.5    Desmet, G.6
  • 35
    • 0347784832 scopus 로고
    • Theory of solvent disturbance peaks and experimental determination of thermodynamic dead-volume in column liquid chromatography
    • [35] Knox, J.H., Kaliszan, R., Theory of solvent disturbance peaks and experimental determination of thermodynamic dead-volume in column liquid chromatography. J. Chromatogr. 349 (1985), 211–234.
    • (1985) J. Chromatogr. , vol.349 , pp. 211-234
    • Knox, J.H.1    Kaliszan, R.2
  • 36
    • 0003563262 scopus 로고    scopus 로고
    • Fundamentals of Preparative and Nonlinear Chromatography
    • second ed. Academic Press, Elsevier
    • [36] Guiochon, G., Felinger, A., Shirazi, D.G., Katti, A.M., Fundamentals of Preparative and Nonlinear Chromatography. second ed., 2006, Academic Press, Elsevier.
    • (2006)
    • Guiochon, G.1    Felinger, A.2    Shirazi, D.G.3    Katti, A.M.4
  • 37
    • 33947489211 scopus 로고
    • New gas chromatographic method for measuring gaseous diffusion coefficients and obstructive factors
    • [37] Knox, J.H., McLaren, L., New gas chromatographic method for measuring gaseous diffusion coefficients and obstructive factors. Anal. Chem. 36 (1964), 1477–1482.
    • (1964) Anal. Chem. , vol.36 , pp. 1477-1482
    • Knox, J.H.1    McLaren, L.2
  • 38
    • 33847659207 scopus 로고    scopus 로고
    • Peak parking-moment analysis. A strategy for the study of the mass-transfer kinetics in the stationary phase
    • [38] Miyabe, K., Matsumoto, Y., Guiochon, G., Peak parking-moment analysis. A strategy for the study of the mass-transfer kinetics in the stationary phase. Anal. Chem. 79 (2007), 1970–1982.
    • (2007) Anal. Chem. , vol.79 , pp. 1970-1982
    • Miyabe, K.1    Matsumoto, Y.2    Guiochon, G.3
  • 39
    • 33947571141 scopus 로고
    • The diffusion of thiourea in water at 25 °C
    • [39] Ludlum, D., Warner, R., Smith, H., The diffusion of thiourea in water at 25 °C. J. Phys. Chem. 66 (1962), 1540–1542.
    • (1962) J. Phys. Chem. , vol.66 , pp. 1540-1542
    • Ludlum, D.1    Warner, R.2    Smith, H.3
  • 40
    • 84891583498 scopus 로고    scopus 로고
    • Surfactants and Interfacial Phenomena
    • Wiley & Sons, Inc. Hoboken, NJ, USA
    • [40] Rosen, M.J., Kunjappu, J.T., Surfactants and Interfacial Phenomena. 2012, Wiley & Sons, Inc., Hoboken, NJ, USA.
    • (2012)
    • Rosen, M.J.1    Kunjappu, J.T.2
  • 42
    • 21644444953 scopus 로고    scopus 로고
    • Geometry-independent plate height representation methods for the direct comparison of the kinetic performance of LC supports with a different size morphology
    • [42] Desmet, G., Clicq, D., Gzil, P., Geometry-independent plate height representation methods for the direct comparison of the kinetic performance of LC supports with a different size morphology. Anal. Chem. 77 (2005), 4058–4070.
    • (2005) Anal. Chem. , vol.77 , pp. 4058-4070
    • Desmet, G.1    Clicq, D.2    Gzil, P.3


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