High performance solid-phase extraction cleanup method coupled with gas chromatography-triple quadrupole mass spectrometry for analysis of polychlorinated naphthalenes and dioxin-like polychlorinated biphenyls in complex samples

Journal of Chromatography A

Volumn 1448, Issue , 2016, Pages 1-8

  Li, Fang ^a,b   Jin, Jing ^a   Tan, Dongqin ^a,b   Xu, Jiazhi ^a,b   Dhanjai, ^a   Ni, Yuwen ^a   Zhang, Haijun ^a   Chen, Jiping ^a  

^a DALIAN INSTITUTE OF CHEMICAL PHYSICS   (China)

^b UNIVERSITY OF CHINESE ACADEMY OF SCIENCES   (China)

Author keywords

Cleanup; Dioxin like polychlorinated biphenyls; Magnesium oxide; Polychlorinated naphthalenes; Solid phase extraction

Indexed keywords

ALUMINA; CHROMATOGRAPHY; GAS CHROMATOGRAPHY; MAGNESIA; MAGNESIUM; MASS SPECTROMETRY; NAPHTHALENE; ORGANIC POLLUTANTS; PHASE SEPARATION; POLYCHLORINATED BIPHENYLS; SOLVENT EXTRACTION; SPECTROMETRY;

ACCELERATED SOLVENT EXTRACTION; CLEANUP; DIOXIN-LIKE POLYCHLORINATED BIPHENYLS; POLYCHLORINATED NAPHTHALENE (PCNS); POLYCHLORINATED NAPHTHALENES; RELATIVE STANDARD DEVIATIONS; SOLID-PHASE EXTRACTION; TRIPLE-QUADRUPOLE MASS SPECTROMETRY;

EXTRACTION;

ADSORBENT; ALUMINUM OXIDE; CHLORINE; DIOXIN; LIPID; MAGNESIUM OXIDE; MICROSPHERE; ORGANOCHLORINE DERIVATIVE; PIGMENT; POLYCHLORINATED BIPHENYL; POLYCHLORINATED NAPHTHALENE; SULFUR; NAPHTHALENE DERIVATIVE;

ANALYTIC METHOD; ARTICLE; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; ELUTION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; SOLVENT EXTRACTION; TRIPLE QUADRUPOLE MASS SPECTROMETRY; ANIMAL; CHEMISTRY; MASS FRAGMENTOGRAPHY; PINE; PROCEDURES; SCALLOP; SEDIMENT; TANDEM MASS SPECTROMETRY;

ANIMALS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GEOLOGIC SEDIMENTS; NAPHTHALENES; PECTINIDAE; PINUS; POLYCHLORINATED BIPHENYLS; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 84964687978     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2016.04.037     Document Type: Article

References (37)

1. Falandysz J. Polychlorinated naphthalenes: an environmental update. Environ. Pollut. 1998, 101:77-90.
2. Debruyn A.M.H., Ikonomou M.G., Gobas F. Magnification and toxicity of PCBs PCDDs, and PCDFs in upriver-migrating Pacific salmon. Environ. Sci. Technol. 2004, 38:6217-6224.
3. Stockholm conventions . http://chm.pops.int/TheConvention/ThePOPs/tabid/673/Default.aspx.
4. Wang D., Atkinson S., Hoover-Miller A., Li Q.X. Polychlorinated naphthalenes and coplanar polychlorinated biphenyls in tissues of harbor seals (Phoca vitulina) from the northern Gulf of Alaska. Chemosphere 2007, 67:2044-2057.
5. Domingo J.L. Polychlorinated naphthalenes in animal aquatic species and human exposure through the diet: a review. J. Chromatogr. A 2004, 1054:327-334.
6. Wolska L., Mechlinska A., Rogowska J., Namiesnik J. Polychlorinated biphenyls (PCBs) in bottom sediments: identification of sources. Chemosphere 2014, 111:151-156.
7. Helm P.A., Bidleman T.F. Current combustion-related sources contribute to polychlorinated naphthalene and dioxin-like polychlorinated biphenyl levels and profiles in air in Toronto Canada. Environ. Sci. Technol. 2003, 37:1075-1082.
8. Ishaq R., Karlson K., Naf C. Tissue distribution of polychlorinated naphthalenes (PCNs) and non-ortho chlorinated bipbenyls (non-ortho CBs) in harbour porpoises (Phocoena phocoena) from Swedish waters. Chemosphere 2000, 41:1913-1925.
9. Li F., Jin J., Sun X.L., Wang X.L., Li Y., Shah S.M., Chen J.P. Gas chromatography-triple quadrupole mass spectrometry for the determination of atmospheric polychlorinated naphthalenes. J. Hazard. Mater. 2014, 280:111-117.
10. Naert C., Van Peteghem C. Development and application of a simplified clean-up procedure for the determination of polychlorinated biphenyls (PCBs) and polybrominated diphenyl ethers (PBDEs) in horse fat by gas chromatography-tandem mass spectrometry (GC-MS/MS). Food Addit. Contam. 2007, 24:1018-1025.
11. Fernandes A., Mortimer D., Gem M., Smith F., Rose M., Penton S., Carr M. Polychlorinated naphthalenes (PCNs): congener specific analysis, occurrence in food, and dietary exposure in the UK. Environ. Sci. Technol. 2010, 44:3533-3538.
12. Zhao X.F., Zhang H.J., Fan J.F., Guan D.M., Zhao H.D., Ni Y.W., Li Y., Chen J.P. Dioxin-like compounds in sediments from the Daliao River Estuary of Bohai Sea: distribution and their influencing factors. Mar. Pollut. Bull. 2011, 62:918-925.
13. Salihovic S., Nilsson H., Hagberg J., Lindström G. Trends in the analysis of persistent organic pollutants (POPs) in human blood. Trends Anal. Chem. 2013, 46:129-138.
14. Dmitrovic J., Chan S.C., Chan S.H.Y. Analysis of pesticides and PCB congeners in serum by GC/MS with SPE sample cleanup. Toxicol. Lett. 2002, 134:253-258.
15. Kärrman A., Lindström G. Trends, analytical methods and precision in the determination of perfluoroalkyl acids in human milk. Trends Anal. Chem. 2013, 46:118-128.
16. Ramos J.J., Gomara B., Fernandez M.A., Gonzalez M.J. A simple and fast method for the simultaneous determination of polychlorinated biphenyls and polybrominated diphenyl ethers in small volumes of human serum. J. Chromatogr. A 2007, 1152:124-129.
17. Lu D.S., Feng C., Lin Y.J., Wang D.L., Ip H.S.S., Qiu X.L., Wang G.Q., She J.W. Determination of organochlorines, polychlorinated biphenyls and polybrominated diphenyl ethers in human hair: estimation of external and internal exposure. Chemosphere 2014, 114:327-336.
18. Lu D.S., Lin Y.J., Feng C., Wang D.L., Qiu X.L., Jin Y., Xiong L.B., Jin Y., Wang G.Q. Determination of polybrominated diphenyl ethers and polychlorinated biphenyls in fishery and aquaculture products using sequential solid phase extraction and large volume injection gas chromatography/tandem mass spectrometry. J. Chromatogr. B 2014, 945:75-83.
19. Zhang Z.L., Rhind S.M. Optimized determination of polybrominated diphenyl ethers and polychlorinated biphenyls in sheep serum by solid-phase extraction-gas chromatography-mass spectrometry. Talanta 2011, 84:487-493.
20. Malavia J., Abalos M., Santos F.J., Abad E., Rivera J., Galceran M.T. Analysis of polychlorinated dibenzo-p-dioxins, dibenzofurans and dioxin-like polychlorinated biphenyls in vegetable oil samples by gas chromatography-ion trap tandem mass spectrometry. J. Chromatogr. A 2007, 1149:321-332.
21. Piazza R., Gambaro A., Argiriadis E., Vecchiato M., Zambon S., Cescon P., Barbante C. Development of a method for simultaneous analysis of PCDDs, PCDFs PCBs, PBDEs, PCNs and PAHs in Antarctic air. Anal. Bioanal.Chem. 2013, 405:917-932.
22. Ravelo-Perez L.M., Herrera-Herrera A.V., Hernandez-Borges J., Angel Rodriguez-Delgado M. Carbon nanotubes: solid-phase extraction. J. Chromatogr. A 2010, 1217:2618-2641.
23. Garcia-Valverde M.T., Lucena R., Cardenas S., Valcarcel M. Titanium-dioxide nanotubes as sorbents in (micro)extraction techniques. Trends Anal. Chem. 2014, 62:37-45.
24. Sun X.L., Wang J.C., Li Y., Jin J., Zhang B.Q., Shah S.M., Wang X.L., Chen J.P. Highly selective dummy molecularly imprinted polymer as a solid-phase extraction sorbent for five bisphenols in tap and river water. J. Chromatogr. A 2014, 1343:33-41.
25. Pichon V., Chapuis-Hugon F. Role of molecularly imprinted polymers for selective determination of environmental pollutants - A review. Anal. Chim. Acta 2008, 622:48-61.
26. Liu Q., Shi J.B., Zeng L.X., Wang T., Cai Y.Q., Jiang G.B. Evaluation of graphene as an advantageous adsorbent for solid-phase extraction with chlorophenols as model analytes. J. Chromatogr. A 2011, 1218:197-204.
27. Huang Z.Z., Lee H.K. Micro-solid-phase extraction of organochlorine pesticides using porous metal-organic framework MIL-101 as sorbent. J. Chromatogr. A 2015, 1401:9-16.
28. Zhang Z.P., Zheng Y.J., Chen J.P., Zhang Q., Ni Y.W., Liang X.M. Facile synthesis of monodisperse magnesium oxide microspheres via seed-induced precipitation and their applications in high-performance liquid chromatography. Adv. Funct. Mater. 2007, 17:2447-2454.
29. Jin J., Li Y., Zhang Z.P., Su F., Qi P.P., Lu X.B., Chen J.P. The selective cleanup of complex matrices and simultaneous separation of benzo[a]pyrene by solid-phase extraction with MgO microspheres as sorbents. J. Chromatogr. A 2011, 1218:9149-9154.
30. Tan L.K., Liem A.J. Evaluation of column cleanup for chlorobenzenes polychlorinated biphenyls, polychlorinated dibenzo-p-dioxins, and polychlorinated dibenzofurans in MM5 flue gas analysis. Anal. Chem. 1998, 70:191-198.
31. Wang D.L., Atkinson S., Hoover-Miller A., Li Q.X. Analysis of organochlorines in harbor seal (Phoca vitulina) tissue samples from Alaska using gas chromatography ion trap mass spectrometry by an isotopic dilution technique. Rapid Commun. Mass Spectrom. 2005, 19:1815-1821.
32. Bidleman T.F., Helm P.A., Braune B.M., Gabrielsen G.W. Polychlorinated naphthalenes in polar environments-a review. Sci. Total Environ. 2010, 408:2919-2935.
33. Blankenship A.L., Kannan K., Villalobos S.A., Villeneuve D.L., Falandysz J., Imagawa T., Jakobsson E., Giesy J.P. Relative potencies of individual polychlorinated naphthalenes and halowax mixtures to induce Ah receptor-mediated responses. Environ. Sci. Technol. 2000, 34:3153-3158.
34. Gao Y., Zhang H.J., Chen J.P., Zhang Q., Tian Y.Z., Qi P.P., Yu Z.K. Optimized cleanup method for the determination of short chain polychlorinated n-alkanes in sediments by high resolution gas chromatography/electron capture negative ion-low resolution mass spectrometry. Anal. Chim. Acta 2011, 703:187-193.
35. Noma Y., Yamamoto T., Sakai S.I. Congener-specific composition of polychlorinated naphthalenes coplanar PCBs, dibenzo-p-dioxins, and dibenzofurans in the halowax series. Environ. Sci. Technol. 2004, 38:1675-1680.
36. Van den Berg M., Birnbaum L., Bosveld A.T.C., Brunstrom B., Cook P., Feeley M., Giesy J.P., Hanberg A., Hasegawa R., Kennedy S.W., Kubiak T., Larsen J.C., van Leeuwen F.X.R., Liem A.K.D., Nolt C., Peterson R.E., Poellinger L., Safe S., Schrenk D., Tillitt D., Tysklind M., Younes M., Waern F., Zacharewski T. Toxic equivalency factors (TEFs) for PCBs, PCDDs PCDFs for humans and wildlife. Environ. Health Perspect. 1998, 106:775-792.
37. USEPA, Environmental Protection Agency Method 1668, Toxic polychlorinated biphenyls by isotope dilution high resolution gas chromatography/high resolution mass spectrometry. http://nepis.epa.gov/Exe/ZyPURL.cgi%3FDockey=200036PX.txt.