Optimized cleanup method for the determination of short chain polychlorinated n-alkanes in sediments by high resolution gas chromatography/electron capture negative ion-low resolution mass spectrometry

Analytica Chimica Acta

Volumn 703, Issue 2, 2011, Pages 187-193

  Gao, Yuan ^a   Zhang, Haijun ^a   Chen, Jiping ^a   Zhang, Qing ^a   Tian, Yuzeng ^a   Qi, Peipei ^a   Yu, Zhengkun ^a  

^a DALIAN INSTITUTE OF CHEMICAL PHYSICS   (China)

Author keywords

Alumina; Cleanup; Column chromatography; Short chain polychlorinated n alkanes; Silica gel

Indexed keywords

CLEANUP; CLEANUP METHODS; HIGH-RESOLUTION GAS CHROMATOGRAPHIES; INTERFERING SUBSTANCES; MASS FRACTION; METHOD DETECTION LIMITS; ORGANOCHLORINE PESTICIDES; POLYCHLORINATED N-ALKANES; RELATIVE STANDARD DEVIATION (R.S.D.); SEDIMENT SAMPLES; SHORT CHAIN POLYCHLORINATED N-ALKANES;

ADSORPTION; ANOXIC SEDIMENTS; COLUMN CHROMATOGRAPHY; DRIERS (MATERIALS); GELS; MASS SPECTROMETRY; NEGATIVE IONS; OPTIMIZATION; ORGANIC POLLUTANTS; PESTICIDES; POLYCHLORINATED BIPHENYLS; SEDIMENTOLOGY; SILICA; SILICA GEL;

PARAFFINS;

ALKANE DERIVATIVE; ALUMINUM OXIDE; HYDROCHLORIC ACID; ORGANOCHLORINE PESTICIDE; POLYCHLORINATED ALKANE DERIVATIVE; POLYCHLORINATED BIPHENYL; SILICA GEL; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CONTROLLED STUDY; ELECTRON CAPTURE NEGATIVE ION LOW RESOLUTION MASS SPECTROMETRY; GAS CHROMATOGRAPHY; LIMIT OF DETECTION; MASS SPECTROMETRY; ORGANOCHLORINE PESTICIDE REMOVAL; POLYCHLORINATED BIPHENYL REMOVAL; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUANTITATIVE ANALYSIS; RIVER; SEDIMENT; SEPARATION TECHNIQUE; WASTE COMPONENT REMOVAL;

EID: 80052265352     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.07.041     Document Type: Article

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