Underivatized oxysterols and nanoLC-ESI-MS: A mismatch

Steroids

Volumn 99, Issue PB, 2015, Pages 125-130

  Roberg Larsen, Hanne ^a   Vesterdal, Caroline ^a   Wilson, Steven Ray ^a   Lundanes, Elsa ^a  

^a UNIVERSITY OF OSLO   (Norway)

Author keywords

Carry over; Derivatization; Girard reagent; Mass spectrometry; NanoLC; Oxysterol

Indexed keywords

OXYSTEROL; SOLUTION AND SOLUBILITY; SOLVENT; STEROL;

ADSORPTION; ARTICLE; COMPARATIVE STUDY; CONTROLLED STUDY; DERIVATIZATION; ELECTROSPRAY MASS SPECTROMETRY; IONIZATION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETER; NANO SCALE LIQUID CHROMATOGRAPHY; NANOANALYSIS; QUADRUPOLE MASS SPECTROMETRY; STEROL ANALYSIS; SURFACE PROPERTY; NANOTECHNOLOGY; PROCEDURES; SOLUTION AND SOLUBILITY; STANDARD;

CHROMATOGRAPHY, LIQUID; NANOTECHNOLOGY; REFERENCE STANDARDS; SOLUTIONS; SOLVENTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; STEROLS;

EID: 84939429889     PISSN: 0039128X     EISSN: 18785867     Source Type: Journal    
DOI: 10.1016/j.steroids.2015.01.023     Document Type: Article

References (23)

1. A.J. Brown, and W. Jessup Oxysterols: sources, cellular storage and metabolism, and new insights into their roles in cholesterol homeostasis Mol Aspects Med 30 2009 111 122
2. E.R. Nelson, S.E. Wardell, and D.P. McDonnell The molecular mechanisms underlying the pharmacological actions of estrogens, SERMs and oxysterols: implications for the treatment and prevention of osteoporosis Bone 53 2013 42 50
3. E.R. Nelson, C.D. DuSell, X. Wang, M.K. Howe, G. Evans, R.D. Michalek, and et al. The oxysterol, 27-hydroxycholesterol, links cholesterol metabolism to bone homeostasis through its actions on the estrogen and liver X receptors Endocrinology 152 2011 4691 4705
4. H. Roberg-Larsen, M.F. Strand, S. Krauss, and S.R. Wilson Metabolites in vertebrate hedgehog signaling Biochem Biophys Res Commun 446 2014 669 674
5. F.D. Porter, D.E. Scherrer, M.H. Lanier, S.J. Langmade, V. Molugu, S.E. Gale, and et al. Cholesterol oxidation products are sensitive and specific blood-based biomarkers for Niemann-Pick C1 disease Sci Trans Med 2 2010 56ra81
6. K. Karu, M. Hornshaw, G. Woffendin, K. Bodin, M. Hamberg, G. Alvelius, and et al. Liquid chromatography-mass spectrometry utilizing multi-stage fragmentation for the identification of oxysterols J Lipid Res 48 2007 976 987
7. A. Honda, K. Yamashita, T. Hara, T. Ikegami, T. Miyazaki, M. Shirai, and et al. Highly sensitive quantification of key regulatory oxysterols in biological samples by LC-ESI-MS/MS J Lipid Res 50 2009 350 357
8. H. Roberg-Larsen, K. Lund, T. Vehus, N.T. Solberg, C. Vesterdal, D. Misaghian, and et al. Highly automated nanoLC-MS-based approach for thousand cell scale quantification of side chain-hydroxylated oxysterols J Lipid Res 55 2014 1531 1536
9. X. Jiang, R. Sidhu, F.D. Porter, N.M. Yanjanin, A.O. Speak, D.T. te Vruchte, and et al. A sensitive and specific LC-MS/MS method for rapid diagnosis of Niemann-Pick C1 disease from human plasma J Lipid Res 52 2011 1435 1445
10. J.G. McDonald, D.D. Smith, A.R. Stiles, and D.W. Russell A comprehensive method for extraction and quantitative analysis of sterols and secosteroids from human plasma J Lipid Res 53 2012 1399 1409
11. M. Rogeberg, H. Malerod, H. Roberg-Larsen, C. Aass, and S.R. Wilson On-line solid phase extraction-liquid chromatography, with emphasis on modern bioanalysis and miniaturized systems J Pharm Biomed Anal 87 2014 120 129
12. P. Kebarle, and U.H. Verkerk Electrospray: from ions in solution to ions in the gas phase, what we know now Mass Spectrom Rev 28 2009 898 917
13. M. Wilm, and M. Mann Analytical properties of the nanoelectrospray ion source Anal Chem 68 1996 1 8
14. C.G. Enke A predictive model for matrix and analyte effects in electrospray ionization of singly-charged ionic analytes Anal Chem 69 1997 4885 4893
15. H. Roberg-Larsen, M.F. Strand, A. Grimsmo, P.A. Olsen, J.L. Dembinski, F. Rise, and et al. High sensitivity measurements of active oxysterols with automated filtration/filter backflush-solid phase extraction-liquid chromatography-mass spectrometry J Chromatogr A 1255 2012 291 297
16. L. Ahonen, F.B.R. Maire, M. Savolainen, J. Kopra, R.J. Vreeken, T. Hankemeier, and et al. Analysis of oxysterols and vitamin D metabolites in mouse brain and cell line samples by ultra-high-performance liquid chromatography-atmospheric pressure photoionization-mass spectrometry J Chromatogr A 1364 2014 214 222
17. K. Raith, C. Brenner, H. Farwanah, G. Müller, K. Eder, and R.H.H. Neubert A new LC/APCI-MS method for the determination of cholesterol oxidation products in food J Chromatogr A 1067 2005 207 211
18. L. Baila-Rueda, A. Cenarro, M. Cofan, I. Orera, S. Barcelo-Batllori, M. Pocovi, and et al. Simultaneous determination of oxysterols, phytosterols and cholesterol precursors by high performance liquid chromatography tandem mass spectrometry in human serum Anal Methods 5 2013 2249 2257
19. B. Seed Silanizing glassware. Current protocols in immunology 2001 John Wiley & Sons, Inc.
20. W.J. Griffiths, M. Hornshaw, G. Woffendin, S.F. Baker, A. Lockhart, S. Heidelberger, and et al. Discovering oxysterols in plasma: a window on the metabolome J Proteome Res 7 2008 3602 3612
21. F. Guan, L.R. Soma, Y. Luo, C.E. Uboh, and S. Peterman Collision-induced dissociation pathways of anabolic steroids by electrospray ionization tandem mass spectrometry J Am Soc Mass Spectrom 17 2006 477 489
22. A.E. DeBarber, D. Lütjohann, L. Merkens, and R.D. Steiner Liquid chromatography-tandem mass spectrometry determination of plasma 24S-hydroxycholesterol with chromatographic separation of 25-hydroxycholesterol Anal Biochem 381 2008 151 153
23. D. Neville, R. Houghton, and S. Garrett Efficacy of plasma phospholipid removal during sample preparation and subsequent retention under typical UHPLC conditions Bioanalysis 4 2012 795 807