Transient Structures of PdO during CO Oxidation over Pd(100)

Journal of Physical Chemistry C

Volumn 119, Issue 27, 2015, Pages 15469-15476

  Shipilin, Mikhail ^a   Gustafson, Johan ^a   Zhang, Chu ^a   Merte, Lindsay R ^a   Stierle, Andreas ^b,c   Hejral, Uta ^b,c   Ruett, Uta ^c   Gutowski, Olof ^c   Skoglundh, Magnus ^d   Carlsson, Per Anders ^d   Lundgren, Edvin ^a  

^a LUND UNIVERSITY   (Sweden)

^b UNIVERSITY OF HAMBURG   (Germany)

^c DESY   (Germany)

^d CHALMERS UNIVERSITY OF TECHNOLOGY   (Sweden)

Author keywords

[No Author keywords available]

Indexed keywords

CRYSTAL STRUCTURE; FLOW OF GASES; MASS SPECTROMETRY; MASS TRANSFER; SINGLE CRYSTALS; SURFACE STRUCTURE; X RAY DIFFRACTION;

COMPLETE INFORMATION; CRYSTALLOGRAPHIC ORIENTATIONS; EXPERIMENTAL TECHNIQUES; RECIPROCAL SPACE MAPPING; SAMPLE TEMPERATURE; STRUCTURE DYNAMICS; TOTAL GAS PRESSURE; TRANSIENT STRUCTURE;

GASES;

EID: 84936853271     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/acs.jpcc.5b04400     Document Type: Article

References (31)

1. Ertl, G.; Knözinger, H.; Weitkamp, J. Handbook of Heterogeneous Catalysis; Wiley-VCH: Weinheim, 2008.
2. Freund, H. J.; Meijer, G.; Scheffler, M.; Schlögl, R.; Wolf, M. CO oxidation as a prototypical reaction for heterogeneous processes Angew. Chem., Int. Ed. 2011, 50, 10064-10094
3. Kašpar, J.; Fornasiero, P.; Hickey, N. Automotive catalytic converters: current status and some perspectives Catal. Today 2003, 77, 419-449
4. Russell, A.; Epling, W. S. Diesel oxidation catalysts Catal. Rev.-Sci. Eng. 2011, 53, 337-423
5. Goodman, D. W. Catalysis: from single crystals to the "real world" Surf. Sci. 1994, 299-300, 837-848
6. Weaver, J. F. Surface chemistry of late transition metal oxides Chem. Rev. 2013, 113, 4164-4215
7. Lundgren, E.; Gustafson, J.; Mikkelsen, A.; Andersen, J. N.; Stierle, A.; Dosch, H.; Todorova, M.; Rogal, J.; Reuter, K.; Scheffler, M. Kinetic hindrance during the initial oxidation of Pd(100) at ambient pressures Phys. Rev. Lett. 2004, 92, 046101
8. Kan, H. H.; Weaver, J. F. A PdO(101) thin film grown on Pd(111) in ultrahigh vacuum Surf. Sci. 2008, 602, L53-L57
9. Westerström, R.; Weststrate, C. J.; Gustafson, J.; Mikkelsen, A.; Schnadt, J.; Andersen, J. N.; Lundgren, E.; Seriani, N.; Mittendorfer, F.; Kresse, G. Lack of surface oxide layers and facile bulk oxide formation on Pd (110) Phys. Rev. B 2009, 80, 125431
10. Gao, F.; Wang, Y.; Cai, Y.; Goodman, D. W. CO oxidation on Pt-group metals from ultrahigh vacuum to near atmospheric pressures. 2. Palladium and platinum J. Phys. Chem. C 2009, 113, 174-181
11. Kasper, N.; Nolte, P.; Stierle, A. Stability of surface and bulk oxides on Pd(111) revisited by in situ X-ray diffraction J. Phys. Chem. C 2012, 116, 21459-21464
12. Todorova, M.; Lundgren, E.; Blum, V.; Mikkelsen, A.; Gray, S.; Gustafson, J.; Borg, M.; Rogal, J.; Reuter, K.; Andersen, J. N. The Pd(100)-(√5× √5)R27°-O surface oxide revisited Surf. Sci. 2003, 541, 101-112
13. Stierle, A.; Kasper, N.; Dosch, H.; Lundgren, E.; Gustafson, J.; Mikkelsen, A.; Andersen, J. N. A surface X-ray study of the structure and morphology of the oxidized Pd(001) surface J. Chem. Phys. 2005, 122, 044706
14. Kostelník, P.; Seriani, N.; Kresse, G.; Mikkelsen, A.; Lundgren, E.; Blum, V.; Šikola, T.; Varga, P.; Schmid, M. The surface oxide: a LEED, DFT and STM study Surf. Sci. 2007, 601, 1574-1581
15. Seriani, N.; Harl, J.; Mittendorfer, F.; Kresse, G. A first-principles study of bulk oxide formation on Pd(100) J. Chem. Phys. 2009, 131, 054701
16. van Rijn, R.; Balmes, O.; Felici, R.; Gustafson, J.; Wermeille, D.; Westerström, R.; Lundgren, E.; Frenken, J. W. M. Comment on "CO oxidation on Pt-group metals from ultrahigh vacuum to near atmospheric pressures. 2. Palladium and platinum" J. Phys. Chem. C 2010, 114, 6875-6876
17. Blomberg, S.; Hoffmann, M.; Gustafson, J.; Martin, N.; Fernandes, V.; Borg, A.; Liu, Z.; Chang, R.; Matera, S.; Reuter, K. In situ X-ray photoelectron spectroscopy of model catalysts: at the edge of the gap Phys. Rev. Lett. 2013, 110, 117601
18. Blomberg, S.; Brackmann, C.; Gustafson, J.; Aldén, M.; Lundgren, E.; Zetterberg, J. Real-time gas-phase imaging over Pd(110) catalyst during CO oxidation by means of planar laser-induced fluorescence ACS Catal. 2015, 5, 2028-2034
19. Gustafson, J.; Shipilin, M.; Zhang, C.; Stierle, A.; Hejral, U.; Ruett, U.; Gutowski, O.; Carlsson, P.-A.; Skoglundh, M.; Lundgren, E. High-energy surface X-ray diffraction for fast surface structure determination Science 2014, 343, 758-761
20. Shipilin, M.; Hejral, U.; Lundgren, E.; Merte, L. R.; Zhang, C.; Stierle, A.; Ruett, U.; Gutowski, O.; Skoglundh, M.; Carlsson, P.-A. Quantitative surface structure determination using in situ high-energy SXRD: surface oxide formation on Pd(100) during catalytic CO oxidation Surf. Sci. 2014, 630, 229-235
21. Westerström, R.; Messing, M. E.; Blomberg, S.; Hellman, A.; Grönbeck, H.; Gustafson, J.; Martin, N. M.; Balmes, O.; Van Rijn, R.; Andersen, J. N. Oxidation and reduction of Pd(100) and aerosol-deposited Pd nanoparticles Phys. Rev. B 2011, 83, 115440
22. van Rijn, R.; Balmes, O.; Resta, A.; Wermeille, D.; Westerström, R.; Gustafson, J.; Felici, R.; Lundgren, E.; Frenken, J. W. M. Surface structure and reactivity of Pd(100) during CO oxidation near ambient pressures Phys. Chem. Chem. Phys. 2011, 13, 13167-13171
23. Han, J.; Zemlyanov, D. Y.; Ribeiro, F. H. Interaction of O2 with Pd single crystals in the range 1-150 Torr: surface morphology transformations Surf. Sci. 2006, 600, 2730-2744
24. van Rijn, R.; Ackermann, M.; Balmes, O.; Dufrane, T.; Geluk, A.; Gonzalez, H.; Isern, H.; de Kuyper, E.; Petit, L.; Sole, V. A. Ultrahigh vacuum/high-pressure flow reactor for surface X-ray diffraction and grazing incidence small angle X-ray scattering studies close to conditions for industrial catalysis Rev. Sci. Instrum. 2010, 81, 014101
25. Reichert, H.; Honkimäki, V.; Snigirev, A.; Engemann, S.; Dosch, H. A new X-ray transmission-reflection scheme for the study of deeply buried interfaces using high-energy microbeams Physica B 2003, 336, 46-55
26. Hinojosa, J. A.; Weaver, J. F. Surface structural evolution during the thermal decomposition of a PdO(101) thin film Surf. Sci. 2011, 605, 1797-1806
27. Hellman, A.; Resta, A.; Martin, N. M.; Gustafson, J.; Trinchero, A.; Carlsson, P.-A.; Balmes, O.; Felici, R.; Van Rijn, R.; Frenken, J. W. M. The active phase of palladium during methane oxidation J. Phys. Chem. Lett. 2012, 3, 678-682
28. Martin, N. M.; Van Den Bossche, M.; Grönbeck, H.; Hakanoglu, C.; Gustafson, J.; Blomberg, S.; Arman, M. A.; Antony, A.; Rai, R.; Asthagiri, A. Dissociative adsorption of hydrogen on PdO(101) studied by HRCLS and DFT J. Phys. Chem. C 2013, 117, 13510-13519
29. Müller, P.; Hejral, U.; Rütt, U.; Stierle, A. In situ oxidation study of Pd-Rh nanoparticles on MgAl2O4(001) Phys. Chem. Chem. Phys. 2014, 16, 13866-13874
30. Vlieg, E. ROD, a program for surface X-ray crystallography J. Appl. Crystallogr. 2000, 33, 401-405
31. Waser, J.; Levy, H. A.; Peterson, S. W. The structure of PdO Acta Crystallogr. 1953, 6, 661-663