Formation Mechanisms of Pt and Pt3Gd Nanoparticles under Solvothermal Conditions: An in Situ Total X-ray Scattering Study

Journal of Physical Chemistry C

Volumn 119, Issue 23, 2015, Pages 13357-13362

  Saha, Dipankar ^a   Bøjesen, Espen D ^a   Jensen, Kirsten M Ø ^b   Dippel, Ann Christin ^c   Iversen, Bo B ^a  

^a AARHUS UNIVERSITY   (Denmark)

^b Columbia University ^*  (United States)

^c DESY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

BINARY ALLOYS; DISTRIBUTION FUNCTIONS; NANOPARTICLES; PLATINUM ALLOYS; PLATINUM COMPOUNDS; RIETVELD ANALYSIS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION; X RAY SCATTERING;

CHEMICAL AND PHYSICAL PROPERTIES; EXPERIMENTAL DIFFICULTIES; NANOCRYSTAL FORMATION; NANOPARTICLE FORMATION; PAIR DISTRIBUTION FUNCTION ANALYSIS; POWDER X RAY DIFFRACTION; SOLVOTHERMAL CONDITIONS; SOLVOTHERMAL SYNTHESIS;

GADOLINIUM ALLOYS;

EID: 84931291834     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/acs.jpcc.5b03394     Document Type: Article

References (53)

1. Stepanov, A.; Golubev, A.; Nikitin, S.; Osin, Y. A Review on the Fabrication and Properties of Platinum Nanoparticles Rev. Adv. Mater. Sci. 2014, 38, 160-175
2. Yu, W.; Porosoff, M. D.; Chen, J. G. Review of Pt-Based Bimetallic Catalysis: From Model Surfaces To Supported Catalysts Chem. Rev. 2012, 112, 5780-5817
3. Zhang, S.; Yuan, X.-Z.; Hin, J. N. C.; Wang, H.; Friedrich, K. A.; Schulze, M. A Review of Platinum-Based Catalyst Layer Degradation in Proton Exchange Membrane Fuel Cells J. Power Sources 2009, 194, 588-600
4. Carpenter, M. K.; Moylan, T. E.; Kukreja, R. S.; Atwan, M. H.; Tessema, M. M. Solvothermal Synthesis of Platinum Alloy Nanoparticles for Oxygen Reduction Electrocatalysis J. Am. Chem. Soc. 2012, 134, 8535-8542
5. Wu, J.; Yang, H. Platinum-Based Oxygen Reduction Electrocatalysts Acc. Chem. Res. 2013, 46, 1848-1857
6. Murphy, C. J.; Sau, T. K.; Gole, A. M.; Orendorff, C. J.; Gao, J.; Gou, L.; Hunyadi, S. E.; Li, T. Anisotropic Metal Nanoparticles: Synthesis, Assembly, and Optical Applications J. Phys. Chem. B 2005, 109, 13857-13870
7. Wang, Y.-J.; Wilkinson, D. P.; Zhang, J. Noncarbon Support Materials for Polymer Electrolyte Membrane Fuel Cell Electrocatalysts Chem. Rev. 2011, 111, 7625-7651
8. Stephens, I. E. L.; Bondarenko, A. S.; Gronbjerg, U.; Rossmeisl, J.; Chorkendorff, I. Understanding the Electrocatalysis of Oxygen Reduction on Platinum and Its Alloys Energy Environ. Sci. 2012, 5, 6744-6762
9. Anderson, A. B.; Grantscharova, E.; Seong, S. Systematic Theoretical Study of Alloys of Platinum for Enhanced Methanol Fuel Cell Performance J. Electrochem. Soc. 1996, 143, 2075-2082
10. Greeley, J.; Stephens, I. E. L.; Bondarenko, A. S.; Johansson, T. P.; Hansen, H. A.; Jaramillo, T. F.; Rossmeisl, J.; Chorkendorff, I.; Nørskov, J. K. Alloys of Platinum and Early Transition Metals as Oxygen Reduction Electrocatalysts Nat. Chem. 2009, 1, 552-556
11. Gyenge, E.; Atwan, M.; Northwood, D. Electrocatalysis of Borohydride Oxidation on Colloidal Pt And Pt-Alloys (Pt-Ir, Pt-Ni, and Pt-Au) and Application for Direct Borohydride Fuel Cell Anodes J. Electrochem. Soc. 2006, 153, A150-A158
12. Teliska, M.; Murthi, V. S.; Mukerjee, S.; Ramaker, D. E. Correlation of Water Activation, Surface Properties, and Oxygen Reduction Reactivity of Supported Pt-M/C Bimetallic Electrocatalysts Using XAS J. Electrochem. Soc. 2005, 152, A2159-A2169
13. Cui, C.; Gan, L.; Heggen, M.; Rudi, S.; Strasser, P. Compositional Segregation in Shaped Pt Alloy Nanoparticles and Their Structural Behaviour during Electrocatalysis Nat. Mater. 2013, 12, 765-771
14. Mukerjee, S.; Srinivasan, S.; Soriaga, M. P.; McBreen, J. Role of Structural and Electronic Properties of Pt And Pt Alloys on Electrocatalysis of Oxygen Reduction an In Situ XANES and EXAFS Investigation J. Electrochem. Soc. 1995, 142, 1409-1422
15. 5Gd as a Highly Active and Stable Catalyst for Oxygen Electroreduction J. Am. Chem. Soc. 2012, 134, 16476-16479
16. http://www1.asminternational.org/asmenterprise/apd/: Alloy Phase Diagram Database.
17. Kim, H. The Role of the Local Structure in Electronic Properties of Various Materials; ProQuest: Ann Arbor, MI, 2007.
18. Billinge, S. J. L. The Nanostructure Problem Physics 2010, 3, 25
19. Jensen, K. M. Ø.; Tyrsted, C.; Bremholm, M.; Iversen, B. B. In Situ Studies of Solvothermal Synthesis of Energy Materials ChemSusChem 2014, 7, 1594-1611
20. Egami, T.; Billinge, S. J. Underneath the Bragg Peaks: Structural Analysis of Complex Materials; Pergamon: Oxford, 2012; Vol. 16.
21. Billinge, S. J. L.; Kanatzidis, M. G. Beyond Crystallography: The Study of Disorder, Nanocrystallinity and Crystallographically Challenged Materials with Pair Distribution Functions Chem. Commun. (Cambridge, U. K.) 2004, 749-760
22. Becker, J.; Bremholm, M.; Tyrsted, C.; Pauw, B.; Jensen, K. M. O.; Eltzholt, J.; Christensen, M.; Iversen, B. B. Experimental Setup for In Situ X-Ray SAXS/WAXS/PDF Studies of the Formation and Growth of Nanoparticles in Near- and Supercritical Fluids J. Appl. Crystallogr. 2010, 43, 729-736
23. Chupas, P. J.; Chapman, K. W.; Kurtz, C.; Hanson, J. C.; Lee, P. L.; Grey, C. P. A Versatile Sample-Environment Cell for Non-Ambient X-Ray Scattering Experiments J. Appl. Crystallogr. 2008, 41, 822-824
24. Juhas, P.; Davis, T.; Farrow, C. L.; Billinge, S. J. L. Pdfgetx3: A Rapid and Highly Automatable Program for Processing Powder Diffraction Data into Total Scattering Pair Distribution Functions J. Appl. Crystallogr. 2013, 46, 560-566
25. Farrow, C. L.; Juhas, P.; Liu, J. W.; Bryndin, D.; Božin, E. S.; Bloch, J.; Proffen, T.; Billinge, S. J. L. Pdffit2 and Pdfgui: Computer Programs for Studying Nanostructure in Crystals J. Phys.: Condens. Matter 2007, 19, 335219-335226
26. 2 Nanoparticle Formation and Growth during Hydrothermal Synthesis: An In Situ Total Scattering Study J. Am. Chem. Soc. 2012, 134, 6785-6792
27. 3 Nanoparticle Formation under Hydrothermal Conditions Angew. Chem., Int. Ed. 2014, 53, 3667-3670
28. Tyrsted, C.; Lock, N.; Jensen, K. M. O.; Christensen, M.; Bojesen, E. D.; Emerich, H.; Vaughan, G.; Billinge, S. J. L.; Iversen, B. B. Evolution of Atomic Structure During Nanoparticle Formation IUCrJ 2014, 1, 165-171
29. Jensen, K. M. Ø.; Andersen, H. L.; Tyrsted, C.; Bøjesen, E. D.; Dippel, A.-C.; Lock, N.; Billinge, S. J. L.; Iversen, B. B.; Christensen, M. Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An In Situ Total Scattering Study ACS Nano 2014, 8, 10704-10714
30. Hammersley, A.; Svensson, S.; Hanfland, M.; Fitch, A.; Hausermann, D. Two-Dimensional Detector Software: From Real Detector To Idealised Image or Two-Theta Scan Int. J. High Pressure Res. 1996, 14, 235-248
31. Rodríguez-Carvajal, J. Recent Advances in Magnetic Structure Determination by Neutron Powder Diffraction Physica B 1993, 192, 55-69
32. Dippel, A.-C.; Bindzus, N.; Saha, D.; Delitz, J. T.; Liermann, H.-P.; Wahlberg, N.; Becker, J.; Bøjesen, E. D.; Brummerstedt Iversen, B. Synchrotron Powder Diffraction at P02.1 at Petra III: From Electron Density Distributions to In Situ Total Scattering Z. Anorg. Allg. Chem. 2014, 640, 3094-3099
33. 4 with Estimates of the Factors Affecting Accuracy Acta Crystallogr., Sect. B: Struct. Sci. 1972, 28, 393-399
34. Finney, E. E.; Finke, R. G. The Four-Step, Double-Autocatalytic Mechanism for Transition-Metal Nanocluster Nucleation, Growth, and Then Agglomeration: Metal, Ligand, Concentration, Temperature, and Solvent Dependency Studies Chem. Mater. 2008, 20, 1956-1970
35. Varghese, N.; Rao, C. N. R. Growth Kinetics of Platinum Nanocrystals Prepared by Two Different Methods: Role of the Surface J. Colloid Interface Sci. 2012, 365, 117-121
36. Harada, M.; Kamigaito, Y. Nucleation and Aggregative Growth Process af Platinum Nanoparticles Studied by In Situ Quick XAFS Spectroscopy Langmuir 2011, 28, 2415-2428
37. Zheng, H.; Smith, R. K.; Jun, Y.-w.; Kisielowski, C.; Dahmen, U.; Alivisatos, A. P. Observation of Single Colloidal Platinum Nanocrystal Growth Trajectories Science 2009, 324, 1309-1312
38. Simonsen, S. B.; Chorkendorff, I.; Dahl, S.; Skoglundh, M.; Sehested, J.; Helveg, S. Direct Observations of Oxygen-Induced Platinum Nanoparticle Ripening Studied by In Situ TEM J. Am. Chem. Soc. 2010, 132, 7968-7975
39. 2- in Aqueous and Tetrahydrofuran Solutions of PVP J. Phys. Chem. C 2013, 117, 26667-26674
40. Cheong, S.; Watt, J.; Ingham, B.; Toney, M. F.; Tilley, R. D. In Situ and Ex Situ Studies of Platinum Nanocrystals: Growth and Evolution in Solution J. Am. Chem. Soc. 2009, 131, 14590-14595
41. Ren, J.; Tilley, R. D. Preparation, Self-Assembly, and Mechanistic Study of Highly Monodispersed Nanocubes J. Am. Chem. Soc. 2007, 129, 3287-3291
42. Cameron, R. E.; Bocarsly, A. B. Multielectron-Photoinduced Reduction of Chloroplatinum Complexes: Visible Light Deposition of Platinum Metal Inorg. Chem. 1986, 25, 2910-2913
43. Santacesaria, E.; Galli, C.; Carrà, S. Kinetics of Hexachloroplatinic Acid Reduction React. Kinet. Catal. Lett. 1977, 7, 361-366
44. Avrami, M. Kinetics of Phase Change. I. General Theory J. Chem. Phys. 1939, 7, 1103-1112
45. Avrami, M. Kinetics of Phase Change. II. Transformation-Time Relations for Random Distribution of Nuclei J. Chem. Phys. 1940, 8, 212-224
46. Avrami, M. Granulation, Phase Change, and Microstructure Kinetics of Phase Change. III J. Chem. Phys. 1941, 9, 177-184
47. Shields, S. P.; Richards, V. N.; Buhro, W. E. Nucleation Control of Size and Dispersity in Aggregative Nanoparticle Growth. A Study of the Coarsening Kinetics of Thiolate-Capped Gold Nanocrystals Chem. Mater. 2010, 22, 3212-3225
48. Richards, V. N.; Rath, N. P.; Buhro, W. E. Pathway From a Molecular Precursor to Silver Nanoparticles: The Prominent Role of Aggregative Growth Chem. Mater. 2010, 22, 3556-3567
49. Richards, V. N.; Shields, S. P.; Buhro, W. E. Nucleation Control in the Aggregative Growth of Bismuth Nanocrystals Chem. Mater. 2011, 23, 137-144
50. 2O-Type Oxides of Platinum and Palladium on Carbon and Alumina Support Films J. Less-Common Met. 1989, 147, 59-71
51. Oemry, F.; Padama, A. A. B.; Kishi, H.; Kunikata, S.; Nakanishi, H.; Kasai, H.; Maekawa, H.; Osumi, K.; Sato, K. Effects of Cluster Size on Platinum-Oxygen Bonds Formation in Small Platinum Clusters Jpn. J. Appl. Phys. 2012, 51, 035002
52. Newton, M. A.; Chapman, K. W.; Thompsett, D.; Chupas, P. J. Chasing Changing Nanoparticles with Time-Resolved Pair Distribution Function Methods J. Am. Chem. Soc. 2012, 134, 5036-5039
53. Davey, W. P. Precision Measurements of the Lattice Constants of Twelve Common Metals Phys. Rev. 1925, 25, 753-761