Mechanisms for iron oxide formation under hydrothermal conditions: An in situ total scattering study

ACS Nano

Volumn 8, Issue 10, 2014, Pages 10704-10714

  Jensen, Kirsten M Ø ^a,b   Andersen, Henrik L ^a   Tyrsted, Christoffer ^a   Bøjesen, Espen D ^a   Dippel, Ann Christin ^c   Lock, Nina ^a   Billinge, Simon J L ^b,d   Iversen, Bo B ^a   Christensen, Mogens ^a  

^a AARHUS UNIVERSITY   (Denmark)

^b Columbia University ^*  (United States)

^c DESY   (Germany)

^d BROOKHAVEN NATIONAL LABORATORY   (United States)

Author keywords

hydrothermal; in situ; maghemite; pair distribution function analysis; total scattering

Indexed keywords

COORDINATION REACTIONS; CRYSTALLITE SIZE; DISTRIBUTION FUNCTIONS; HEMATITE; NANOCRYSTALLITES; PARTICLE SIZE ANALYSIS;

CRYSTALLIZATION PROCESS; HYDROTHERMAL; HYDROTHERMAL CONDITIONS; HYDROTHERMAL TREATMENTS; LOCAL ATOMIC STRUCTURES; MAGHEMITES; PAIR DISTRIBUTION FUNCTION ANALYSIS; TOTAL SCATTERING;

HYDROTHERMAL SYNTHESIS;

EID: 84908409627     PISSN: 19360851     EISSN: 1936086X     Source Type: Journal    
DOI: 10.1021/nn5044096     Document Type: Article

References (66)

1. Zeng, H.; Li, J.; Liu, J. P.; Wang, Z. L.; Sun, S. H. Exchange-Coupled Nanocomposite Magnets by Nanoparticle Self-Assembly Nature 2002, 420, 395-398
2. Jones, N. The Pull of Stronger Magnets Nature 2011, 472, 22-23
3. Lu, A. H.; Salabas, E. L.; Schuth, F. Magnetic Nanoparticles: Synthesis, Protection, Functionalization, and Application Angew. Chem., Int. Ed. 2007, 46, 1222-1244
4. Pankhurst, Q. A.; Connolly, J.; Jones, S. K.; Dobson, J. Applications of Magnetic Nanoparticles in Biomedicine J. Phys. D: Appl. Phys. 2003, 36, R167-R181
5. Pankhurst, Q. A.; Thanh, N. T. K.; Jones, S. K.; Dobson, J. Progress in Applications of Magnetic Nanoparticles in Biomedicine J. Phys. D: Appl. Phys. 2009, 42, 224001
6. Berry, C. C. Progress in Functionalization of Magnetic Nanoparticles for Applications in Biomedicine J. Phys. D: Appl. Phys. 2009, 42, 224003
7. 3 Nanoparticles and Vacancy Ordering: An in Situ X-ray Powder Diffraction Study J. Solid State Chem. 2007, 180, 180-185
8. Dronskowski, R. The Little Maghemite Story: A Classic Functional Material Adv. Funct. Mater. 2001, 11, 27-29
9. Byrappa, K.; Adschiri, T. Hydrothermal Technology for Nanotechnology Prog. Cryst. Growth Charact. Mater. 2007, 53, 117-166
10. Aymonier, C.; Loppinet-Serani, A.; Reveron, H.; Garrabos, Y.; Cansell, F. Review of Supercritical Fluids in Inorganic Materials Science J. Supercrit. Fluids 2006, 38, 242-251
11. 4 Nanocrystals J. Phys. D: Appl. Phys. 2009, 42, 055004
12. Daou, T. J.; Pourroy, G.; Begin-Colin, S.; Greneche, J. M.; Ulhaq-Bouillet, C.; Legare, P.; Bernhardt, P.; Leuvrey, C.; Rogez, G. Hydrothermal Synthesis of Monodisperse Magnetite Nanoparticles Chem. Mater. 2006, 18, 4399-4404
13. 4) Nanoparticles with the Magnetic and Electrochemical Properties J. Cryst. Growth 2008, 310, 5453-5457
14. 4) Powders Mater. Lett. 2002, 56, 571-577
15. Bremholm, M.; Felicissimo, M.; Iversen, B. B. Time-Resolved in Situ Synchrotron X-ray Study and Large-Scale Production of Magnetite Nanoparticles in Supercritical Water Angew. Chem., Int. Ed. 2009, 48, 4788-4791
16. Horner, O.; Neveu, S.; de Montredon, S.; Siaugue, J. M.; Cabuil, V. Hydrothermal Synthesis of Large Maghemite Nanoparticles: Influence of the pH on the Particle Size J. Nanopart. Res. 2009, 11, 1247-1250
17. Adschiri, T.; Kanazawa, K.; Arai, K. Rapid and Continuous Hydrothermal Crystallization of Metal Oxide Particles in Supercritical Water J. Am. Ceram. Soc. 1992, 75, 1019-1022
18. Cabanas, A.; Poliakoff, M. The Continuous Hydrothermal Synthesis of Nano-Particulate Ferrites in Near Critical and Supercritical Water J. Mater. Chem. 2001, 11, 1408-1416
19. Walton, R. I. Subcritical Solvothermal Synthesis of Condensed Inorganic Materials Chem. Soc. Rev. 2002, 31, 230-238
20. Lester, E.; Blood, P.; Denyer, J.; Giddings, D.; Azzopardi, B.; Poliakoff, M. Reaction Engineering: The Supercritical Water Hydrothermal Synthesis of Nano-Particles J. Supercrit. Fluids 2006, 37, 209-214
21. Adschiri, T.; Lee, Y. W.; Goto, M.; Takami, S. Green Materials Synthesis with Supercritical Water Green Chem. 2011, 13, 1380-1390
22. Yoshimura, M.; Byrappa, K. Hydrothermal Processing of Materials: Past, Present and Future J. Mater. Sci. 2008, 43, 2085-2103
23. Jensen, K. M. Ø.; Tyrsted, C.; Bremholm, M.; Iversen, B. B. In-Situ Studies of Solvothermal Synthesis of Energy Materials ChemSusChem 2014, 7, 1594-1611
24. Bremholm, M.; Jensen, H.; Iversen, S. B.; Iversen, B. B. Reactor Design for in Situ X-ray Scattering Studies of Nanoparticle Formation in Supercritical Water Syntheses J. Supercrit. Fluids 2008, 44, 385-390
25. 2 Nanoparticles Synthesized in Supercritical Water Chem. Mater. 2010, 22, 1814-1820
26. 3 in Biomolecule-Assisted Near-Critical Water: In Situ Synchrotron Radiation Study J. Phys. Chem. C 2010, 114, 12133-12138
27. Jensen, K. M. Ø.; Christensen, M.; Tyrsted, C.; Bremholm, M.; Iversen, B. B. Structure, Size, and Morphology Control of Nanocrystalline Lithium Cobalt Oxide Cryst. Growth Des. 2011, 11, 753-758
28. 4 Nanoparticles J. Appl. Crystallogr. 2011, 44, 287-294
29. 3 Under Hydrothermal Conditions Eur. J. Inorg. Chem. 2011, 2011, 2221-2226
30. Tyrsted, C.; Pauw, B. R.; Jensen, K. M. O.; Becker, J.; Christensen, M.; Iversen, B. B. Watching Nanoparticles Form: An In Situ (Small-/Wide-Angle X-ray Scattering/Total Scattering) Study of the Growth of Yttria-Stabilised Zirconia in Supercritical Fluids Chem.-Eur. J. 2012, 18, 5759-5766
31. 6 Nanomaterials Eur. J. Inorg. Chem. 2012, 783-789
32. Walton, R. I.; OHare, D. Watching Solids Crystallise Using in Situ Powder Diffraction Chem. Commun. 2000, 2, 2283-2291
33. 4 J. Am. Chem. Soc. 2012, 134, 17889-17891
34. Cheetham, A. K.; Mellot, C. F. In Situ Studies of the Sol-Gel Synthesis of Materials Chem. Mater. 1997, 9, 2269-2279
35. 3 Nanocrystallites: An in Situ Study Cryst. Growth Des. 2014, 14, 1307-1313
36. Billinge, S. J. L.; Kanatzidis, M. G. Beyond Crystallography: The Study of Disorder, Nanocrystallinity and Crystallographically Challenged Materials with Pair Distribution Functions Chem. Commun. 2004, 749-760
37. Billinge, S. J. L. Nanostructure Studied Using the Atomic Pair Distribution Function Z. Kristallogr. 2007, 17-26
38. 2 Nanoparticle Formation and Growth during Hydrothermal Synthesis: An In Situ Total Scattering Study J. Am. Chem. Soc. 2012, 134, 6785-6792
39. Tyrsted, C.; Jensen, K. M. O.; Bojesen, E. D.; Lock, N.; Christensen, M.; Billinge, S. J. L.; Iversen, B. B. Understanding the Formation and Evolution of Ceria Nanoparticles under Hydrothermal Conditions Angew. Chem., Int. Ed. 2012, 51, 9030-9033
40. 3 Nanoparticle Formation under Hydrothermal Conditions Angew. Chem., Int. Ed. 2014, 53, 3667-3670
41. Tyrsted, C.; Lock, N.; Jensen, K. M. O.; Christensen, M.; Bojesen, E. D.; Emerich, H.; Vaughan, G.; Billinge, S. J. L.; Iversen, B. B. Evolution of Atomic Structure during Nanoparticle Formation IUCrJ. 2014, 1, 165-171
42. Adschiri, T.; Hakuta, Y.; Arai, K. Hydrothermal Synthesis of Metal Oxide Fine Particles at Supercritical Conditions Ind. Eng. Chem. Res. 2000, 39, 4901-4907
43. Park, S. Preparation of Iron Oxides using Ammonium Iron Citrate Precursor: Thin Films and Nanoparticles J. Solid State Chem. 2009, 182, 2456-2460
44. Jensen, K. M. Ø. Watching Materials Form: Particle Formation and Growth in Hydrothermal Synthesis. Ph.D. Thesis, Aarhus University, 2013.
45. Shannon, R. D. Revised Effective Ionic-Radii and Systematic Studies of Interatomic Distances in Halides and Chalcogenides Acta Crystallogr., Sect. A 1976, 32, 751-767
46. Silva, A. M. N.; Kong, X.; Parkin, M. C.; Cammack, R.; Hider, R. C. Iron(III) Citrate Speciation in Aqueous Solution Dalton Trans. 2009, 40, 8616-8625
47. Vukosav, P.; Mlakar, M.; Tomisic, V. Revision of Iron(III)-Citrate Speciation in Aqueous Solution. Voltammetric and Spectrophotometric Studies Anal. Chim. Acta 2012, 745, 85-91
48. Shweky, I.; Bino, A.; Goldberg, D. P.; Lippard, S. J. Syntheses, Structures, and Magnetic-Properties of 2 Dinuclear Iron(Iii) Citrate Complexes Inorg. Chem. 1994, 33, 5161-5162
49. Celic, T. B.; Jaglicic, Z.; Lazar, K.; Logar, N. Z. Structure and Magnetic Properties of a New Iron(II) Citrate Coordination Polymer Acta Crystallogr. Sect. B: Struct. Sci. 2013, 69, 490-495
50. Hussein, G. A. M. Physicochemical Investigation of the Decomposition Products of Ammonium Metal Carboxylates-Ammonium Ferric Citrate Hydrate Powder Technol. 1994, 80, 265-270
51. Gajbhiye, N. S.; Bhattacharya, U.; Darshane, V. S. Thermal-Decomposition of Zinc-Iron Citrate Precursor Thermochim. Acta 1995, 264, 219-230
52. Rayner-Canham, G.; Overton, T. Descriptive Inorganic Chemistry. W.H. Freeman and Company: New York, 2010.
53. Flynn, C. M. Hydrolysis of Inorganic Iron(III) Salts Chem. Rev. 1984, 84, 31-41
54. Magini, M.; Radnai, T. X-Ray-Diffraction Study of Ferric-Chloride Solutions and Hydrated Melt-Analysis of the Iron (III)-Chloride Complexes Formation J. Chem. Phys. 1979, 71, 4255-4262
55. 3 J. Am. Ceram. Soc. 2001, 84, 2313-2317
56. Yu, J. G.; Yu, X. X.; Huang, B. B.; Zhang, X. Y.; Dai, Y. Hydrothermal Synthesis and Visible-Light Photocatalytic Activity of Novel Cage-like Ferric Oxide Hollow Spheres Cryst. Growth Des. 2009, 9, 1474-1480
57. Wang, S. B.; Min, Y. L.; Yu, S. H. Synthesis and Magnetic Properties of Uniform Hematite Nanocubes J. Phys. Chem. C 2007, 111, 3551-3554
58. Jing, Z. H.; Wu, S. H. Synthesis and Characterization of Monodisperse Hematite Nanoparticles Modified by Surfactants via Hydrothermal Approach Mater. Lett. 2004, 58, 3637-3640
59. 3 J. Solid State Chem. 1983, 49, 325-333
60. 4 Nanoparticles with Improved Magnetic Properties Mater. Res. Bull. 2003, 38, 1113-1118
61. Kodama, R. H. Magnetic Nanoparticles J. Magn. Magn. Mater. 1999, 200, 359-372
62. Kvick, A. Materials Science Research at the European Synchrotron Radiation Facility Nucl. Instrum. Methods Phys. Res. Sect. B 2003, 199, 531-535
63. Becker, J.; Bremholm, M.; Tyrsted, C.; Pauw, B.; Jensen, K. M. O.; Eltzholt, J.; Christensen, M.; Iversen, B. B. Experimental Setup for in Situ X-ray SAXS/WAXS/PDF Studies of the Formation and Growth of Nanoparticles in Near- and Supercritical Fluids J. Appl. Crystallogr. 2010, 43, 729-736
64. Hammersley, A. P.; Svensson, S. O.; Hanfland, M.; Fitch, A. N.; Hausermann, D. Two-Dimensional Detector Software: From Real Detector to Idealised Image or Two-Theta Scan High Pressure Res. 1996, 14, 235-248
65. Juhas, P.; Davis, T.; Farrow, C. L.; Billinge, S. J. L. PDFgetX3: A Rapid and Highly Automatable Program for Processing Powder Diffraction Data Into Total Scattering Pair Distribution Functions J. Appl. Crystallogr. 2013, 46, 560-566
66. Farrow, C. L.; Juhas, P.; Liu, J. W.; Bryndin, D.; Bozin, E. S.; Bloch, J.; Proffen, T.; Billinge, S. J. L. PDFfit2 and PDFgui: Computer Programs for Studying Nanostructure in Crystals J. Phys.: Condens. Matter 2007, 19, 335219