Chromatographic separation of PTAD-derivatized 25-hydroxyvitamin D3 and its C-3 epimer from human serum and murine skin

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 991, Issue , 2015, Pages 118-121

  Teegarden, Matthew D ^a   Riedl, Kenneth M ^a   Schwartz, Steven J ^a  

^a OHIO STATE UNIVERSITY   (United States)

Author keywords

25 Hydroxyvitamin D analysis; C3 epi 25 hydroxyvitamin D; HPLC MS MS; PTAD; Vitamin D

Indexed keywords

ATMOSPHERIC IONIZATION; ATMOSPHERIC PRESSURE; CHEMICAL DETECTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLITES; PHASE SEPARATION; VITAMINS;

25-HYDROXYVITAMIN D; ATMOSPHERIC PRESSURE CHEMICAL IONIZATION; CHROMATOGRAPHIC SEPARATIONS; DETECTION AND QUANTIFICATIONS; HPLC-MS/MS; LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY (LC MS/MS); PTAD; VITAMIN-D;

BODY FLUIDS;

3 EPI 25 HYDROXYVITAMIN D; 4 PHENYL 1,2,4 TRIAZOLINE 3,5 DIONE; CALCIFEDIOL; TRIAZOLINE DERIVATIVE; UNCLASSIFIED DRUG; VITAMIN D DERIVATIVE; 4-PHENYL-1,2,4-TRIAZOLINE-3,5-DIONE; TRIAZOLE DERIVATIVE; VITAMIN;

ADULT; ARTICLE; BLOOD SAMPLING; CORD SERUM; DERIVATIZATION; DILUTION; ELUTION; EPIMER; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; LIPOPHILICITY; MALE; METABOLITE; MOUSE; NONHUMAN; PARTICLE SIZE; PRIORITY JOURNAL; SKIN; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; ANIMAL; BLOOD; CHEMISTRY; EVALUATION STUDY; ISOLATION AND PURIFICATION; PROCEDURES; STEREOISOMERISM;

MURINAE;

ANIMALS; CALCIFEDIOL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; MALE; MICE; SKIN; SOLID PHASE EXTRACTION; STEREOISOMERISM; TANDEM MASS SPECTROMETRY; TRIAZOLES; VITAMINS;

EID: 84928749409     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2015.04.011     Document Type: Article

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