Assessing stability-indicating methods for coelution by two-dimensional liquid chromatography with mass spectrometric detection

Journal of Separation Science

Volumn 37, Issue 22, 2014, Pages 3214-3225

  Venkatramani, C J ^a   Girotti, James ^a   Wigman, Larry ^a   Chetwyn, Nicholas ^a  

^a GENENTECH INC   (United States)

Author keywords

Mass spectrometry; Multidimensional chromatography; Pharmaceutical analysis; Pseudocomprehensive analysis; Stability indicating methods

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; DRUG PRODUCTS; LIQUIDS; MASS SPECTROMETRY; PHASE SEPARATION;

ACTIVE PHARMACEUTICAL INGREDIENTS; MASS SPECTROMETRIC DETECTION; MULTIDIMENSIONAL CHROMATOGRAPHY; PHARMACEUTICAL ANALYSIS; PSEUDOCOMPREHENSIVE ANALYSIS; STABILITY INDICATING METHOD; TWO-DIMENSIONAL CHROMATOGRAPHY; TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY;

LIQUID CHROMATOGRAPHY;

BENZOIC ACID DERIVATIVE; CORTICOSTERONE; DRUG;

ARTICLE; CHROMATOGRAPHY; DRUG IMPURITY; ELUTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PHASE SEPARATION; TWO DIMENSIONAL LIQUID CHROMATOGRAPHY; CHEMICAL PHENOMENA; CHEMISTRY; DRUG CONTAMINATION; LABORATORY DIAGNOSIS; MEDICINAL CHEMISTRY; REPRODUCIBILITY;

BENZOATES; CHEMISTRY, PHARMACEUTICAL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, LIQUID; DRUG CONTAMINATION; FALSE NEGATIVE REACTIONS; HYDROPHOBIC AND HYDROPHILIC INTERACTIONS; MASS SPECTROMETRY; PHARMACEUTICAL PREPARATIONS; REPRODUCIBILITY OF RESULTS;

EID: 84910133393     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201400590     Document Type: Article

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