Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4 and LiFe1-xMnxPO4 nanoparticles

Journal of Applied Crystallography

Volumn 44, Issue 2, 2011, Pages 287-294

  Jensen, Kirsten ^a   Christensen, Mogens ^a   Tyrsted, Christoffer ^a   Iversen, Bo Brummerstedt ^a  

^a AARHUS UNIVERSITY   (Denmark)

Author keywords

antisite defects; hydrothermal synthesis; in situ X ray diffraction; Li ion batteries

Indexed keywords

ANTI-SITE DEFECT; DEFECT-FREE; FLOW SYNTHESIS; IN SITU X-RAY DIFFRACTION; IN-SITU; IN-SITU SYNCHROTRONS; INTERMEDIATE PHASE; IRON PRECURSORS; LI-ION BATTERIES; LIFEPO; LIFEPO4; LOW TEMPERATURES; MANGANESE DOPING; POWDER X RAY DIFFRACTION; POWDER X-RAY DIFFRACTION (PXRD); REACTION TIME; SUPER-CRITICAL; SUPERCRITICAL CONDITION;

AMMONIUM COMPOUNDS; DEFECTS; DIFFRACTION; LITHIUM ALLOYS; MANGANESE; NANOPARTICLES; REACTION INTERMEDIATES; SYNCHROTRONS; X RAY DIFFRACTION; X RAYS;

HYDROTHERMAL SYNTHESIS;

EID: 79953058873     PISSN: 00218898     EISSN: 16005767     Source Type: Journal    
DOI: 10.1107/S0021889811006522     Document Type: Article

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