Analysis of trace organic compounds in environmental, food and biological matrices using large-volume sample injection in column-switching liquid chromatography

TrAC - Trends in Analytical Chemistry

Volumn 62, Issue , 2014, Pages 69-85

  Fernández Ramos, Carolina ^a   Šatínský, Dalibor ^a   Šmídová, Barbora ^a   Solich, Petr ^a  

^a Charles University in Prague Faculty of Pharmacy   (Czech Republic)

Author keywords

Biological sample; Column switching chromatography; Contaminant; Environmental sample; Food sample; High performance liquid chromatography; Large volume sample injection; On line solid phase extraction; Solid phase extraction; Trace analysis

Indexed keywords

ADDITIVES; CHEMICAL CONTAMINATION; CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IMPURITIES; LIQUIDS; ORGANIC COMPOUNDS; PHASE SEPARATION; TRACE ANALYSIS;

BIOLOGICAL SAMPLES; COLUMN SWITCHING; ENVIRONMENTAL SAMPLE; FOOD SAMPLES; LARGE-VOLUME SAMPLE INJECTION; ON-LINE SOLID PHASE EXTRACTION; SOLID-PHASE EXTRACTION;

EXTRACTION;

ORGANIC COMPOUND;

ANTIBODY AFFINITY; AQUATIC ENVIRONMENT; BODY FLUID; CHEMICAL ANALYSIS; COLUMN CHROMATOGRAPHY; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHOBICITY; LIMIT OF DETECTION; PARTICLE SIZE; PHYSICAL CHEMISTRY; PROCESS OPTIMIZATION; REVIEW; SEPARATION TECHNIQUE; URINALYSIS; WATER SAMPLING;

EID: 84907465513     PISSN: 01659936     EISSN: 18793142     Source Type: Journal    
DOI: 10.1016/j.trac.2014.07.008     Document Type: Review

References (77)

1. Petrovic M., Farré M., de Alda M.L., Perez S., Postigo C., Köck M., et al. Recent trends in the liquid chromatography-mass spectrometry analysis of organic contaminants in environmental samples. J. Chromatogr. A 2010, 1217:4004-4017.
2. Armenta S., Garrigues S., de la Guardia M. Green analytical chemistry. TrAC Trend. Anal. Chem 2008, 27:497-511.
3. Rybár I., Góra R., Hutta M. Method of fast trace microanalysis of the chiral pesticides epoxiconazole and novaluron in soil samples using off-line flow through extraction and on-column direct large volume injection in reversed-phase high performance liquid chromatography. J. Sep. Sci 2007, 30:3164-3173.
4. Busetti F., Backe W.J., Bendixen N., Maier U., Place B., Giger W., et al. Trace analysis of environmental matrices by large-volume injection and liquid chromatography-mass spectrometry. Anal. Bional. Chem 2012, 402:175-186.
5. Kiso Y., Li H., Shigetoh K., Kitao T., Jinno K. Pesticide analysis by high performance liquid chromatography using the direct injection method. J. Chromatogr. A 1996, 733:259-265.
6. Ingelse B.A., van Dam R.C.J., Vreeken R.J., Mol H.G.J., Steijger O.M. Determination of polar organophosphorous pesticides in aqueous samples by direct injection using liquid chromatography-tandem mass spectrometry. J. Chromatogr. A 2001, 918:67-78.
7. Simpkins S.W., Bedard J.W., Groskreutz S.R., Swenson M.M., Liskutin T.E., Stoll D.R. Targeted three-dimensional liquid chromatography: a versatile tool for quantitative trace analysis in complex matrices. J. Chromatogr. A 2010, 1217:7648-7660.
8. Sadílek P., Šatínský D., Solich P. Using restricted-access materials and column switching in high-performance liquid chromatography for direct analysis of biologically-active compounds in complex matrices. TrAC Trend. Anal. Chem 2007, 26:375-384.
9. Rogatsky E., Braaten K., Cruikshank G., Jayatillake H., Zheng B., Stein D.T. Flow inconsistency: the evil twin of column switching - Hardware aspects. J. Chromatogr. A 2009, 1216:7721-7727.
10. Slobodník J., Lingeman H., Brinkman U.A.T. Large-volume liquid chromatographic trace-enrichment system for environmental analysis. Chromatographia 1999, 50:141-149.
11. Lara F.J., del Olmo-Iruela M., García-Campaña A.M. On-line anion exchange solid-phase extraction coupled to liquid chromatography with fluorescence detection to determine quinolones in water and human urine. J. Chromatogr. A 2013, 1310:91-97.
12. Nováková L. Challenges in the development of bioanalytical liquid chromatography-mass spectrometry method with emphasis on fast analysis. J. Chromatogr. A 2013, 1292:25-37.
13. Kole P.L., Venkatesh G., Kotecha J., Sheshala R. Recent advances in sample preparation techniques for effective bioanalytical methods. Biomed. Chromatogr 2011, 25:199-217.
14. Huntscha S., Singer H.P., McArdell C.S., Frank C.E., Hollender J. Multiresidue analysis of 88 polar organic micropollutants in ground, surface and wastewater using on line mixed bed multilayer solid phase extraction coupled to high performance liquid chromatography- tandem mass spectrometry. J. Chromatogr. A 2012, 1268:74-83.
15. Ou J., Hu L., Hu L., Li X., Zou H. Determination of phenolic compounds in river water with on line coupling bisphenol A imprinted monolithic precolumn with high performance liquid chromatography. Talanta 2006, 69:1001-1006.
16. Chávez-Moreno C.A., Guzmán-Mar J.L., Hinojosa-Reyes L., Hernández-Ramírez A., Ferrer L., Cerdá V. Applicability of multisyringe chromatography coupled to on line solid phase extraction to the simultaneous determination of dicamba, 2,4-D, and atrazine. Anal. Bional. Chem 2012, 403:2705-2714.
17. Ammerman J.L., Aldstadt J.H. Monolithic solid-phase extraction for the rapid on-line monitoring of microcystins in surface waters. Microchim. Acta 2009, 164:185-196.
18. Zhu T., Row K.H. A weak cation-exchange monolithic SPE column for extraction and analysis of caffeine and theophylline in human urine. Chromatographia 2009, 69:1477-1480.
19. Núñez O., Gallart-Ayala H., Martins C.P.B., Lucci P. New trends in fast liquid chromatography for food and environmental analysis. J. Chromatogr. A 2012, 1228:298-323.
20. Rodriguez-Mozaz S., Lopez de Alda M.J., Barceló D. Advantages and limitations of on-line solid phase extraction coupled to liquid chromatography-mass spectrometry technologies versus biosensors for monitoring of emerging contaminants in water. J. Chromatogr. A 2007, 1152:97-115.
21. Gros M., Pizzolato T.M., Petrovic M., Lopez de Alda M.J., Barceló D. Trace level determination of β-blockers in waste waters by highly selective molecularly imprinted polymers extraction followed by liquid chromatography-quadrupole-linear ion trap mass spectrometry. J. Chromatogr. A 2008, 1189:374-384.
22. O'Connor S., Aga D.S. Analysis of tetracycline antibiotics in soil: advances in extraction, clean-up, and quantification. TrAC Trend. Anal. Chem 2007, 26:456-465.
23. Hoshina K., Horiyama S., Matsunaga H., Haginaka J. Molecularly imprinted polymers for simultaneous determination of antiepileptics in river water samples by liquid chromatography-tandem mass spectrometry. J. Chromatogr. A 2009, 1216:4957-4962.
24. Zhao C., Guan X., Liu X., Zhang H. Synthesis of molecularly imprinted polymer using attapulgite as matrix by ultrasonic irradiation for simultaneous on-line solid phase extraction and high performance liquid chromatography determination of four estrogens. J. Chromatogr. A 2012, 1229:72-78.
25. Hoshina K., Horiyama S., Matsunaga H., Haginaka J. Simultaneous determination of non-steroidal anti-inflammatory drugs in river water samples by liquid chromatography tandem mass spectrometry using molecularly imprinted polymers as a pretreatment column. J. Pharm. Biomed. Anal 2011, 55:916-922.
26. Beltran A., Borrull F., Cormack P.A.G., Marcé R.M. Molecularly-imprinted polymers: useful sorbent for selective extractions. TrAC Trend. Anal. Chem 2010, 29:1363-1375.
27. Xu W., Su S., Jiang P., Wang H., Dong X., Zhang M. Determination of sulfonamides in bovine milk with column-switching high performance liquid chromatography using surface imprinted silica with hydrophilic external layer as restricted access and selective extraction material. J. Chromatogr. A 2010, 1217:7198-7207.
28. Watabe Y., Kubo T., Nishikawa T., Fujita T., Kaya K., Hosoya K. Fully automated liquid chromatography-mass spectrometry determination of 17-β-estradiol in river water. J. Chromatogr. A 2006, 1120:252-259.
29. Sambe H., Hoshina K., Haginaka J. Molecularly imprinted polymers for triazine herbicides prepared by multi-step swelling and polymerization method. Their application to the determination of methylthiotriazine herbicides in river water. J. Chromatogr. A 2007, 1152:130-137.
30. Gallart-Ayala H., Moyano E., Galceran M.T. On-line solid phase extraction fast liquid chromatography-tandem mass spectrometry for the analysis of bisphenol A and its chlorinated derivatives in water samples. J. Chromatogr. A 2010, 1217:3511-3518.
31. Wode F., Reilich C., van Baar P., Dünnbier U., Jekel M., Reemtsma T. Multiresidue analytical method for the simultaneous determination of 72 micropollutants in aqueous samples with ultra high performance liquid chromatography-high resolution mass spectrometry. J. Chromatogr. A 2012, 1270:118-126.
32. Kortz L., Dorow J., Becker S., Thiery J., Ceglarek U. Fast liquid chromatography-quadrupole linear ion trap mass spectrometry analysis of polyunsaturated fatty acids and eicosanoids in human plasma. J. Chromatogr. B 2013, 927:209-213.
33. Calleri E., Marrubini G., Brusotti G., Massolini G., Caccialanza G. Development and integration of an immunoaffinity monolithic disk for the on-line solid phase extraction and HPLC determination with fluorescence detection of aflatoxin B1 in aqueous solutions. J. Pharm. Biomed. Anal 2007, 44:396-403.
34. Li L., Wang J., Zhou S., Zhao M. Development and characterization of an immunoaffinity monolith for selective on line extraction of bisphenol A from environmental water samples. Anal. Chim. Acta 2008, 620:1-7.
35. García M.D.G., Pedrosa B.P., Galera M.M. Column-switching linked to large sample volumes to preconcentrate β-blockers at trace levels in environmental water. Talanta 2011, 83:1665-1672.
36. Nunez O., Gallart-Ayala H., Martins C.P.B., Lucci P., Busquets R. State of the art in fast liquid chromatography-mass spectrometry for bio-analytical applications. J. Chromatogr. B 2013, 927:3-21.
37. Šatínský D., Havlíková L., Solich P. HPLC column-switching technique for sample preparation and fluorescence determination of propranolol in urine using fused-core columns in both dimensions. Anal. Bioanal. Chem 2013, 405:6583-6587.
38. Beltrán E., Ibañez M., Sancho J.V., Hernández F. Determination of six microcystins and nodularin in surface and drinking waters by on line solid phase extraction-ultra high pressure liquid chromatography tandem mass spectrometry. J. Chromatogr. A 2012, 1266:61-68.
39. Gosetti F., Chiuminatto U., Mazzucco E., Robotti E., Calabrese G., Gennaro M.C., et al. Simultaneous determination of thirteen polycyclic aromatic hydrocarbons and twelve aldehydes in cooked food by an automated on line solid phase extraction ultra high performance liquid chromatography tandem mass spectrometry. J. Chromatogr. A 2011, 1218:6308-6318.
40. Gosetti F., Chiuminatto U., Zampieri D., Mazzucco E., Robotti E., Calabrese G., et al. Determination of perfluorochemicals in biological, environmental and food samples by an automated on-line solid phase extraction ultra high performance liquid chromatography tandem mass spectrometry method. J. Chromatogr. A 2010, 1217:7864-7872.
41. Vega-Morales T., Sosa-Ferrera Z., Santana-Rodríguez J.J. Development and optimisation of an on-line solid phase extraction coupled to ultra-high-performance liquid chromatography-tandem mass spectrometry methodology for the simultaneous determination of endocrine disrupting compounds in wastewater samples. J. Chromatogr. A 2012, 1230:66-76.
42. Chiuminatto U., Gosetti F., Dossetto P., Mazzucco E., Zampieri D., Robotti E., et al. Automated Online Solid Phase Extraction Ultra High Performance Liquid Chromatography Method Coupled with Tandem Mass Spectrometry for Determination of Forty-Two Therapeutic Drugs and Drugs of Abuse in Human Urine. Anal. Chem 2010, 82:5636-5645.
43. van der Heeft E., Dijkman E., Baumann R.A., Hogendoorn E.A. Comparison of various liquid chromatographic methods involving UV and atmospheric pressure chemical ionization mass spectrometric detection for the efficient trace analysis of phenylurea herbicides in various types of water samples. J. Chromatogr. A 2000, 879:39-50.
44. Hutta M., Rybár I., Chalányová M. Liquid chromatographic method development for determination of fungicide epoxiconazole enantiomers by achiral and chiral column switching technique in water and soil. J. Chromatogr. A 2002, 959:143-152.
45. Hogendoorn E.A., Huls R., Dijkman E., Hoogerbrugge R. Microwave assisted solvent extraction and coupled-column reversed-phase liquid chromatography with UV detection: use of an analytical restricted-access-medium column for the efficient multi-residue analysis of acidic pesticides in soils. J. Chromatogr. A 2001, 938:23-33.
46. Hutta M., Chalányová M., Halko R., Góra R., Dokupilová S., Rybár I. Reversed phase liquid chromatography trace analysis of pesticides in soil by on-column sample pumping large volume injection and UV detection. J. Sep. Sci 2009, 32:2034-2042.
47. Hutta M., Chalányová M., Halko R., Góra R., Rybár I., Pajchl M., et al. New approach to large-volume injection in reversed-phase high performance liquid chromatography: determination of atrazine and hydroxyatrazine in soil samples. J. Sep. Sci 2006, 29:1977-1987.
48. Galera M.M., García M.D.G., Culzoni M.J., Goicoechea H.C. Determination of pharmaceuticals in river water by column switching of large simple volumes and liquid chromatography-diode array detection, assisted by chemometrics: an integrated approach to green analytical methodologies. J. Chromatogr. A 2010, 1217:2042-2049.
49. Chalányová M., Hutta M., Pagáč M. On-line flow - through extraction-preconcentration - large volume injection-RP LC for trace determination of pyrethroids in Slovak soil. J. Sep. Sci 2010, 33:134-142.
50. Chalányová M., Paulechová M., Hutta M. Method of analysis of a selected group of pyrethroids in soil samples using off-line flow-through extraction and on-column direct large volume injection in reversed phase high performance liquid chromatography. J. Sep. Sci 2006, 29:2149-2157.
51. Singer H., Jaus S., Hanke I., Lück A., Hollender J., Alder A.C. Determination of biocides and pesticides by on line solid phase extraction coupled with mass spectrometry and their behavior in wastewater and surface water. Environ. Pollut 2010, 158:3054-3064.
52. López de Alda M.J., Barceló D. Determination of steroid sex hormones and related synthetic compounds considered as endocrine disrupters in water by fully automated on-line solid phase extraction liquid chromatography-diode array detection. J. Chromatogr. A 2001, 911:203-210.
53. Stoob K., Singer H.P., Goetz C.W., Ruff M., Mueller S.R. Fully automated on line solid phase extraction coupled directly to liquid chromatography-tandem mass spectrometry. Quantification of sulfonamide antibiotics, neutral and acidic pesticides at low concentrations in surface waters. J. Chromatogr. A 2005, 1097:138-147.
54. Peng X.T., Shi Z.G., Feng Y.Q. Rapid and high throughput determination of cationic surfactants in environmental water samples by automated on-line polymer monolith microextraction coupled to high performance liquid chromatography-mass spectrometry. J. Chromatogr. A 2011, 1218:3588-3594.
55. Negreira N., López de Alda M., Barceló D. On-line solid phase extraction-liquid chromatography-tandem mass spectrometry for the determination of 17 cytostatics and metabolites in waste, surface and ground waters samples. J. Chromatogr. A 2013, 1280:64-74.
56. García-Ac A., Segura P.A., Viglino L., Fürtos A., Gagnon C., Prévost M., et al. On-line solid phase extraction of large volume injections coupled to liquid chromatography-tandem mass spectrometry for the quantitation and confirmation of 14 selected trace organic contaminants in drinking and surface water. J. Chromatogr. A 2009, 1216:8518-8527.
57. Ripollés C., Sancho J.V., López F.J., Hernández F. Liquid chromatography coupled to tandem mass spectrometry for the residue determination of ethylenethiourea (ETU) and propylenethiourea (PTU) in water. J. Chromatogr. A 2012, 1243:53-61.
58. Crescenzi C., Albiñana J., Carlsson H., Holmgren E., Batlle R. On-line strategies for determining trace levels of nitroaromatic explosives and related compounds in water. J. Chromatogr. A 2007, 1153:186-193.
59. Guo F., Liu Q., Qu G.B., Song S.J., Sun J.T., Shi J.B., et al. Simultaneous determination of five estrogens and four androgens in water samples by online solid-phase extraction coupled with high-performance liquid chromatography-tandem mass spectrometry. J. Chromatogr. A 2013, 1281:9-18.
60. Ding J., Ren N., Chen L., Ding L. On-line coupling of solid-phase extraction to liquid chromatography-tandem mass spectrometry for the determination of macrolide antibiotics in environmental water. Anal. Chim. Acta 2009, 634:215-221.
61. García-Galán M.J., Díaz-Cruz M.S., Barceló D. Determination of 19 sulfonamides in environmental water samples by automated on-line solid-phase extraction-liquid chromatography-tandem mass spectrometry (SPE-LC-MS/MS). Talanta 2010, 81:355-366.
62. Asperger A., Efer J., Koal T., Engewald W. Trace determination of priority pesticides in water by means of high-speed on-line solid-phase extraction-liquid chromatography-tandem mass spectrometry using turbulent-flow chromatography columns for enrichment and a short monolithic column for fast liquid chromatographic separation. J. Chromatogr. A 2002, 960:109-119.
63. Hurtado-Sánchez M.C., Romero-González R., Rodríguez-Cáceres M.I., Durán-Merás I., Garrido Frenich A. Rapid and sensitive on-line solid phase extraction-ultra high performance liquid chromatography-electrospray-tandem mass spectrometry analysis of pesticides in surface waters. J. Chromatogr. A 2013, 1305:193-202.
64. Ciofi L., Fibbi D., Chiuminatto U., Coppini E., Checchini L., Del Bubba M. Fully-automated on-line solid phase extraction coupled to high-performance liquid chromatography-tandem mass spectrometric analysis at sub-ng/L levels of selected estrogens in surface water and wastewater. J. Chromatogr. A 2013, 1283:53-61.
65. Gosetti F., Chiuminatto U., Zampieri D., Mazzucco E., Marengo E., Gennaro M.C. A new on-line solid phase extraction high performance liquid chromatography tandem mass spectrometry method to study the sun light photodegradation of mono-chloroanilines in river water. J. Chromatogr. A 2010, 1217:3427-3434.
66. Amini N., Crescenzi C. Feasibility of an on-line restricted access material/liquid chromatography/tandem mass spectrometry method in the rapid and sensitive determination of organophosphorous triesters in human blood plasma. J. Chromatogr. B 2003, 795:245-256.
67. Preuss R., Koch H.M., Angerer J. Biological monitoring of the five major metabolites of di-(2-ethylhexyl)phthalate (DEHP) in human urine using column-switching liquid chromatography-tandem mass spectrometry. J. Chromatogr. B 2005, 816:269-280.
68. Gordi T., Nielsen E., Yu Z., Westerlund D., Ashton M. Direct analysis of artemisinin in plasma and saliva using coupled-column high-performance liquid chromatography with a restricted-access material pre-column. J. Chromatogr. B 2000, 74:155-162.
69. Ye X., Tao L.J., Needham L.L., Calafat A.M. Automated on-line column-switching HPLC-MS/MS method for measuring environmental phenols and parabens in serum. Talanta 2008, 76:865-871.
70. Ye X., Bishop A.M., Needham L.L., Calafat A.M. Automated on-line column-switching HPLC-MS/MS method with peak focusing for measuring parabens, triclosan and other environmental phenols in human milk. Anal. Chim. Acta 2008, 622:150-156.
71. Šatínský D., Brabcová I., Solich P. A fast on-line micro-column sample pretreatment with a HPLC column switching technique and large volume sample injection for determination of non-steroidal anti-inflammatory drugs in human serum. Anal. Methods 2013, 5:6153-6159.
72. Wilson S.R., Jankowski M., Pepaj M., Mihailova A., Boix F., Truyols G.V., et al. 2D LC separation and determination of bradykinin in rat muscle tissue dialysate with on-line SPE-HILIC-SPE-RP-MS. Chromatographia 2007, 66:469-474.
73. Preuss R., Angerer J. Simultaneous determination of 1- and 2-naphtol in human urine using on-line clean-up column-switching liquid chromatography-fluorescence detection. J. Chromatogr. B 2004, 801:307-316.
74. Christiaens B., Chiap P., Rbeida O., Cello D., Crommen J., Hubert P. Fully automated method for the liquid chromatographic determination of cyproterone acetate in plasma using restricted access material for sample pre-treatment. J. Chromatogr. B 2003, 795:73-82.
75. Zhixiang X., Shuo W., Guozhen F., Jiajia S., Yan Z. On-line SPE coupled with LC for analysis of traces of sudan dyes in foods. Chromatographia 2010, 71:397-403.
76. Chen L., Ding L., Jin H., Song D., Zhang H., Li J., et al. The determination of organochlorine pesticides based on dynamic microwave-assisted extraction coupled with on-line solid-phase extraction of high-performance liquid chromatography. Anal. Chim. Acta 2007, 589:239-246.
77. Vázquez P.P., García M.D.G., Martínez D.B., Galera M.M. Application of coupled-column liquid chromatography combined with post-column photochemically induced fluorimetry derivatization and fluorescence detection to the determination of pyrethroid insecticides in vegetable samples. Anal. Bioanal. Chem 2005, 381:1217-1225.