Method of fast trace microanalysis of the chiral pesticides epoxiconazole and novaluron in soil samples using off-line flow-through extraction and on-column direct large volume injection in reversed-phase high performance liquid chromatography

Journal of Separation Science

Volumn 30, Issue 18, 2007, Pages 3164-3173

  Rybár, Ivan ^a   Góra, Robert ^a   Hutta, Milan ^a  

^a Faculty of Natural Sciences   (Slovakia)

Author keywords

Direct flow through extraction; Epoxiconazole; Large volume injection (LVI) HPLC; Novaluron; Soil micro sample

Indexed keywords

DIRECT FLOW-THROUGH EXTRACTION; EPOXICONAZOLE; LARGE VOLUME INJECTION; NOVALURON;

ENANTIOMERS; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MICROANALYSIS; TRACE ANALYSIS;

PESTICIDES;

EPOXICONAZOLE; FUNGICIDE; INSECTICIDE; NOVALURON; PESTICIDE; UNCLASSIFIED DRUG; WATER;

AGRICULTURE; ANALYTIC METHOD; ARTICLE; CALIBRATION; CHEMICAL ANALYSIS; CHIRAL CHROMATOGRAPHY; COLUMN CHROMATOGRAPHY; CONTROLLED STUDY; ENANTIOMER; MICROANALYSIS; OFF LINE FLOW THROUGH EXTRACTION; ON COLUMN DIRECT LARGE VOLUME INJECTION; PRIORITY JOURNAL; RADIATION DETECTION; REPRODUCIBILITY; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SLOVAKIA; SOIL ANALYSIS; SOIL QUALITY; ULTRAVIOLET RADIATION;

CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; EPOXY COMPOUNDS; FLOW INJECTION ANALYSIS; HYDROPHOBICITY; MOLECULAR STRUCTURE; PESTICIDES; PHENYLUREA COMPOUNDS; REPRODUCIBILITY OF RESULTS; SOIL; STEREOISOMERISM; TIME FACTORS; TRIAZOLES;

EID: 37849044365     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200700180     Document Type: Article

References (35)

1. Tomlin, C. D. S. (Ed.), The e-Pesticide Manual 2000-2001, A World Compendium, The British Crop Protection Council, Twelfth Edition.
2. Barber, J. A. S., Parkin, C. S., Chowdhury, A. B. M. N. U., Crop Protection 2003, 22, 949-957.
3. Blake, G. R., Hartge, K. H., in: A., Klute (Ed.), Methods of Soil Analysis, Part I. Physical and Mineralogical Methods, Agronomy Monograph No. 9 (2nd Edn.), American Society of Agronomy, Madison, WI, 1986, pp. 363-375.
4. Busher, H.-P., Francotte, E., in Ahuja, S. (Ed.), Chiral Separations: Applications and Technology, ACS, Washington, DC, 1997, pp. 93-138.
5. Buser, H. R., Muller, M. D., Environ. Sci. Technol. 1995, 29, 664-672.
6. Bromilow, R. H., Evans, A. A., Nicholls, P. H., Pestic. Sci. 1999, 55, 1129-1134.
7. Bromilow, R. H., Evans, A. A., Nicholls, P. H., Pestic. Sci. 1999, 55, 1135-1142.
8. Hutta, M., Rybár, I., Chalányová, M., J. Chromatogr. A 2002, 959, 143-152.
9. Schermerhorn, P. G., Golden, P. E., Krynitsky, A. J., Leimkuehler, W. M., J. AOAC Int. 2005, 88, 1491-502.
10. Kovalczuk, T., Jech, M., Poustka, J., Hajšlová, J., Anal. Chim. Acta 2006, 577, 8-17.
11. Zrostlíková, J., Hajšlová, J., Kovalczuk, T., Štpán, R., Poustka, J., J. AOAC Int. 2003, 86, 612-622.
12. Trosken, E. R., Bittner, N., Vogel, W., J. Chromatogr. A 2005, 1083, 113-119.
13. Anastassiades, M., Scherbaum, E., Schwack, W., Deutsche Lebensmittel-Rundschau 2001, 97, 176-190.
14. CIPAC/4492/P, CIPAC Collaborative International Pesticides Analytical Council Limited Commission Internationale des Méthodes d'Analyse des Pesticides (CIMAP), Summary of the decisions taken at the 49th CIPAC Meeting in Utrecht, the Netherlands, on Wednesday, June 8, and Thursday, June 9, 2005.
15. Hutta, M., Chalányova, M., Halko, R., Góra, R., Rybár, I., Pajchl, M., Dokupilová, S., J. Sep. Sci. 2006, 29, 1977-1987.
16. Chalányová, M., Paulechová, M., Hutta, M., J. Sep. Sci. 2006, 29, 2149-2157.
17. Ruijten, H. M., van Amsterdam, P. H., de Bree, H., J. Chromatogr. 1984, 314, 183-191.
18. Ruijten, H. M., van Amsterdam, P. H., de Bree, H., Trends Anal. Chem. 1987, 5, 134-138.
19. Lagana, A., Fago, G., Marino, A., Mosso, M., Anal. Chim. Acta 1998, 375, 107-116.
20. Li, Z., Zhang, Z., Zhou, Q., Gao, R., Wang, Q., J. Chromatogr. A 2002, 997, 17-25.
21. Long, A. R., Hsieh, L. C., Malbrough, M. S., Short, C. R., Barker, S. A., J. AOAC 1990, 73, 379-384.
22. Viana, E., Moltó, J. C., Font, G., J. Chromatogr. A 1996, 754, 437-444.
23. Fernández, M., Picó, Y., Manes, J., J. Chromatogr. A 2000, 871, 43-56.
24. Tekel, J., Hudecová, T., Pecníková, K., Eur. Food Res. Technol. 2001, 213, 250-258.
25. Andreu, V., Picó, Y., Trends Anal. Chem. 2004, 23, 772-789.
26. Howell, T. A., in: Hillel, D. (Ed.), Encyclopaedia of Soils in the Environment, Oxford, UK, Elsevier Press, 2004, pp. 379-386.
27. Xu, F., Liang, X.-M., Lin, B., Su, F., Zhong, H., Schramm, K.-W., Kettrup, A., Bull. Environ. Contam. Toxicol. 1999, 63, 87-93.
28. Xu, F., Liang, X., Lin, B., Su, F., Schramm, K.-W., Kettrup, A., Chemosphere 1999, 39, 2239-2248.
29. Xu, F., Liang, X., Lin, B., J. Environ. Qual. 2002, 31, 1972-1979.
30. Xua, F., Liang, X., Lin, B., Schramm, K.-W., Kettrup, A., J. Chromatogr. A 2002, 968, 7-16.
31. Guo, R., Liang, X., Chen, J., Wu, w., Zhang, Q., Martens, D., Kettrup, A., J. Chromatogr. A 2004, 1035, 31-36.
32. Landscape Atlas of the Slovak Republic, 1st Edn., Ministry of Environment of the Slovak Republic in Bratislava, Slovak Environmental Agency in Banská Bystrica, 2002, 344 pp.
33. Hutta, M., Góra, R., J. Chromatogr. A 2003, 1012, 67-79.
34. Hubaux, A., Vos, G., Anal. Chem. 1970, 42, 849-855.
35. Burdge, J. R., MacTaggart, D. L., Farwell, S. O., J. Chem. Educ. 1999, 76, 434-439.