메뉴 건너뛰기




Volumn 118, Issue 34, 2014, Pages 19548-19555

Mechanism of solid-state thermolysis of ammonia borane: A 15N NMR study using fast magic-angle spinning and dynamic nuclear polarization

Author keywords

[No Author keywords available]

Indexed keywords

MAGIC ANGLE SPINNING; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPIN POLARIZATION; AMMONIA; CHEMICAL SHIFT; DENSITY FUNCTIONAL THEORY; DYNAMICS; POLARIZATION; POLYMER BLENDS;

EID: 84906875755     PISSN: 19327447     EISSN: 19327455     Source Type: Journal    
DOI: 10.1021/jp504328x     Document Type: Article
Times cited : (56)

References (57)
  • 1
    • 0042890410 scopus 로고    scopus 로고
    • Materials for Hydrogen Storage
    • Zuttel, A. Materials for Hydrogen Storage Mater. Today 2003, 6, 24-33
    • (2003) Mater. Today , vol.6 , pp. 24-33
    • Zuttel, A.1
  • 2
    • 0033285933 scopus 로고    scopus 로고
    • A Panoramic Overview of Hydrogen Storage Alloys from a Gas Reaction Point of View
    • Sandrock, G. A Panoramic Overview of Hydrogen Storage Alloys from a Gas Reaction Point of View J. Alloys Compd. 1999, 293, 877-888
    • (1999) J. Alloys Compd. , vol.293 , pp. 877-888
    • Sandrock, G.1
  • 3
    • 9244258546 scopus 로고    scopus 로고
    • Light Metal Hydrides and Complex Hydrides for Hydrogen Storage
    • Schuth, F.; Bogdanovic, B.; Felderhoff, M. Light Metal Hydrides and Complex Hydrides for Hydrogen Storage Chem. Commun. 2004, 2249-2258
    • (2004) Chem. Commun. , pp. 2249-2258
    • Schuth, F.1    Bogdanovic, B.2    Felderhoff, M.3
  • 7
    • 75749122603 scopus 로고    scopus 로고
    • Ammonia Borane as a Hydrogen Carrier: Dehydrogenation and Regeneration
    • Smythe, N. C.; Gordon, J. C. Ammonia Borane as a Hydrogen Carrier: Dehydrogenation and Regeneration Eur. J. Inorg. Chem. 2010, 509-521
    • (2010) Eur. J. Inorg. Chem. , pp. 509-521
    • Smythe, N.C.1    Gordon, J.C.2
  • 10
    • 0037068089 scopus 로고    scopus 로고
    • Thermal Decomposition of B-N-H Compounds Investigated by Using Combined Thermoanalytical Methods
    • Baitalow, F.; Baumann, J.; Wolf, G.; Jaenicke-Rossler, K.; Leitner, G. Thermal Decomposition of B-N-H Compounds Investigated by Using Combined Thermoanalytical Methods Thermochim. Acta 2002, 391, 159-168
    • (2002) Thermochim. Acta , vol.391 , pp. 159-168
    • Baitalow, F.1    Baumann, J.2    Wolf, G.3    Jaenicke-Rossler, K.4    Leitner, G.5
  • 11
    • 0009929387 scopus 로고    scopus 로고
    • Calorimetric Process Monitoring of Thermal Decomposition of B-N-H Compounds
    • Wolf, G.; Baumann, J.; Baitalow, F.; Hoffmann, F. P. Calorimetric Process Monitoring of Thermal Decomposition of B-N-H Compounds Thermochim. Acta 2000, 343, 19-25
    • (2000) Thermochim. Acta , vol.343 , pp. 19-25
    • Wolf, G.1    Baumann, J.2    Baitalow, F.3    Hoffmann, F.P.4
  • 12
    • 34147103836 scopus 로고    scopus 로고
    • In Situ Solid State B-11 MAS-NMR Studies of the Thermal Decomposition of Ammonia Borane: Mechanistic Studies of the Hydrogen Release Pathways from a Solid State Hydrogen Storage Material
    • Stowe, A. C.; Shaw, W. J.; Linehan, J. C.; Schmid, B.; Autrey, T. In Situ Solid State B-11 MAS-NMR Studies of the Thermal Decomposition of Ammonia Borane: Mechanistic Studies of the Hydrogen Release Pathways from a Solid State Hydrogen Storage Material Phys. Chem. Chem. Phys. 2007, 9, 1831-1836
    • (2007) Phys. Chem. Chem. Phys. , vol.9 , pp. 1831-1836
    • Stowe, A.C.1    Shaw, W.J.2    Linehan, J.C.3    Schmid, B.4    Autrey, T.5
  • 13
    • 84871956140 scopus 로고    scopus 로고
    • Mechanistic Studies of Ammonia Borane Dehydrogenation
    • Al-Kukhun, A.; Hwang, H. T.; Varma, A. Mechanistic Studies of Ammonia Borane Dehydrogenation Int. J. Hydrogen Energy 2013, 38, 169-179
    • (2013) Int. J. Hydrogen Energy , vol.38 , pp. 169-179
    • Al-Kukhun, A.1    Hwang, H.T.2    Varma, A.3
  • 16
    • 84859254550 scopus 로고    scopus 로고
    • Solid-State NMR Study of Li-Assisted Dehydrogenation of Ammonia Borane
    • Kobayashi, T.; Hlova, I. Z.; Singh, N. K.; Pecharsky, V. K.; Pruski, M. Solid-State NMR Study of Li-Assisted Dehydrogenation of Ammonia Borane Inorg. Chem. 2012, 51, 4108-4115
    • (2012) Inorg. Chem. , vol.51 , pp. 4108-4115
    • Kobayashi, T.1    Hlova, I.Z.2    Singh, N.K.3    Pecharsky, V.K.4    Pruski, M.5
  • 18
    • 80455158005 scopus 로고    scopus 로고
    • Probing Quadrupolar Nuclei by Solid-State NMR Spectroscopy: Recent Advances
    • Fernandez, C.; Pruski, M.; Chan, J. C. C. Probing Quadrupolar Nuclei by Solid-State NMR Spectroscopy: Recent Advances Top. Curr. Chem. 2012, 306, 119-188
    • (2012) Top. Curr. Chem. , vol.306 , pp. 119-188
    • Fernandez, C.1    Pruski, M.2    Chan, J.C.C.3
  • 19
    • 0002616982 scopus 로고
    • Sensitivity Enhanced Detection of Weak Nuclei Using Heteronuclear Multiple Quantum Coherence
    • Muller, L. Sensitivity Enhanced Detection of Weak Nuclei Using Heteronuclear Multiple Quantum Coherence J. Am. Chem. Soc. 1979, 101, 4481-4484
    • (1979) J. Am. Chem. Soc. , vol.101 , pp. 4481-4484
    • Muller, L.1
  • 20
    • 0000195671 scopus 로고
    • Natural Abundance N-15 NMR by Enhanced Heteronuclear Spectroscopy
    • Bodenhausen, G.; Ruben, D. J. Natural Abundance N-15 NMR by Enhanced Heteronuclear Spectroscopy Chem. Phys. Lett. 1980, 69, 185-189
    • (1980) Chem. Phys. Lett. , vol.69 , pp. 185-189
    • Bodenhausen, G.1    Ruben, D.J.2
  • 21
    • 0033629934 scopus 로고    scopus 로고
    • Sensitivity Enhancement in Solid State N-15 NMR by Indirect Detection with High-Speed Magic Angle Spinning
    • Ishii, Y.; Tycko, R. Sensitivity Enhancement in Solid State N-15 NMR by Indirect Detection with High-Speed Magic Angle Spinning J. Magn. Reson. 2000, 142, 199-204
    • (2000) J. Magn. Reson. , vol.142 , pp. 199-204
    • Ishii, Y.1    Tycko, R.2
  • 22
    • 84894026592 scopus 로고    scopus 로고
    • Indirectly Detected Heteronuclear Correlation Solid-State NMR Spectroscopy of Naturally Abundant N-15 Nuclei
    • Althaus, S. M.; Mao, K.; Stringer, J. A.; Kobayashi, T.; Pruski, M. Indirectly Detected Heteronuclear Correlation Solid-State NMR Spectroscopy of Naturally Abundant N-15 Nuclei Solid State Nucl. Magn. Reson. 2014, 57-58, 17-21
    • (2014) Solid State Nucl. Magn. Reson. , vol.5758 , pp. 17-21
    • Althaus, S.M.1    Mao, K.2    Stringer, J.A.3    Kobayashi, T.4    Pruski, M.5
  • 24
    • 84883090158 scopus 로고    scopus 로고
    • Dynamic Nuclear Polarization
    • In; Grant, D. M. Harris, R. K. John Wiley: Chichester, U.K.
    • Wind, R. A. Dynamic Nuclear Polarization. In Encyclopedia of NMR; Grant, D. M.; Harris, R. K., Eds.; John Wiley: Chichester, U.K., 1996; pp 1798-1807.
    • (1996) Encyclopedia of NMR , pp. 1798-1807
    • Wind, R.A.1
  • 25
    • 36149016620 scopus 로고
    • Polarization of Nuclei in Metals
    • Overhauser, A. W. Polarization of Nuclei in Metals Phys. Rev. 1953, 92, 411-415
    • (1953) Phys. Rev. , vol.92 , pp. 411-415
    • Overhauser, A.W.1
  • 26
    • 36149002108 scopus 로고
    • Polarization of Nuclear Spins in Metals
    • Carver, T. R.; Slichter, C. P. Polarization of Nuclear Spins in Metals Phys. Rev. 1953, 92, 212-213
    • (1953) Phys. Rev. , vol.92 , pp. 212-213
    • Carver, T.R.1    Slichter, C.P.2
  • 31
  • 32
    • 33748353607 scopus 로고    scopus 로고
    • Totapol: A Biradical Polarizing Agent for Dynamic Nuclear Polarization Experiments in Aqueous Media
    • Song, C.; Hu, K.-N.; Joo, C.-G.; Swager, T. M.; Griffin, R. G. Totapol: A Biradical Polarizing Agent for Dynamic Nuclear Polarization Experiments in Aqueous Media J. Am. Chem. Soc. 2006, 128, 11385-11390
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 11385-11390
    • Song, C.1    Hu, K.-N.2    Joo, C.-G.3    Swager, T.M.4    Griffin, R.G.5
  • 34
    • 84885087694 scopus 로고    scopus 로고
    • Highly Efficient, Water-Soluble Polarizing Agents for Dynamic Nuclear Polarization at High Frequency
    • Sauvee, C.; Rosay, M.; Casano, G.; Aussenac, F.; Weber, R. T.; Ouari, O.; Tordo, P. Highly Efficient, Water-Soluble Polarizing Agents for Dynamic Nuclear Polarization at High Frequency Angew. Chem., Int. Ed. 2013, 52, 10858-10861
    • (2013) Angew. Chem., Int. Ed. , vol.52 , pp. 10858-10861
    • Sauvee, C.1    Rosay, M.2    Casano, G.3    Aussenac, F.4    Weber, R.T.5    Ouari, O.6    Tordo, P.7
  • 38
    • 0001421829 scopus 로고
    • Isotropic Spectra of Half-Integer Quadrupolar Spins from Bidimensional Magic-Angle-Spinning NMR
    • Frydman, L.; Harwood, J. S. Isotropic Spectra of Half-Integer Quadrupolar Spins from Bidimensional Magic-Angle-Spinning NMR J. Am. Chem. Soc. 1995, 117, 5367-5368
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367-5368
    • Frydman, L.1    Harwood, J.S.2
  • 41
    • 0034500179 scopus 로고    scopus 로고
    • Application of Seven Borane Complexes in Paper Conservation
    • Bicchieri, M.; Sementilli, F. M.; Sodo, A. Application of Seven Borane Complexes in Paper Conservation Restaurator 2000, 21, 213-228
    • (2000) Restaurator , vol.21 , pp. 213-228
    • Bicchieri, M.1    Sementilli, F.M.2    Sodo, A.3
  • 45
    • 0033693127 scopus 로고    scopus 로고
    • Efficient Synthesis and NMR Data of N- or B-Substituted Borazines
    • Framery, E.; Vaultier, M. Efficient Synthesis and NMR Data of N- or B-Substituted Borazines Heteroat. Chem. 2000, 11, 218-225
    • (2000) Heteroat. Chem. , vol.11 , pp. 218-225
    • Framery, E.1    Vaultier, M.2
  • 46
    • 0036742074 scopus 로고    scopus 로고
    • High Resolution Solid State NMR Investigation of Various Boron Nitride Preceramic Polymers
    • Gervais, C.; Babonneau, F. High Resolution Solid State NMR Investigation of Various Boron Nitride Preceramic Polymers J. Organomet. Chem. 2002, 657, 75-82
    • (2002) J. Organomet. Chem. , vol.657 , pp. 75-82
    • Gervais, C.1    Babonneau, F.2
  • 47
    • 33747799315 scopus 로고    scopus 로고
    • Dynamic Nuclear Polarization of Amyloidogenic Peptide Nanocrystals: Gnnqqny, a Core Segment of the Yeast Prion Protein Sup35p
    • van der Wel, P. C. A.; Hu, K.-N.; Lewandowski, J.; Griffin, R. G. Dynamic Nuclear Polarization of Amyloidogenic Peptide Nanocrystals: Gnnqqny, a Core Segment of the Yeast Prion Protein Sup35p J. Am. Chem. Soc. 2006, 128, 10840-10846
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 10840-10846
    • Van Der Wel, P.C.A.1    Hu, K.-N.2    Lewandowski, J.3    Griffin, R.G.4
  • 48
    • 0027110802 scopus 로고
    • Mechanism of DNP-Enhanced Polarization Transfer across the Interface of Polycarbonate Polystyrene Heterogeneous Blends
    • Afeworki, M.; Schaefer, J. Mechanism of DNP-Enhanced Polarization Transfer across the Interface of Polycarbonate Polystyrene Heterogeneous Blends Macromolecules 1992, 25, 4092-4096
    • (1992) Macromolecules , vol.25 , pp. 4092-4096
    • Afeworki, M.1    Schaefer, J.2
  • 53
    • 33745398042 scopus 로고    scopus 로고
    • Amineborane-Based Chemical Hydrogen Storage: Enhanced Ammonia Borane Dehydrogenation in Ionic Liquids
    • Bluhm, M. E.; Bradley, M. G.; Butterick, R.; Kusari, U.; Sneddon, L. G. Amineborane-Based Chemical Hydrogen Storage: Enhanced Ammonia Borane Dehydrogenation in Ionic Liquids J. Am. Chem. Soc. 2006, 128, 7748-7749
    • (2006) J. Am. Chem. Soc. , vol.128 , pp. 7748-7749
    • Bluhm, M.E.1    Bradley, M.G.2    Butterick, R.3    Kusari, U.4    Sneddon, L.G.5
  • 54
    • 0001757277 scopus 로고    scopus 로고
    • Ab Initio Prediction of N-15-NMR Chemical Shift in Alpha-Boron Nitride Based on an Analysis of Connectivities
    • Gastreich, M.; Marian, C. M. Ab Initio Prediction of N-15-NMR Chemical Shift in Alpha-Boron Nitride Based on an Analysis of Connectivities J. Comput. Chem. 1998, 19, 716-725
    • (1998) J. Comput. Chem. , vol.19 , pp. 716-725
    • Gastreich, M.1    Marian, C.M.2
  • 55
    • 84879861358 scopus 로고    scopus 로고
    • Regeneration of Ammonia Borane from Spent Fuel Materials
    • Summerscales, O. T.; Gordon, J. C. Regeneration of Ammonia Borane from Spent Fuel Materials Dalton Trans. 2013, 42, 10075-10084
    • (2013) Dalton Trans. , vol.42 , pp. 10075-10084
    • Summerscales, O.T.1    Gordon, J.C.2
  • 57
    • 33947458677 scopus 로고
    • The Dehydrocyclization Reaction
    • Hansch, C. The Dehydrocyclization Reaction Chem. Rev. 1953, 53, 353-396
    • (1953) Chem. Rev. , vol.53 , pp. 353-396
    • Hansch, C.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.