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Volumn 142, Issue 1, 2000, Pages 199-204

Sensitivity Enhancement in Solid State 15 N NMR by Indirect Detection with High-Speed Magic Angle Spinning

Author keywords

Indirect detection; Magic angle spinning; Nitrogen 15 NMR; Peptides; Solid state NMR

Indexed keywords

NITROGEN; PEPTIDE;

EID: 0033629934     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1999.1976     Document Type: Editorial
Times cited : (231)

References (41)
  • 1
    • 0000880175 scopus 로고
    • Nuclear magnetic resonance in the cesium halides
    • N. Bloembergen and P. P. Sorokin, Nuclear magnetic resonance in the cesium halides, Phys. Rev. 110, 865-875 (1958).
    • (1958) Phys. Rev. , vol.110 , pp. 865-875
    • Bloembergen, N.1    Sorokin, P.P.2
  • 2
    • 36149026370 scopus 로고
    • Nuclear double resonance in the rotating frame
    • S. R. Hartmann and E. L. Hahn, Nuclear double resonance in the rotating frame, Phys. Rev. 128, 2042-2053 (1962).
    • (1962) Phys. Rev. , vol.128 , pp. 2042-2053
    • Hartmann, S.R.1    Hahn, E.L.2
  • 3
    • 0009650639 scopus 로고
    • Spin temperature in nuclear double resonance
    • F. M. Lurie and C. P. Slichter, Spin temperature in nuclear double resonance, Phys. Rev. A 133, 1108-1122 (1964).
    • (1964) Phys. Rev. A , vol.133 , pp. 1108-1122
    • Lurie, F.M.1    Slichter, C.P.2
  • 4
    • 0000195290 scopus 로고
    • Improved resolution of small resonance shifts of dilute nuclear spin systems in solids by pulsed double resonance
    • P. Mansfield and P. K. Grannell, Improved resolution of small resonance shifts of dilute nuclear spin systems in solids by pulsed double resonance, J. Phys. C 4, L197-L200 (1971).
    • (1971) J. Phys. C , vol.4
    • Mansfield, P.1    Grannell, P.K.2
  • 5
    • 36849106840 scopus 로고
    • Proton-enhanced NMR of dilute spins in solids
    • A. Pines, M. G. Gibby, and J. S. Waugh, Proton-enhanced NMR of dilute spins in solids, J. Chem. Phys. 59, 569-590 (1973).
    • (1973) J. Chem. Phys. , vol.59 , pp. 569-590
    • Pines, A.1    Gibby, M.G.2    Waugh, J.S.3
  • 6
    • 0000624060 scopus 로고
    • Pure nuclear electric quadrupole resonance in impure copper
    • A. G. Redfield, Pure nuclear electric quadrupole resonance in impure copper, Phys. Rev. 130, 589-595 (1963).
    • (1963) Phys. Rev. , vol.130 , pp. 589-595
    • Redfield, A.G.1
  • 7
    • 0001469535 scopus 로고
    • Sensitive detection of nuclear quadrupole interactions in solids
    • R. E. Slusher and E. L. Hahn, Sensitive detection of nuclear quadrupole interactions in solids, Phys. Rev. 166, 332-347 (1968).
    • (1968) Phys. Rev. , vol.166 , pp. 332-347
    • Slusher, R.E.1    Hahn, E.L.2
  • 8
    • 49449126641 scopus 로고
    • Cross-correlation of spin-decoupled NMR spectra by heteronuclear two-dimensional spectroscopy
    • A. A. Maudsley, L. Müller, and R. R. Ernst, Cross-correlation of spin-decoupled NMR spectra by heteronuclear two-dimensional spectroscopy, J. Magn. Reson. 28, 463-469 (1977).
    • (1977) J. Magn. Reson. , vol.28 , pp. 463-469
    • Maudsley, A.A.1    Müller, L.2    Ernst, R.R.3
  • 9
    • 0002616982 scopus 로고
    • Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence
    • L. Müller, Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence, J. Am. Chem. Soc. 101, 4481-4484 (1979).
    • (1979) J. Am. Chem. Soc. , vol.101 , pp. 4481-4484
    • Müller, L.1
  • 10
    • 33644757144 scopus 로고
    • Correlation of proton and nitrogen-15 chemical shifts by multiple quantum NMR
    • A. Bax, R. H. Griffey, and B. L. Hawkins, Correlation of proton and nitrogen-15 chemical shifts by multiple quantum NMR, J. Magn. Reson. 55, 301-315 (1983).
    • (1983) J. Magn. Reson. , vol.55 , pp. 301-315
    • Bax, A.1    Griffey, R.H.2    Hawkins, B.L.3
  • 11
    • 0000195671 scopus 로고
    • Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy
    • G. Bodenhausen and D. J. Ruben, Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy, Chem. Phys. Lett. 69, 185-189 (1980).
    • (1980) Chem. Phys. Lett. , vol.69 , pp. 185-189
    • Bodenhausen, G.1    Ruben, D.J.2
  • 12
    • 0001173504 scopus 로고
    • Stimulated echo NMR spectra and their use for heteronuclear two-dimensional shift correlation
    • A. G. Redfield, Stimulated echo NMR spectra and their use for heteronuclear two-dimensional shift correlation, Chem. Phys. Lett. 96, 537 (1983).
    • (1983) Chem. Phys. Lett. , vol.96 , pp. 537
    • Redfield, A.G.1
  • 16
    • 0032607798 scopus 로고    scopus 로고
    • Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning
    • C. Filip, S. Hafner, I. Schnell, D. E. Demco, and H. W. Spiess, Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning, J. Chem. Phys. 110, 423-440 (1999).
    • (1999) J. Chem. Phys. , vol.110 , pp. 423-440
    • Filip, C.1    Hafner, S.2    Schnell, I.3    Demco, D.E.4    Spiess, H.W.5
  • 17
    • 0032152041 scopus 로고    scopus 로고
    • Selective residual dipolar couplings in cross-linked elastomers by H-1 double-quantum NMR spectroscopy
    • R. Graf, D. E. Demco, S. Hafner, and H. W. Spiess, Selective residual dipolar couplings in cross-linked elastomers by H-1 double-quantum NMR spectroscopy, Solid State Nucl. Magn. Reson. 12, 139-152 (1998).
    • (1998) Solid State Nucl. Magn. Reson. , vol.12 , pp. 139-152
    • Graf, R.1    Demco, D.E.2    Hafner, S.3    Spiess, H.W.4
  • 19
    • 0031081882 scopus 로고    scopus 로고
    • Multiple-pulse assisted line-narrowing by fast magic-angle spinning
    • S. Hafner and H. W. Spiess, Multiple-pulse assisted line-narrowing by fast magic-angle spinning, Solid State Nucl. Magn. Reson. 8, 17-24 (1997).
    • (1997) Solid State Nucl. Magn. Reson. , vol.8 , pp. 17-24
    • Hafner, S.1    Spiess, H.W.2
  • 20
    • 33646745803 scopus 로고    scopus 로고
    • Multiple-pulse line narrowing under fast magic-angle spinning
    • S. Hafner and H. W. Spiess, Multiple-pulse line narrowing under fast magic-angle spinning, J. Magn. Reson. Ser. A 121, 160-166 (1996).
    • (1996) J. Magn. Reson. Ser. A , vol.121 , pp. 160-166
    • Hafner, S.1    Spiess, H.W.2
  • 21
    • 0001037883 scopus 로고    scopus 로고
    • High magnetic field for enhanced proton resolution in high-speed CP/ MAS heteronuclear H-1-C-13 dipolar-correlation spectroscopy
    • B. J. vanRossum, G. J. Boender, and H. J. M. deGroot, High magnetic field for enhanced proton resolution in high-speed CP/ MAS heteronuclear H-1-C-13 dipolar-correlation spectroscopy, J. Magn. Reson. Ser. A 120, 274-277 (1996).
    • (1996) J. Magn. Reson. Ser. A , vol.120 , pp. 274-277
    • VanRossum, B.J.1    Boender, G.J.2    DeGroot, H.J.M.3
  • 22
    • 0032246292 scopus 로고    scopus 로고
    • Proton MAS NMR spectra at high magnetic fields and high spinning frequencies: Spectral simulations using Roquet theory
    • S. Ray, E. Vinogradov, G. J. Boender, and S. Vega, Proton MAS NMR spectra at high magnetic fields and high spinning frequencies: Spectral simulations using Roquet theory, J. Magn. Reson. 135, 418-426 (1998).
    • (1998) J. Magn. Reson. , vol.135 , pp. 418-426
    • Ray, S.1    Vinogradov, E.2    Boender, G.J.3    Vega, S.4
  • 23
    • 0000014095 scopus 로고
    • Adiabatic passage Hartmann-Hahn cross polarization in NMR under magic angle sample spinning
    • S. Hediger, B. H. Meier, and R. R. Ernst, Adiabatic passage Hartmann-Hahn cross polarization in NMR under magic angle sample spinning, Chem. Phys. Lett. 240, 449-456 (1995).
    • (1995) Chem. Phys. Lett. , vol.240 , pp. 449-456
    • Hediger, S.1    Meier, B.H.2    Ernst, R.R.3
  • 24
    • 0032558088 scopus 로고    scopus 로고
    • Biopolymer conformational distributions from solid-state NMR: Alpha-helix and 3(10)-helix contents of a helical peptide
    • H. W. Long and R. Tycko, Biopolymer conformational distributions from solid-state NMR: alpha-helix and 3(10)-helix contents of a helical peptide, J. Am. Chem. Soc. 120, 7039-7048 (1998).
    • (1998) J. Am. Chem. Soc. , vol.120 , pp. 7039-7048
    • Long, H.W.1    Tycko, R.2
  • 25
    • 0024707204 scopus 로고
    • Unusually Stable Helix Formation in Short Alanine-Based Peptides
    • S. Marqusee, V. H. Robbins, and R. L. Baldwin, Unusually Stable Helix Formation in Short Alanine-Based Peptides, Proc. Natl. Acad. Sci. U.S.A. 86, 5286-5290 (1989).
    • (1989) Proc. Natl. Acad. Sci. U.S.A. , vol.86 , pp. 5286-5290
    • Marqusee, S.1    Robbins, V.H.2    Baldwin, R.L.3
  • 26
    • 0023461350 scopus 로고
    • Helix Stabilization by Glu- . . . Lys+ Salt Bridges in Short Peptides of Denovo Design
    • S. Marqusee and R. L. Baldwin, Helix Stabilization By Glu- . . . Lys+ Salt Bridges in Short Peptides of Denovo Design, Proc. Natl. Acad. Sci. U.S.A. 84, 8898-8902 (1987).
    • (1987) Proc. Natl. Acad. Sci. U.S.A. , vol.84 , pp. 8898-8902
    • Marqusee, S.1    Baldwin, R.L.2
  • 27
    • 4244132605 scopus 로고
    • Measurement of nuclear magnetic dipole-dipole couplings in magic angle spinning NMR
    • R. Tycko and G. Dabbagh, Measurement of nuclear magnetic dipole-dipole couplings in magic angle spinning NMR, Chem. Phys. Lett. 173, 461-465 (1990).
    • (1990) Chem. Phys. Lett. , vol.173 , pp. 461-465
    • Tycko, R.1    Dabbagh, G.2
  • 28
    • 0027205775 scopus 로고
    • Symmetry Principles in the Design of Pulse Sequences for Structural Measurements in Magic Angle Spinning Nuclear-Magnetic-Resonance
    • R. Tycko and S. O. Smith, Symmetry Principles in the Design of Pulse Sequences For Structural Measurements in Magic Angle Spinning Nuclear-Magnetic-Resonance, J. Chem. Phys. 98, 932-943 (1993).
    • (1993) J. Chem. Phys. , vol.98 , pp. 932-943
    • Tycko, R.1    Smith, S.O.2
  • 29
    • 0001614068 scopus 로고    scopus 로고
    • Quantitative conformational measurements in solid state NMR by constant-time homonuclear dipolar recoupling
    • A. E. Bennett, D. P. Weliky, and R. Tycko, Quantitative conformational measurements in solid state NMR by constant-time homonuclear dipolar recoupling, J. Am. Chem. Soc. 120, 4897-4898 (1998).
    • (1998) J. Am. Chem. Soc. , vol.120 , pp. 4897-4898
    • Bennett, A.E.1    Weliky, D.P.2    Tycko, R.3
  • 30
    • 0000137948 scopus 로고
    • Windowless dipolar recoupling - The detection of weak dipolar couplings between spin1/2 nuclei with large chemical-shift anisotropies
    • D. M. Gregory, D. J. Mitchell, J. A. Stringer, S. Kiihne, J. C. Shiels, J. Callahan, M. A. Mehta, and G. P. Drobny, Windowless dipolar recoupling - the detection of weak dipolar couplings between spin1/2 nuclei with large chemical-shift anisotropies, Chem. Phys. Lett. 246, 654-663 (1995).
    • (1995) Chem. Phys. Lett. , vol.246 , pp. 654-663
    • Gregory, D.M.1    Mitchell, D.J.2    Stringer, J.A.3    Kiihne, S.4    Shiels, J.C.5    Callahan, J.6    Mehta, M.A.7    Drobny, G.P.8
  • 32
    • 0000321871 scopus 로고
    • Chemical shift correlation spectroscopy in rotating solids: Radio frequency-driven dipolar recoupling and longitudinal exchange
    • A. E. Bennett, J. H. Ok, R. G. Griffin, and S. Vega, Chemical shift correlation spectroscopy in rotating solids: radio frequency-driven dipolar recoupling and longitudinal exchange, J. Chem. Phys. 96, 8624-8627 (1992).
    • (1992) J. Chem. Phys. , vol.96 , pp. 8624-8627
    • Bennett, A.E.1    Ok, J.H.2    Griffin, R.G.3    Vega, S.4
  • 33
    • 0000432697 scopus 로고    scopus 로고
    • Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy
    • M. Hohwy, C. M. Rienstra, C. P. Jaroniec, and R. G. Griffin, Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy, J. Chem. Phys. 110, 7983-7992 (1999).
    • (1999) J. Chem. Phys. , vol.110 , pp. 7983-7992
    • Hohwy, M.1    Rienstra, C.M.2    Jaroniec, C.P.3    Griffin, R.G.4
  • 34
    • 36449004247 scopus 로고
    • Internuclear distance measurements in solid-state nuclear-magnetic-resonance-dipolar recoupling via rotor Synchronized spin locking
    • B. Q. Sun, P. R. Costa, D. Kocisko, P. T. Lansbury, and R. G. Griffin, Internuclear distance measurements in solid-state nuclear-magnetic-resonance-dipolar recoupling via rotor Synchronized spin locking, J. Chem. Phys. 102, 702-707 (1995).
    • (1995) J. Chem. Phys. , vol.102 , pp. 702-707
    • Sun, B.Q.1    Costa, P.R.2    Kocisko, D.3    Lansbury, P.T.4    Griffin, R.G.5
  • 36
    • 0003193780 scopus 로고
    • Efficient Dipolar Recoupling in the Nmr of Rotating Solids - A Sevenfold Symmetrical Radiofrequency Pulse Sequence
    • Y. K. Lee, N. D. Kurur, M. Helmle, O. G. Johannessen, N. C. Nielsen, and M. H. Levitt, Efficient Dipolar Recoupling in the Nmr of Rotating Solids - a Sevenfold Symmetrical Radiofrequency Pulse Sequence, Chem. Phys. Lett. 242, 304-309 (1995).
    • (1995) Chem. Phys. Lett. , vol.242 , pp. 304-309
    • Lee, Y.K.1    Kurur, N.D.2    Helmle, M.3    Johannessen, O.G.4    Nielsen, N.C.5    Levitt, M.H.6
  • 37
    • 0002215317 scopus 로고    scopus 로고
    • Manipulation of nuclear spin Hamiltonians by rf-field modulations and its applications to observation of powder patterns under magic-angle spinning
    • Y. Ishii and T. Terao, Manipulation of nuclear spin Hamiltonians by rf-field modulations and its applications to observation of powder patterns under magic-angle spinning, J. Chem. Phys. 109, 1366-1374 (1998).
    • (1998) J. Chem. Phys. , vol.109 , pp. 1366-1374
    • Ishii, Y.1    Terao, T.2
  • 38
    • 0000245811 scopus 로고
    • Broad-band polarization-transfer experiments for rotating solids
    • M. Baldus, M. Tomaselli, B. H. Meier, and R. R. Ernst, Broad-band polarization-transfer experiments for rotating solids, Chem. Phys. Lett. 230, 329-336 (1994).
    • (1994) Chem. Phys. Lett. , vol.230 , pp. 329-336
    • Baldus, M.1    Tomaselli, M.2    Meier, B.H.3    Ernst, R.R.4
  • 39
    • 0031345626 scopus 로고    scopus 로고
    • Measurement of Heteronuclear Dipolar Interactions by Rotational-Echo, Double-Resonance Nuclear Magnetic Resonance
    • T. Gullion, Measurement of Heteronuclear Dipolar Interactions by Rotational-Echo, Double-Resonance Nuclear Magnetic Resonance, Magn. Reson. Rev. 17, 83-131 (1997).
    • (1997) Magn. Reson. Rev. , vol.17 , pp. 83-131
    • Gullion, T.1
  • 40
    • 0346938543 scopus 로고    scopus 로고
    • High-field and high-speed CP-MAS C-13 NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling
    • B. J. vanRossum, H. Forster, and H. J. M. deGroot, High-field and high-speed CP-MAS C-13 NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling, J. Magn. Reson. 124, 516-519 (1997).
    • (1997) J. Magn. Reson. , vol.124 , pp. 516-519
    • VanRossum, B.J.1    Forster, H.2    DeGroot, H.J.M.3
  • 41
    • 0032561821 scopus 로고    scopus 로고
    • Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy
    • A. Lesage, D. Sakellariou, S. Steuernagel, and L. Emsley, Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy, J. Am. Chem. Soc. 120, 13194-13201 (1998).
    • (1998) J. Am. Chem. Soc. , vol.120 , pp. 13194-13201
    • Lesage, A.1    Sakellariou, D.2    Steuernagel, S.3    Emsley, L.4


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