Capillary electrophoresis-mass spectrometry as a new approach to analyze neonicotinoid insecticides

Journal of Chromatography A

Volumn 1359, Issue , 2014, Pages 317-324

  Sánchez Hernández, Laura ^a,b   Hernández Domínguez, Deamelys ^a   Bernal, José ^a   Neusüß, Christian ^b   Martín, María T ^a   Bernal, José L ^a  

^a UNIVERSITY OF VALLADOLID   (Spain)

^b AALEN UNIVERSITY   (Germany)

Author keywords

Beeswax; Capillary electrophoresis; Insecticides; Mass spectrometry; Neonicotinoids

Indexed keywords

CAPILLARY ELECTROPHORESIS; DRUG PRODUCTS; FOOD PRODUCTS; INSECTICIDES; OXALIC ACID;

BEESWAX; CAPILLARY ELECTROPHORESIS SEPARATION; CAPILLARY ELECTROPHORESIS-MASS SPECTROMETRIES; DINOTEFURAN; IMIDACLOPRIDS; NEONICOTINOID INSECTICIDES; NEONICOTINOIDS; NEW APPROACHES; THIACLOPRID; THIAMETHOXAM;

MASS SPECTROMETRY;

ACETAMIPRID; CLOTHIANIDIN; DINOTEFURAN; IMIDACLOPRID; INSECTICIDE; NEONICOTINOID INSECTICIDE; NITENPYRAM; OXALIC ACID; PROPOLIS; THIACLOPRID; THIAMETHOXAM; UNCLASSIFIED DRUG;

ARTICLE; CAPILLARY ELECTROPHORESIS; CONTROLLED STUDY; ELECTRIC POTENTIAL; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS SPECTROMETRY; MEASUREMENT ACCURACY; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION;

BEESWAX; CAPILLARY ELECTROPHORESIS; INSECTICIDES; MASS SPECTROMETRY; NEONICOTINOIDS;

ELECTROPHORESIS, CAPILLARY; GUANIDINES; IMIDAZOLES; INSECTICIDES; LIMIT OF DETECTION; MASS SPECTROMETRY; NITRO COMPOUNDS; OXAZINES; PYRIDINES; TANDEM MASS SPECTROMETRY; THIAZINES; THIAZOLES; WAXES;

EID: 84906046384     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2014.07.028     Document Type: Article

References (29)

1. Yáñez K.P., Bernal J.L., Nozal M.J., Martín M.T., Bernal J. Determination of seven neonicotinoid insecticides in beeswax by liquid chromatography coupled to electrospray-mass spectrometry using a fused-core column. J. Chromatogr. A 2013, 1285:110-117.
2. Mullin C.A., Frazier M., Frazier J.L., Ashcraft S., Simonds R., vanEngelsdorp D., Pettis J.S. High levels of miticides and agrochemicals in North American apiaries: implications for honey bee health. PLOS ONE 2010, 5:e9754. 1-19.
3. Nguyen B.K., Saegerman C., Pirard C., Mignon J., Widart J., Thirionet B., Verheggen F.J., Berkvens D., De Pauw E., Haubruge E. Does imidacloprid seed-treated maize have an impact on honey bee mortality?. J. Econ. Entomol. 2009, 102:616-623.
4. Ko A.-Y., Rahman Md.M., El-Aty A.M.A., Jang J., Park J.-H., Cho S.-K., Shim J.-H. Development of a simple extraction and oxidation procedure for the residue analysis of imidacloprid and its metabolites in lettuce using gas chromatography. Food Chem. 2014, 148:402-409.
5. Tapparo A., Giorio C., Soldà L., Bogialli S., Marton D., Marzaro M., Girolami V. UHPLC-DAD method for the determination of neonicotinoid insecticides in single bees and its relevance in honeybee colony loss investigations. Anal. Bioanal. Chem. 2013, 405:1007-1014.
6. Vichapong J., Burakham R., Srijaranai S. Vortex-assisted surfactant-enhanced-emulsification liquid-liquid microextraction with solidification of floating organic droplet combined with HPLC for the determination of neonicotinoid pesticides. Talanta 2013, 117:221-228.
7. Hou R.-Y., Jiao W.-T., Qian X.-S., Wang X.-H., Xiao Y., Wan X.-C. Effective extraction method for determination of neonicotinoid residues in tea. J. Agric. Food Chem. 2013, 61:12565-12571.
8. Paramasivam M., Chandrasekaran S., Harischandra Naik R., Karthik P., Thangachamy P., Mahalingam C.A. Determination of imidacloprid residues in mulberry leaves by QuEChERS and liquid chromatography with diode array detection. J. Liq. Chromatogr. Relat. Technol. 2014, 37:122-129.
9. Gil M.D., Martínez M., Santiago R., Galanti A., Girotti S. Column switching liquid chromatography and post-column photochemically fluorescence detection to determine imidacloprid and 6-chloronicotinic acid in honeybees. J. Chromatogr. A 2007, 1147:17-23.
10. Rancan M., Sabatini A.G., Achilli G., Galletti G.C. Determination of imidacloprid and metabolites by liquid chromatography with an electrochemical detector and post column photochemical reactor. Anal. Chim. Acta 2006, 555:20-24.
11. Zhang F., Li Y., Yu C., Pan C. Determination of six neonicotinoid insecticides residues in spinach, cucumber, apple and pomelo by QuEChERS method and LC-MS/MS. Bull. Environ. Contam. Toxicol. 2012, 88:885-890.
12. Zhang Y., Xu J., Dong F., Liu X., Li X., Li Y., Wu X., Liang X., Zheng Y. Simultaneous determination of four neonicotinoid insecticides residues in cereals, vegetables and fruits using ultra-performance liquid chromatography/tandem mass spectrometry. Anal. Methods 2013, 5:1449-1455.
13. Xiao Z., Yang Y., Li Y., Fan X., Ding S. Determination of neonicotinoid insecticides residues in eels using subcritical water extraction and ultra-performance liquid chromatography-tandem mass spectrometry. Anal. Chim. Acta 2013, 777:32-40.
14. Campillo N., Viñas P., Férez-Melgarejo G., Hernández-Coórdoba M. Liquid chromatography with diode array detection and tandem mass spectrometry for the determination of neonicotinoid insecticides in honey samples using dispersive liquid-liquid microextraction. J. Agric. Food Chem. 2013, 61:4799-4805.
15. Jovanov P., Guzsvány V., Franko M., Lazić S., Sakač M., Šarić B., Banjac V. Multi-residue method for determination of selected neonicotinoid insecticides in honey using optimized dispersive liquid-liquid microextraction combined with liquid chromatography-tandem mass spectrometry. Talanta 2013, 111:125-133.
16. Chen M., Collins E.M., Tao L., Lu C. Simultaneous determination of residues in pollen and high-fructose corn syrup from eight neonicotinoid insecticides by liquid chromatography-tandem mass spectrometry. Anal. Bioanal. Chem. 2013, 405:9251-9264.
17. Giroud B., Vauchez A., Vulliet E., Wiest L., Buleté A. Trace level determination of pyrethroid and neonicotinoid insecticides in beebread using acetonitrile-based extraction followed by analysis with ultra-high-performance liquid chromatography-tandem mass spectrometry. J. Chromatogr. A 2013, 1316:53-61.
18. Yáñez K.P., Martín M.T., Bernal J.L., Nozal M.J., Bernal J. Trace analysis of seven neonicotinoid insecticides in bee pollen by solid-liquid extraction and liquid chromatography coupled to electrospray ionization mass spectrometry. Food Anal. Methods 2014, 7:490-499.
19. Cacho J., Fierro I., Deban L., Vega M., Pardo R. Monitoring of the photochemical degradation of metamitron and imidacloprid by micellar electrokinetic chromatography and differential pulse polarography. Pest. Sci. 1999, 55:949-954.
20. Segura Carretero A., Cruces-Blanco C., Pérez Durán S., Fernández Gutiérrez A. Determination of imidacloprid and its metabolite 6-chloronicotinic acid in greenhouse air by application of micellar electrokinetic capillary chromatography with solid-phase extraction. J. Chromatogr. A 2003, 1003:189-195.
21. Ettiene G., Bauza R., Plata M.R., Contento A.M., Ríos A. Determination of neonicotinoid insecticides in environmental samples by micellar electrokinetic chromatography using solid-phase treatments. Electrophoresis 2012, 33:2969-2977.
22. Zhang S., Yang X., Yin X., Wang C., Wang Z. Dispersive liquid-liquid microextraction combined with sweeping micellar electrokinetic chromatography for the determination of some neonicotinoid insecticides in cucumber samples. Food Chem. 2012, 133:544-550.
23. Amelin V.G., Bol'shakov D.S., Tretyakov A.V. Separation and quantification of polar pesticides in well, surface, and drinking water by capillary electrophoresis. J. Anal. Chem. 2012, 67:904-924.
24. Amelin V.G., Bol'shakov D.S., Tret'yakov A.V. Dispersive liquid-liquid microextraction and solid-phase extraction of polar pesticides from natural water and their determination by micellar electrokinetic chromatography. J. Anal. Chem. 2013, 68:386-397.
25. Bol'shakov D.S., Amelin V.G., Tret'yakov A.V. Determination of polar pesticides in soil by micellar electrokinetic chromatography using QuEChERS sample preparation. J. Anal. Chem. 2014, 69:89-97.
26. Chen G.-H., Sun J., Dai Y.-J., Dong M. Determination of nicotinyl pesticide residues in vegetables by micellar electrokinetic capillary chromatography with quantum dot indirect laser-induced fluorescence. Electrophoresis 2012, 33:2192-2196.
27. (accessed 09.07.14). http://eur-lex.europa.eu/LexUriServ/LexUriServ.do%3Furi=OJ:L:2013:139:FULL:EN:PDF.
28. (accessed 09.07.14). http://www.bee-hexagon.net/files/file/fileE/Wax/WaxBook2.pdf.
29. (accessed 09.07.14). http://www.chemaxon.com/marvin/sketch/index.jsp.