NMR spectroscopy of inorganic earth materials

Reviews in Mineralogy and Geochemistry

Volumn 78, Issue , 2014, Pages 605-653

  Stebbins, Jonathan F ^a   Xue, Xianyu ^b  

^a STANFORD UNIVERSITY   (United States)

^b OKAYAMA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84905721011     PISSN: 15296466     EISSN: None     Source Type: Book Series    
DOI: 10.2138/rmg.2014.78.15     Document Type: Article

References (314)

1. Abragam A (1961) Principles of Nuclear Magnetism. Clarendon Press, Oxford
2. 29Si nuclear magnetic resonance study of opal and other hydrous silicas. Am Mineral 76:1863-1871
3. Alba MD, Castro MA, Chain P, Naranjo M., Perdigon A.C. (2005) Structural studies of synthetic mica-montmorillonite by means of 2D MAS NMR experiments. Phys Chem Miner 32:248-254
4. Alba MA, Castro MA, Chain P, Orta M.M., Pazos MC, Pavón E (2010) Hydrothermal stability of layered silicates in neutral and acidic media: effect on engineered-barrier safety. Clays Clay Miner 58:501-514
5. 23Na MAS NMR spectroscopy. Am Mineral 97:883-889
6. Allwardt JR, Stebbins J.F. (2004) Ca-Mg and K-Mg mixing around non-bridging oxygens in silicate glasses: An investigation using oxygen-17 MAS and 3QMAS NMR. Am Mineral 89:777-784
7. 170 MAS and 3QMAS NMR on calcium aluminate and low-silica Ca-aluminosilicate glasses. Am Mineral 88:949-954
8. 9 glasses: An investigation utilizing Raman and NMR spectroscopy of high-pressure glasses and crystals. Chem Geol 213:137-151
9. Allwardt JR, Stebbins JF, Schmidt B.C., Frost DJ, Withers AC, Hirschmann M.M. (2005) Aluminum coordination and the densification of high-pressure aluminosilicate glasses. Am Mineral 90:1218-1222
10. 29Si NMR for the structure of mixed-layer illite/smectite clay minerals. Nature 331:699-702
11. 1 MAS NMR studies of zeolite ZSM-5. Chem Phys Lett 285:10-14
12. Andrew ER, Bradbury A, Eades R.G. (1959) Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation. Nature 183:1802-1803
13. Angeli F, Villain O, Schuller S., Ispas S, Charpentier T. (2011) Insight into sodium silicate glass structural organization by multinuclear NMR combined with first-principles calculations. Geochim Cosmochim Acta 75:2453-2469
14. Apperley DC, Harris RK, Hodgkinson P. (2012) Solid-State NMR: Basic Principles & Practice. Momentum Press, LLC, New York
15. Ashbrook SE, Wimperis S. (2004) High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment. Prog Nucl Magn Reson Spectrosc 45:53-108
16. 4). Am Mineral 90:1861-1870
17. 27Al NMR. J Am Ceram Soc 88:1575-1583
18. 4 polymorphs. Phys Chem Chem Phys 9:1587-1598
19. 3 phases from high-resolution solid-state NMR spectroscopy and first-principles calculations. J Am Chem Soc 129:13213-13224
20. 27Al magic-angle spinning nuclear magnetic resonance spectroscopic study of aluminosilicate and aluminate crystals and glasses. J Am Chem Soc 118:7209-7214
21. Barron PF, Slade P, Frost R.L. (1985) Ordering of aluminum in tetrahedral sites in mixed-layer 2:1 phyllosilicates by solid-state high-resolution NMR. J Phys Chem 89:3880-3885
22. 3N. Phys Rev Lett 54:1192-1195
23. Borsa F, Rigmonti A. (1990) Comparison of NMR and NQR studies of phase transitions in disordered and ordered crystals. In: Structural Phase Transitions-II. Muller KA, Thomas H (eds) Springer-Verlag, New York, p 83-175
24. 29Si MAS NMR spectroscopy. Am Mineral 84:1422-1432
25. Bowers GM, Ravella R, Komarneni S., Mueller K.T. (2006) NMR study of strontium binding by a micaceous mineral. J Phys Chem B 110:7159-7164
26. 39K NMR investigations of hectorite. J Phys Chem C 112:6430-6438
27. 2O dynamics at the smectite/water interface. J Phys Chem C 115:23395-23407
28. 29Si NMR results. Geochim Cosmochim Acta 52:2659-2670
29. 29Si chemical shift tensors. J Magn Reson 194:136-146
30. Brouwer DH, Darton RJ, Morris R.E., Levitt M.H. (2005) A solid-state NMR method for solution of zeolite crystal structures. J Am Chem Soc 127:10365-10370
31. 27A1 NMR study of amorphous and paracrystalline opals from Australia. J Non-Cryst Solids 332:242-248
32. 3. ZKristallogr 117:37-62
33. Carroll SA, Maxwell RS, Bourcier W, Martin S., Hulzey S. (2002) Evaluation of silica-water surface chemistry using NMR spectroscopy. Geochim Cosmochim Acta 66:913-926
34. Casey WH, Rustad J.R. (2007) Reaction dynamics, molecular clusters, and aqueous geochemistry. Annu Rev Earth Planet Sci 35:21-46
35. Charpentier T (2011) The PAW/GIPAW approach for computing NMR parameters: A new dimension added to NMR study of solids. Solid State Nucl Magn Reson 40:1-20
36. 23 NMR spectra of sodium silicate crystals and glasses. J Phys Chem B 108:4147-4161
37. 29Si NMR and vibrational spectroscopy. Am Mineral 97:203-211
38. Childs CW, Hayashi S, Newman R.H. (1999) Five-coordinate aluminum in allophane. Clays Clay Miner 47:64-69
39. Cho H, Rossman G.R. (1993) Single-crystal NMR studies of low-concentration hydrous species in minerals-grossular garnet. Am Mineral 78:1149-1164
40. [64]A1 in phlogopite: high-temperature solution calorimetry, heat capacities, and thermodynamic properties of the phlogopite-eastonite join. Am Mineral 77:1191-1205
41. 29Si MAS-NMR spectroscopy, and Al-Si distribution in the tetrahedral sheet. Am Mineral 76:1485-1501
42. Cismasu AC, Michel FM, Stebbins J.F., Levard CM, Brown GE Jr (2012) Properties of impurity-bearing ferrihydrite I. Effects of Al content and precipitation rate on the structure of 2-line ferrihydrite. Geochim Cosmochim Acta 92:275-291
43. 17O quadrupolar coupling parameters in alkali silicates: A combined ab initio investigation. Solid State Nucl Magn Reson 27:233-241
44. Clark TM, Grandinetti PJ, Florian P, Stebbins J.F. (2004) Correlated structural distributions in silica glass. Phys Rev B 70:064202-064201-064208
45. 27A1 d'aluminates liquides dans le domaine 1600-2100 °C. C R Acad Sci Paris II 310:1041-1045
46. 4 from multinuclear solid-state NMR. Phys Rev B 67:024201-024201-024201-024209
47. 25Mg CP QCPMG NMR. Phys Chem Chem Phys 11:7013-7021
48. 29Si 2D magic-angle flipping NMR. J Non-Cryst Solids 357:2787-2795
49. 27A1 MAS NMR investigation of laponite and synthetic saponites of variable layer charge. Clay Miner 38:63-69
50. Derome AE (1987) Modern NMR Techniques for Chemistry Research. Pergamon Press, New York
51. 2 sequestration at elevated pressure and temperature. Rev Sci Instrum 82:076107-1-3
52. 170 multiple quantum magic angle spinning NMR spectroscopy. Chem Phys Let 266:568-574
53. Dubinsky EV, Stebbins J.F. (2006) Quench rate and temperature effects on framework ordering in aluminosilicate melts. Am Mineral 91:753-761
54. Duer MJ (2002) Solid-State NMR Spectroscopy: Principles and Applications. Blackwell, Oxford, U.K.
55. Duer MJ (2004) Introduction to solid-state NMR spectroscopy. Blackwell, Oxford, U.K.
56. Dupree R, Holland D, McMillan P.W., Pettifer R.F. (1984) The structure of soda-silica glasses: a MAS NMR study. J Non-Cryst Solids 68:399-410
57. Dupree R, Holland D, Mortuza M.G. (1990) A MAS-NMR investigation of lithium silicate glasses and glass ceramics. J Non-Cryst Solids 116:148-160
58. 43Ca NMR. Chem Phys Let 276:399-404
59. Dupree R, Kohn SC, Mortuza M.G., Holland D. (1992) NMR studies of glass structure. In: Physics of Non-Crystalline Solids. Pye LD, La Course WC, Stevens HJ (eds) Taylor and Francis, London, p 718-723
60. Eckert H (1994) Structural studies of non-crystalline solids using solid state NMR. New experimental approaches and results. In: Solid-State NMR IV Methods and Applications of Solid-State NMR. Blümich B (ed) Springer-Verlag, Berlin, p 127-198
61. Engelhardt G, Michel D. (1987) High-Resolution Solid-State NMR of Silicates and Zeolites. Wiley, New York
62. Ernst RR, Bodenhausen G, Wokaun A. (1987) Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Oxford Science Publications, Oxford
63. Faman I (1991) NMR spectroscopy in the Earth sciences. In: Encyclopedia of Earth System Science. Nierenberg W A (ed) Academic Press, San Diego, CA, p 750
64. Farnan I, Cho H, Weber W.J., Scheele RD, Johnson NR, Kozelisky A.E. (2004) High-resolution solid-state nuclear magnetic resonance experiments on highly radioactive ceramics. Rev Sci Instrum 75:5232-5236
65. wSi nuclear magnetic resonance. J Appl Phys 89:2084-2090
66. 29Si NMR investigation of solid and molten silicates. J Am Chem Soc 112:32-39
67. 2,Si NMR. J Non-Cryst Solids 124:207-215
68. Farnan I, Stebbins J.F. (1994) The nature of the glass transition in a silica-rich oxide melt. Science 265:1206-1209
69. 207Pb NMR study of local order in lead silicate glasses. J Non-Cryst Solids 232-2:403-408
70. 23Na MAS NMR study. Solid State Nucl Magn Reson 18:70-88
71. Fechtelkord M (2004) Solid state NMR spectroscopy as supporting method in Rietveld structure refinements of rock-forming minerals: New developments and examples. In: Spectroscopic Methods in Mineralogy. Beran A, Libowitsky E (eds) Eotvos University Press, Budapest, p 421-464
72. 27A1 HETCOR and REDOR experiments. Am Mineral 88:1046-1054
73. 29Si NMR study. Am Mineral 79:848-861
74. 29Si MAS NMR study of diopside-Ca-Tschermak clinopyroxenes: Detecting both tetrahedral and octahedral Al substitution. Am Mineral 87:25-36
75. Florian P, Vermillion KE, Grandinetti P.J., Farnan I., Stebbins J.F. (1996) Cation distribution in mixed alkali disilicate glasses. J Am Chem Soc 118:3493-3497
76. 27A1 NMR/quantum chemical calculations. Chem Mater 24:4068-4079
77. Fukushima E, Roedder SBW (1981) Experimental Pulse NMR. Addison-Wesley, Reading, MA
78. Fyfe CA (1983) Solid State NMR for Chemists. CFC Press, Guelph
79. 3. Geochim Cosmochim Acta 72:1222-1230
80. 23Na NMR data for albite: comparison to chemical shift models. Am Mineral 80:878-884
81. George AM, Stebbins J.F. (1996) Dynamics of Na in sodium aluminosilicate glasses and liquids. Phys Chem Miner 23:526-534
82. 4)3. Solid State Commun 2:361-362
83. 3+ in aluminosilicates. Am Mineral 58:748-755
84. 29Si MAS NMR studies of the spin-lattice relaxation time and bond-angle distribution in vitreous silica. Philos Mag B 53:L81-L87
85. Graetsch H, Gies H, Topalovic I. (1994) NMR, XRD and IR study on microcrystalline opals. Phys Chem Miner 21:166-175
86. Grey CP, Dupré N (2004) NMR studies of cathode materials for lithium-ion rechargeable batteries. Chem Rev 104:4493-4512
87. 119Sn MAS NMR. The use of parmagnetic shift probes in the solid state. J Am Chem Soc 111:505-511
88. 89Y MAS NMR study of rare-earth pyrochlores-paramagnetic shifts in the solid state. J Am Chem Soc 112:4670-4680
89. 170 NMR spectroscopy of hydrous magnesium silicates: Evidence for proton dyanmics. J Phys Chem C 113:465-471
90. Griffin JM, Berry AJ, Frost D.J., Wimperis S., Ashbrook S.E. (2013) Water in the Earth's mantle: a solid-state NMR study of hydrous wadsleyite. Chem Sci 4:1523-1538
91. 3 groups in clinopyroxene. Geochim Cosmochim Acta 74:5672-5679
92. Harley SJ, Ohlin CA, Casey W.H. (2011) Geochemical kinetics via the Swift-Connick equations and solution NMR. Geochim Cosmochim Acta 75:3711-3725
93. Harris RK (1983) Nuclear Magnetic Resonance Spectroscopy. Pitman, London
94. Harris RK, Knight CTG (1983) Silicon-29 nuclear magnetic resonance studies of aqueous silicate solutions. V. First-order patterns in potassium silicate solutions enriched with silicon-29. J Chem Soc Farad Trans 79:1524-1538
95. 29Si NMR spin-lattice relaxation studies. Can J Chem 85:56-65
96. Hawthorne FC, Welch MD, Delia Ventura G, Liu S, Robert J-L, Jenkins DM (2000) Short-range order in synthetic aluminous tremolites: An infrared and triple-quantum MAS NMR study. Am Mineral 85:1716-1724
97. Herrero CP, Sanz J. (1991) Short-range order of the Si, Al distribution in layer silicates. J Phys Chem Solids 52:1129-1135
98. 29Si MAS-NMR spectroscopy of mica-type silicates: observed and predicted distribution of tetrahedral Al-Si. Phys Chem Mineral 15:84-90
99. Hidalgo C, Etchevers JD, Martinez-Richa A, Yee-Madeira H, Calderon HA, Vera-Graziano R, Matus F. (2010) Mineralogical characterization of the fine fraction (<2 μm) of degraded volcanic soils and tepetes in Mexico. Appl Clay Sci 49:348-358
100. wSi solid-state NMR. Clays Clay Miner 53:401-408
101. 29Si MAS-NMR investigation of nepheline-kalsilite crystalline solutions. Am Mineral 77:19-29
102. Hoyt DW, Turcu RVF, Sears JA, Rosso K.M., Burton SD, Felmy AR, Hu JZ (2011) High-pressure magic angle spinning nuclear magnetic resonance. J Magn Reson 212:378-385
103. 27A1 MAS NMR and aluminum x-ray absorption near-edge structure study of imogolite and allophanes. Clays Clay Miner 42:276-287
104. Jakobsen HJ, Nielsen NC, Lindgreen H. (1995) Sequences of charged sheets in rectorite. Am Mineral 80:247-252
105. Jenkins DM, Sherriff BL, Cramer J, Xu Z. (1997) Al, Si, and Mg occupancies in tetrahedrally and octahedrally coordinated sites in synthetic aluminous tremolite. Am Mineral 82:280-290
106. 1H MAS NMR. Am Mineral 88:901-911
107. Jonas J (ed) (1991) High Pressure NMR. Springer-Verlag, Berlin
108. 6] at ambient and high pressure. Phys Chem Miner 27:225-233
109. 27Al NMR study on dynamics of calcium aluminosilicate glass and melt. J Non-Cryst Solids 353:4001-4010
110. -2. Mineral J 18:1-8
111. Kanzaki M (2010) Crystal structure of a new high-pressure polymorph of topaz-OH. Am Mineral 95:1349-1352
112. 4 by NMR and powder X-ray diffraction. Inorg Chem 51:6164-6172
113. 4 by X-ray powder diffraction and NMR spectroscopy. Acta Crystallogr B 67:30-40
114. Keeler J (2010) Understanding NMR Spectroscopy. John Wiley & Sons Ltd., Chichester
115. Kelsey KE, Stebbins JF, Du L-S, Hankins B. (2007) Constraining "O and "Al NMR spectra of high pressure crystals and glasses: new data for jadeite, pyrope, grossular, and mullite. Am Mineral 92:210-216
116. 27Al MAS NMR spectroscopic study. Am Mineral 93:134-143
117. Kelsey KE, Stebbins JF, Mosenfelder J.L., Asimow P.D. (2009) Simultaneous aluminum, silicon, and sodium coordination changes in 6 GPa sodium aluminosilicate glasses. Am Mineral 94:1205-1215
118. 29Si RAPT-CPMG-HETCOR NMR. Solid State Nucl Magn Reson 33:76-81
119. 133Cs NMR study of cation adsorption on mineral surfaces: Local environments, dynamics, and effects of mixed cations. Geochim Cosmochim Acta 61:5199-5208
120. 11B NMR investigation of boron interaction with mineral surfaces: Results for boehmite, silica gel and illite. Geochim Cosmochim Acta 70:3231-3238
121. Kim N, Stebbins JF, Quartieri S, Oberti R. (2007) Scandium-45 NMR of pyrope-grossular garnets: resolution of multiple scandium sites and comparison with x-ray diffraction and x-ray spectroscopy. Am Mineral 92:1875-1880
122. 7Li solid-state MAS NMR study. J Am Chem Soc 130:1285-1295
123. 7Li solid-state NMR study of paramagnetic Fe(III) phosphates. J Am Chem Soc 132:16825-16840
124. 31P NMR study. Energy Environ Sci 4:4298-4305
125. Kinsey RA, Kirkpatrick RJ, Hower J, Smith K.A., Oldfield E. (1985) High resolution aluminum-27 and silicon-29 nuclear magnetic resonance studies of layer silicates, including clay minerals. Am Mineral 70:537-548
126. Kirkpatrick RJ (1988) MAS NMR spectroscopy of minerals and glasses. In: Spectroscopic Methods in Mineralogy and Geology. Hawthorne FC (ed) Mineralogical Society of America, Washington D.C., p 341-403
127. 27Al NMR spectroscopy of minerals and related materials. Appl Magn Reson 4:213-236
128. Kirkpatrick RJ, Dunn T, Schramm S., Smith KA, Oestrike R, Turner G. (1986) Magic-angle sample-spinning nuclear magnetic resonance spectroscopy of silicate glasses: a review. In: Structure and Bonding in Noncrystalline Solids. Walrafen G E, Revesz A G (eds) Plenum Press, New York, p 302-327
129. 29Si magic-angle NMR spectroscopy of low-temperature ordered plagioclase feldspars. Nature 325:236-238
130. 29Si MAS NMR studies of structural phase transitions of tridymite. Am Mineral 96:550-560
131. Klimm K, Kohn SC, O'Dell LA, Botcharnikov RE, Smith M.E. (2012) The dissolution mechanism of sulfur in hydrous silicate glasses. I: Assessment of analytical techniques in determining the sulfur speciation in iron-free and iron-poor glasses. Chem Geol 322:237-249
132. 11B MAS NMR. Am Mineral 73:1890-1900
133. 29Si nuclear magnetic resonance spectroscopic study of chemical exchange pathways in potassium silicate solutions. J Magn Reson 78:31-40
134. Kohn SC (2004) NMR studies of silicate glasses. EMU Notes Mineral 6:399-419
135. Kohn SC (2006) Structural studies of OH in nominally anhydrous minerals using NMR. Rev Mineral Geochem 62:53-62
136. 2 speciation in glasses. Geochim Cosmochim Acta 55:3879-3884
137. Kohn SC, Dupree R, Mortuza M.G., Henderson CMB (1991b) Evidence for five- and six-coordinated aluminum fluoride complexes in F-bearing aluminosilicate glasses. Am Mineral 76:309-312
138. Kohn SC, Henderson CMB, Dupree R. (1995) Si-Al order in leucite revisited; new information from an analcite-derived analogue. Am Mineral 80:705-714
139. Kohn SC, Roome BM, Smith M.E., Howes A.P. (2005) Testing a potential mantle geohygrometer; the effect of dissolved water on the intracrystalline partitioning of Al in orthopyroxene. Earth Planet Sci Lett 238:342-350
140. Kristensen JH, Farnan I. (2001) Measurement of molecular motion in solids by nuclear magnetic resonance spectroscopy of half-integer quadrupolar nuclei. J Chem Phys 114:9608-9624
141. 5 (titanite). Am Mineral 87:572-579
142. 27A1 solid-state NMR. J Phys Chem B 108:9764-9771
143. 29Si MAS NMR studies of illite and illite-smectite from shale. Am Mineral 84:1433-1438
144. Lee SK (2005) Microscopic origins of macroscopic properties of silicate melts and glasses at ambient and high pressure: implications for melt generation and dynamics. Geochim Cosmochim Acta 69:3695-3710
145. Lee SK, Stebbins J.F. (1999) The degree of aluminum avoidance in aluminosilicate glasses. Am Mineral 84:937-945
146. Lee SK, Stebbins J.F. (2000a) Al-O-Al and Si-O-Si sites in framework aluminosilicate glasses with Si/Al=l: quantification of framework disorder. J Non-Cryst Solids 270:260-264
147. 27A1 MAS and 3QMAS NMR study. J Phys Chem B 104:4091-4100
148. Lee SH, Conradi MS, Norberg R.E. (1992) Improved NMR resonator for diamond anvil cells. Rev Sci Instrum 63:36743676
149. Lee SK, Cody GD, Fei Y, Mysen B.O. (2004) Nature of polymerization and properties of silicate melts and glasses at high pressure. Geochim Cosmochim Acta 68:4189-4200
150. Lee SK, Cody GD, Mysen B.O. (2005) Structure and extent of disorder in quaternary (Ca-Mg and Ca-Na) aluminosilicate glasses and melts. Am Mineral 90:1393-1401
151. 170) 1D and 2D solid-state NMR study. Chem Geol 229:162-172
152. Lesage A (2009) Recent advances in solid-state NMR spectroscopy of spin 1= 1/2 nuclei. Phys Chem Chem Phys 11:6876-6891
153. Li W, Xu W, Parise J.B., Phillips B.L. (2012) Formation of hydroxylapatite from co-sorption of phosphate and calcium by boehmite. Geochim Cosmochim Acta 85:289-301
154. 31P solid-state NMR, ATR-FTIR and quantum chemical calculation. Geochim Cosmochim Acta 107:252-266
155. 29Si NMR spectroscopy. J Am Chem Soc 102:4889-4893
156. 170 NMR spectroscopy Geochim Cosmochim Acta 68:2791-2798
157. MacKenzie KJD, Smith M.E. (2002) Multinuclear Solid-State NMR of Inorganic Materials. Pergamon, New York
158. 5. Geochim Cosmochim Acta 61:2569-2576
159. 29Si MAS-NMR. J Non-Cryst Solids 127:53-64
160. 27A1 NMR study. Am Mineral 82:1125-1132
161. Mägi M, Lippmaa E, Samoson A., Engelhardt G, Grimmer A.R. (1984) Solid-state high-resolution silicon-29 chemical shifts in silicates. J Phys Chem 88:1518-1522
162. 1H NMR spectroscopy. Geochim Cosmochim Acta 74:719-737
163. 29Si NMR spectroscopy on alkali-silicate glasses. Geochim Cosmochim Acta 71:6002-6018
164. 2O: phase characterization, compositional relations, and excess H. Mineral Mag 73:957-996
165. Mason HE, Frisia S, Tang Y., Reeder RJ, Phillips B.L. (2007) Phosphorus speciation in calcite speleothems determined from solid-state NMR spectroscopy. Earth Planet Sci Lett 254:313-322
166. Mason HE, Montagna P, Kubista L., Taviani M, McCulloch M, Phillips B.L. (2011) Phosphate defects and apatite inclusions in coral skeletal aragonite revealed by solid-state NMR spectroscopy. Geochim Cosmochim Acta 75:7446-7457
167. Mason J (ed) (1987) Multinuclear NMR. Plenum Press, New York
168. 27A1 NMR time-resolved study. J Phys Chem 99:16455-16459
169. Massiot D, Fayon F, Deschamps M., Cadars S, Florian P, Montouillout V., Pellerin N, Hiet J, Rakhmatullin A, Bessada C (2010) Detection and use of small J couplings in solid state NMR experiments. C R Acad Sci Paris 13:117-129
170. McMillan PF, Kirkpatrick R.J. (1992) Al coordination in magnesium aluminosilicate glasses. Am Mineral 77:898-900
171. 12 join: an infrared, Raman, and NMR study. Phys Chem Miner 16:428-435
172. 27Al NMR study of alkaline earth aluminosilicate glasses. J Non-Cryst Solids 124:194-206
173. 170 magic-angle spinning NMR. Am Mineral 77:44-52
174. 170 MAS NMR and Rietveld refinement of X-ray diffraction data. Am Mineral 80:885-896
175. Morrow CP, Yazaydin AO, Krishnan M, Bowers G.M., Kalinichev AG, Kirkpatrick R.J. (2013) Structure, energetics, and dynamics of smectite clay interlayer hydration: molecular dynamics and metadynamics investigation of Na-hectorite. J Phys Chem C 117:5172-5187
176. wSi NMR study of silicate and aluminosilicate glasses: the effect of network-modifying cations. Am Mineral 70:332-343
177. Murdoch JB, Stebbins JF, Carmichael ISE, Pines A. (1988) A silicon-29 nuclear magnetic resonance study of silicon-aluminum ordering in leucite and analcite. Phys Chem Miner 15:370-382
178. Mysen BO, Richet P. (2005) Silicate Glasses and Melts, Properties and Structure. Elsevier, Amsterdam
179. 170 NMR spectroscopy. J Phys Chem B 116:2696-2702
180. 27A1 MAS NMR study. Am Mineral 87:1307-1320
181. Neuhoff PS, Stebbins JF, Bird D.K. (2003) Si-Al disorder and solid solutions in analcime, chabazite, and wairikite. Am Mineral 88:410-423
182. 27AlMQ-MAS NMR and Raman spectroscopy. Chem Geol 229:173-185
183. 6Li MAS NMR study of adsorption and absorption on goethite. J Phys Chem B 109:18310-18315
184. 33S MAS NMR of a disordered sulfur-doped silicate: signal enhancement via RAPT, QCPMG and adiabatic pulses. Appl Magn Reson 35:247-259
185. 4, monazite/xenotime) solid solutions. Am Mineral 96:1343-1353
186. 29Si NMR studies of synthetic forsterite and Fe-bearing Dora Maira pyrope garnet: temperature dependence and mechanisms of contact-shifted peaks. Am Mineral 96:1090-1099
187. 29Si NMR spectroscopy. Am Mineral 97:1955-1964
188. 3 glass: simulation from first-principles. Phys Chem Chem Phys 12:6054-6066
189. Petch HE, Cranna NG, Volkoff G.M. (1953) Second order nuclear quadrupolar effects in single crystals, part II. Experimental results for spodumene. Can J Phys 31:837-858
190. 27A1 and variable-temperature "Si NMR spectroscopy of leucite, its Cs- and Rb-exchanged derivatives, and analcime. Am Mineral 79:1025-1036
191. 8) and its P1-I1 structural phase transition. Phys Chem Miner 22:268-276
192. 23Na MAS NMR study of an Al, Si ordered alkali feldspar solid solution series. Phys Chem Miner 16:262-275
193. 27Al MAS NMR spectroscopy. Am Mineral 77:704-712
194. 29Si MAS NMR spectroscopy. Am Mineral 77:484-495
195. 1H NMR spectroscopy of high-pressure hydrous magnesium silicates. Phys Chem Mineral 24:179-190
196. 3-x(aq) complexes: ligand-directed labilization of water as an analog for ligand-induced dissolution of oxide minerals. Geochim Cosmochim Acta 61:3041-3049
197. 29Si MAS-NMR spectroscopic study. Am Mineral 82:1-7
198. 4): The enthalpy of Si, Al ordering. Am Mineral 85:181-188
199. Phillips BL, Mason HE, Guggenheim S. (2007) Hydrogen bonded silanols in the 10 Å phase: Evidence from NMR spectroscopy. Am Mineral 92:1474-1485
200. Pickard CJ, Mauri FPRB (2001) All-electron magnetic response with pseudopotentials: NMR chemical shifts. Phys Rev B 63:245101
201. Pound RV (1950) Nuclear quadrupolar interactions in crystals. Phys Rev 79:685-702
202. 2: Assignment of the zeolite ferrierite spectrum. J Am Chem Soc 125:541-548
203. 170 NMR parameters in Ca oxide and Ca aluminosilicates: the partially covalent nature of the Ca-0 bond, a challenge for density functional theory. J Am Chem Soc 126:12628-12635
204. Putnis A (1988) Solid state NMR spectroscopy and phase transitions in minerals. In: Physical Properties and Thermodynamic Behaviour of Minerals. Salje EKH (ed) Reidel, Dordrecht, p 325-358
205. Putnis A (1992) Introduction to Mineral Sciences. Cambridge University Press, Cambridge
206. Putnis A, Angel R.J. (1985) Al, Si ordering in cordierite using magic angle spinning NMR. 2. Models of Al, Si order from NMR data. Phys Chem Miner 12:217-222
207. Putnis A, Fyfe CA, Gobbi G.C. (1985) Al, Si ordering in cordierite using "magic angle spinning" NMR. Phys Chem Miner 12:211-216
208. 19F MAS NMR spectroscopy. Am Mineral 72:580-593
209. Richet P (1984) Viscosity and configurational entropy of silicate melts. Geochim Cosmochim Acta 48:471-483
210. 2O/OH ratio determination in hydrous aluminosilicate glasses by static proton NMR and the effect of chemical shift anisotropy. Solid State Nucl Magn Reson 15:201-207
211. Sanders RL, Washton NM, Mueller K.T. (2010) Measurement of the reactive surface area of clay minerals using solid-state NMR studies of a probe molecule. J Phys Chem C 114:5491-5498
212. 35C1 MAS-NMR study. Geochim Cosmochim Acta 68:5059-5069
213. 27Al NMR chemical shifts of 2:1 phyllosilicates. Phys Chem Miner 19:39-45
214. - in the octahedral sheet of phlogopites. Am Mineral 64:119-126
215. Sanz J, Herrero CP, Robert J-L (2003) Distribution of Si and Al in clintonites: a combined NMR and Monte-Carlo study. J Phys Chem B 107
216. 29Si NMR chemical shift of 2:1 phyllosilicates. Am Mineral 91:544-550
217. Schmidt BC, Riemer T, Kohn S.C., Behrens H., Dupree R. (2000) Different water solubility mechanisms in hydrous glasses along the Qz-Ab join: evidence from NMR spectroscopy. Geochim Cosmochim Acta 64:513-526
218. 27A1 MAS NMR investigation of Miocene Gulf Coast shales with application to understanding illite/smectite crystal-chemistry. Clays Clay Miner 41:668-679
219. Sen S (2008) Differential mobility and spatially heterogeneous dynamics of oxygen atoms in a supercooled glass-forming network liquid. Phys Rev B 78:100201
220. 29Si MAS NMR spin-lattice relaxation study. Phys Rev 50:822-830
221. 11B NMR spin-lattice relaxation study. Phys Rev B 55:3512-3519
222. 4 glass and melt. Am Mineral 93:946-949
223. 11B MAS NMR study. Am Mineral 79:819-825
224. 25Mg MAS NMR spectroscopy. J Phys Chem B 113:152434-115248
225. Sharps JA, Brown GE, Jr., Stebbins JF (1993) Kinetics and mechanism of ligand exchange of Au(III), Zn(II), and Cd(II) chlorides in aqueous solution: An NMR study from 28-98 °C. Geochim Cosmochim Acta 57:721-731
226. 29Si NMR of feldspars: Al-Si disorder and the effects of paramagnetic centres. Can Mineral 23:205-212
227. 29Si MAS NMR chemical shift and silicate mineral structure. Eur J Mineral 3:751-768
228. Sideris PJ, Nielsen UG, Gan Z.H., Grey C.P. (2008) Mg/Al ordering in layered double hydroxides revealed by multinuclear NMR spectroscopy. Science 5885:113-117
229. 43Ca NMR and computational molecular dynamics investigation. Chem Mater 24:1828-1836
230. Smith KA, Kirkpatrick RJ, Oldfield E, Henderson D.M. (1983) High-resolution silicon-29 nuclear magnetic resonance spectroscopic study of rock-forming silicates. Am Mineral 68:1206-1215
231. 29Si NMR shielding tensor in low quartz. Am Mineral 74:956-959
232. 17O NMR. Phys Chem Miner 19:307-321
233. 14): multi-nuclear NMR studies. Phys Chem Miner 21:373-386
234. 8. Zeit Kristallogr 140:360-373
235. 29Si NMR. Nature 330:465-467
236. Stebbins JF (1988) NMR spectroscopy and dynamic processes in mineralogy and geochemistry. Rev Mineral 18:405-430
237. Stebbins JF (1991a) Experimental confirmation of five-coordinated silicon in a silicate glass at 1 atmosphere pressure. Nature 351:638-639
238. Stebbins JF (1991b) Nuclear magnetic resonance at high temperature. Chem Rev 91:1353-1373
239. Stebbins JF (1995a) Dynamics and structure of silicate and oxide melts: nuclear magnetic resonance studies. In: Structure, Dynamics, and Properties of Silicate Melts. Stebbins JF, McMillan PF, Dingwell DB (eds) Mineralogical Society of America, Washington, D.C., p 191-246
240. Stebbins JF (1995b) Nuclear magnetic resonance spectroscopy of silicates and oxides in geochemistry and geophysics. In: Handbook of Physical Constants. Ahrens TJ (ed) American Geophysical Union, Washington D.C., p 303-332
241. MMg nuclear magnetic resonance spectroscopy. Am Mineral 81:1315-1320
242. Stebbins JF (2002) NMR studies of oxide glass structure. In: Solid State NMR: Theory and Applications. Duer M (ed) Blackwell Scientific, Oxford, p 391-436
243. Stebbins JF (2008) Temperature effects on the network structure of oxide melts and their consequences for configurational heat capacity. Chem Geol 256:80-91
244. Stebbins JF, Farnan I. (1989) NMR spectroscopy in the earth sciences: structure and dynamics. Science 245:257-262
245. Stebbins JF, Farnan I. (1992) The effects of temperature on silicate liquid structure: a multi-nuclear, high temperature NMR study. Science 255:586-589
246. Stebbins JF, Kanzaki M. (1990) Local structure and chemical shifts for six-coordinated silicon in high pressure mantle phases. Science 251:294-298
247. 9 glass quenched from 1.9 GPa and 1200°C. Am Mineral 74:965-968
248. 5). Geophys Res Lett 26:2521-2523
249. Stebbins JF, Sen S. (2013) Oxide ion speciation in potassium silicate glasses: new limits from "0 NMR. J Non-Cryst Solids 368:17-22
250. Stebbins JF, Xu Z. (1997) NMR evidence for excess non-bridging oxygens in an aluminosilicate glass. Nature 390:60-62
251. 29Si in molten silicates. Nature 314:250-252
252. CC. Phys Chem Minerals 16:763-766
253. Stebbins JF, Farnan I, Xue X. (1992) The structure and dynamics of alkali silicate liquids: one view from NMR spectroscopy. Chem Geol 96:371-386
254. Stebbins JF, Zhao P, Lee S.K., Cheng X. (1999) Reactive Al-O-Al sites in a natural zeolite: triple-quantum oxygen-17 nuclear magnetic resonance. Am Mineral 84:1680-1684
255. Stebbins JF, Oglesby JV, Lee S.K. (2001) Oxygen sites in silicate glasses: a new view from oxygen-17 NMR. Chem Geol 174:63-75
256. Stebbins JF, Du L-S, Pratesi G. (2005) Aluminum coordination in natural silica glasses from the Libyan Desert (Egypt): high field NMR results. Phys Chem Glasses 46:340-344
257. 27A1 NMR. Am Mineral 91:337-343
258. Stebbins JF, Dubinsky EV, Kanehashi K, Kelsey K.E. (2008) Temperature effects on non-bridging oxygen and aluminum coordination number in calcium aluminosilicate glasses and melts. Geochim Cosmochim Acta 72:910-925
259. Stebbins JF, Kim N, Andrejcak M.J., Boymel PM, Zoitos B.K. (2009a) Characterization of phase separation and thermal history effects in magnesium silicate glass fibers by NMR spectroscopy. J Am Ceram Soc 92:68-74
260. 3IP NMR. Eur J Mineral 21:667-671
261. 29Si NMR constraints on structural disorder and effects of paramagnetic impurity ions. Am Mineral 94:626-629
262. MSi NMR results for chemical shift anisotropy, spin-lattice relaxation, and mechanism of hydration. Am Mineral 94:905-915
263. Stebbins JF, Wu J, Thompson L.M. (2013) Interactions between network cation coordination and non-bridging oxygen abundance in oxide melts and glasses: insights from NMR spectroscopy. Chem Geol 346:34-46
264. 13C NMR. Environ Sci Technol 47:119-125
265. 2+ ion. Science 308:1450-1453
266. 17 in aqueous solutions of paramagnetic cations and the lifetime of water molecules in the first coordination sphere. J Chem Phys 37:307-320
267. 27A1 multiple quantum MAS NMR. Clays Clay Miner 56:520-525
268. Teertstra DK, Sherriff BL, Xu Z, Cerny P. (1994) MAS and DOR NMR study of Al-Si order in the analcime-pollucite series. Can Mineral 32:69-80
269. 27A1 MAS NMR results. Am Mineral 96:841-853
270. 170 NMR measurements in oxide glasses: Constraints and evidence from crystalline and glassy calcium and barium silicates. J Non-Cryst Solids 358:2999-3006
271. Timken HKC, Janes N, Turner G.L., Lambert SL, Welsh LB, Oldfield E. (1986) Solid-state oxygen-17 nuclear magnetic resonance spectroscopic studies of zeolites and related systems. 2. J Am Chem Soc 108:7236-7241
272. Toplis MJ, Kohn SC, Smith M.E., Poplett JJF (2000) Five coordinate aluminum in tectosilicate glasses observed by triple quantum MAS NMR. Am Mineral 85:1556-1560
273. Tossell JA (2001) Calculating the NMR properties of minerals, glasses, and aqueous species. Rev Mineral Geochem 43:437-458
274. Tsomaia N, Brantley SL, Hamilton J.P., Pantano CG, Mueller K.T. (2003) NMR evidence for formation of octahedral and tetrahedral Al and repolymerization of the Si network during dissolution of aluminosilicate glass and crystal. Am Mineral 88:54-67
275. 29Si NMR spectra. Phys Chem Mineral 22:87-98
276. 29Si NMR data. Phys Chem Minerals 23:391-401
277. Washton NM, Brantley SL, Mueller K.T. (2008) Probing the molecular-level control on aluminosilicate dissolution: A sensitive solid-state NMR proxy for reactive surface area. Geochim Cosmochim Acta 72:5949-5961
278. Wasylishen RE, Ashbrook SE, Wimperis S (eds) (2012) NMR of Quadrupolar Nuclei in Solid Materials. John Wiley & Sons Ltd., Chichester, UK
279. 133Cs variable-temperature MAS NMR spectroscopic study of hectorite. Geochim Cosmochim Acta 54:1655-1669
280. 133Cs MAS nuclear magnetic resonance spectroscopy. Am Mineral 75:970-982
281. Welch MD, Rocha J, Klinowski J. (1992) Characterization of polysomatism in biopyriboles: double-/triple-chain lamellar intergrowths. Phys Chem Mineral 18:460-468
282. Welch MD, Kolodziejski W, Klinowski J. (1994) A multinuclear NMR study of synthetic pargasite. Am Mineral 79:261-268
283. 29Si MAS NMR systematics of calcic and sodic-calcic amphiboles. Am Mineral 83:85-96
284. Wiench JW, Pruski M. (2004) Probing through bond connectivities with MQMAS NMR. Solid State Nucl Magn Reson 26:51-55
285. 27A1 nuclear magnetic resonance spectroscopy. Am Mineral 74:203-215
286. 4 spinel. Am Mineral 71:999-1006
287. 29Si MAS NMR. Mineral Mag 59:46-61
288. Xu Z, Maekawa H, Oglesby J.V., Stebbins J.F. (1998) Oxygen speciation in hydrous silicate glasses - An oxygen-17 NMR study. J Am Chem Soc 120:9894-9901
289. 6Li nuclear magnetic resonance chemical shifts, coordination number and relaxation in crystalline and glassy silicates. Solid State Nucl Magn Reson 5:103-112
290. Xu Z, Stebbins J.F. (1998) Oxygen site exchange kinetics observed with solid state NMR in a natural zeolite. Geochim Cosmochim Acta 62:1803-1809
291. 1H double-resonance NMR. Am Mineral 94:395-398
292. 1H NMR properties and local structures in silicates: an ab initio calculation. Phys Chem Mineral 26:14-30
293. 1H NMR parameters for various OH groups: Implications to the speciation and dynamics of dissolved water in silicate glasses. J Phys Chem B 105: 3422-3434
294. 29Si NMR spectroscopy and ab initio calculations. Geochim Cosmochim Acta 68:5027-5057
295. 27A1 heteronuclear correlation NMR. Am Mineral 91:1922-1926
296. 27Al correlation NMR. Solid State Nucl Magn Reson 31:10-27
297. 27A1 NMR. J Phys Chem B 111:13156-13166
298. 27A1 NMR study. Geochim Cosmochim Acta 72:2331-2348
299. Xue X, Kanzaki M. (2009) Proton distributions and hydrogen bonding in crystalline and glassy hydrous silicates and related inorganic materials: insights from high-resolution solid-state NMR spectroscopy. J Am Ceram Soc 92:2803-2830
300. 2O). J Phys Chem C 116:10714-10722
301. Xue X, Stebbins JF, Kanzaki M, McMillan P.F., Poe B. (1991) Pressure-induced silicon coordination and tetrahedral structural changes in alkali silicate melts up to 12 GPa: NMR, Raman, and infrared spectroscopy. Am Mineral 76:8-26
302. 2O system: An NMR and Raman study. Am Mineral 91:850-861
303. 1H NMR. Am Mineral 93:1099-1111
304. 27Al NMR study. Am Mineral 94:1739-1742
305. Xue X, Kanzaki M, Fukui H. (2010) Unique crystal chemistry of two polymorphs of topaz-OH: A multi-nuclear NMR and Raman study. Am Mineral 95:1276-1293
306. Yang W-H, Kirkpatrick R.J. (1989) Hydrothermal reaction of albite and a sodium aluminosilicate glass: A solid-state NMR study. Geochim Cosmochim Acta 53:805-819
307. Yang W-H, Kirkpatrick R.J. (1990) Hydrothermal reaction of a rhyolitic-composition glass: a solid-state NMR study. Am Mineral 75:1009-1019
308. Yarger JL, Smith KH, Nieman R.A., Diefenbacher J., Wolf GH, Poe BT, McMillan P.F. (1995) Al coordination changes in high-pressure aluminosilicate liquids. Science 270:1964-1967
309. Yates JR (2010) Prediction of NMR J-coupling in solids with the planewave pseudopotential approach. Magn Reson Chem 48:S23-S31
310. 1H MAS NMR at high spinning speeds. J Am Chem Soc 109:6274-6282
311. 1H MAS NMR. J Am Chem Soc 110:1367-1375
312. 19F NMR results. Am Mineral 85:863-867
313. 23 Na TRAPDOOR NMR study. J Phys Chem B 103:7406-7415
314. 29Si nuclear magnetic resonance. J Non-Cryst Solids 204:294-300