High-pressure magic angle spinning nuclear magnetic resonance

Journal of Magnetic Resonance

Volumn 212, Issue 2, 2011, Pages 378-385

  Hoyt, David W ^a,b   Turcu, Romulus V F ^a,b   Sears, Jesse A ^a,b   Rosso, Kevin M ^a,b   Burton, Sarah D ^a,b   Felmy, Andrew R ^a,b   Hu, Jian Zhi ^a,b  

^a PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

^b PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

Author keywords

Carbon sequestration; CO 2; High pressure MAS NMR; In situ NMR

Indexed keywords

APPLICATION EXAMPLES; BACKGROUND SIGNALS; CARBON SEQUESTRATION; CERAMIC CYLINDER; EXTERNAL PRESSURES; FORSTERITES; GEOLOGICAL SEQUESTRATION; IN-SITU; INTERNAL PRESSURE; INTERNAL SURFACES; MAGIC ANGLE SPINNING NMR; MAGIC ANGLE SPINNING NUCLEAR MAGNETIC RESONANCE; MAS NMR; MINERAL CARBONATION; RF COIL; SUPERCRITICAL CO; TECHNICAL CHALLENGES;

CARBON DIOXIDE; CERAMIC MATERIALS; COMPUTER SOFTWARE REUSABILITY; CYLINDERS (SHAPES); O RINGS; OLIVINE; REACTION INTERMEDIATES; SILICON COMPOUNDS;

NUCLEAR MAGNETIC RESONANCE;

BICARBONATE; CARBON DIOXIDE; MAGNESIUM ORTHOSILICATE; SILICON DERIVATIVE; WATER;

ARTICLE; CHEMISTRY; INSTRUMENTATION; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

BICARBONATES; CARBON DIOXIDE; MAGNETIC RESONANCE SPECTROSCOPY; SILICON COMPOUNDS; WATER;

EID: 80053290703     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2011.07.019     Document Type: Article

References (30)

1. F. Bloch, W.W. Hansen, and M. Packard Nuclear induction Phys. Rev. 69 1946 127
2. E.M. Purcell, H.C. Torrey, and R.V. Pound Resonance absorption by nuclear magnetic moments in a solid Phys. Rev. 69 1946 37
3. E.R. Andrew, A. Bradbury, and R.G. Eades Nuclear magnetic resonance spectra from a crystal rotated at high speed Nature 182 1959 1659
4. I.J. Lowe Free induction decays of rotating solids Phys. Rev. Lett. 2 1959 285
5. M.G. Pravica, and I.F. Silvera Nuclear magnetic resonance in a diamond anvil cell at very high pressures Rev. Sci. Instrum. 69 2 1998 479 484 (Pubitemid 128599989)
6. 2 gas Macromolecules 30 21 1997 6582 6585 (Pubitemid 127564848)
7. 129Xe high-pressure MAS NMR Macromolecules 35 1 2002 151 154 (Pubitemid 34064314)
8. 129Xe nmr study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend Polymer 38 21 1997 5475 5480 (Pubitemid 127428162)
9. C.R. Yonker, and J.C. Linehan The use of supercritical fluids as solvents for NMR spectroscopy Prog. Nucl. Magn. Reson. Spectrosc. 47 2005 95 109 (Pubitemid 41446977)
10. T. Deuchande, O. Breton, J. Haedelt, and E. Hughes High-pressure magic angle spinning J. Magn. Reson. 183 2006 178 182
11. D.W. Hoyt, J.A. Sears, R.V.F. Turcu, K.M. Rosso, J.Z. Hu, A method for high-pressure magic angle spinning nuclear magnetic resonance. US Patent and Trademark office - Patent Pending, November 4, 2010.
12. S. Bai, C.M. Taylor, C.L. Mayne, R.J. Pugmire, and D.M. Grant A new high-pressure sapphire nuclear magnetic resonance cell Rev. Sci. Instrum. 67 1 1996 240 243 (Pubitemid 126617886)
13. ISCO DM100, Teledyne Isco, Inc., Lincoln, NE, 68504.
14. High-pressure Generator, High-pressure Equipment Company, Erie, PA, 16505.
15. Cimarec, Thermo Fisher Scientific, Inc., Waltham, MA 02454.
16. D.I. Hoult, and R.E. Richards The signal-to-noise ratio of the nuclear magnetic resonance experiment J. Magn. Reson. 24 1976 71 85
17. D.W. Alderman, and D.M. Grant An efficient decoupling coil design which reduces heating in conductive samples in superconducting spectrometer J. Magn. Reson. 36 1979 447 451
18. 2 space Energy Convers. Manage. 43 1 2002 87 102 (Pubitemid 32998260)
19. 2 in solution Energy Convers. Manage. 44 20 2003 3151 3175
20. 2 storage in geological media: role, means, status and barriers to deployment Prog. Energy Combust. 34 2 2008 254 273 (Pubitemid 351179081)
21. S.M. Benson, and T. Surles Carbon dioxide capture and storage: an overview with emphasis on capture and storage in deep geological formations Proc. IEEE 94 10 2006 1795 1805
22. S. Angus, B. Armstrong, K.M. deRuck (Eds.), International Thermodynamic Tables of the Fluid State - Carbon Dioxide, Pergamon, Oxford, New York, Toronto, Sydney, Paris, Frankfut, 1976.
23. J.P. Kaszuba, D.R. Janecky, and M.G. Snow Carbon dioxide reaction processes in a model brine aquifer at 200 °C and 200° bars: implications for geologic sequestration of carbon Appl. Geochem. 18 7 2003 1065 1080 (Pubitemid 36573191)
24. J.P. Kaszuba, D.R. Janecky, and M.G. Snow Experimental evaluation of mixed fluid reactions between supercritical carbon dioxide and NaCl brine: relevance to the integrity of a geologic carbon repository Chem. Geol. 217 3-4 2005 277 293
25. 2 SPE J. 8 1 2003 49 60
26. 2 in a sandstone formation Chem. Geol. 242 3-4 2007 319 346 (Pubitemid 47022913)
27. DuPont Performance Elastomers L.L.C., Wilmington, DE, 19809.
28. 2, Int. J. Greenhouse Gas Control, 10.1016/j.ijggc.2011.05.013.
29. G. Rasul, V.P. Reddy, L.Z. Zdunek, G.K.S. Prakash, and G.A. Olah Chemistry in superacids. 12. Carbonic acid and its mono- and diprotonation: NMR, ab initio, and IGLO investigation J. Am. Chem. Soc. 115 6 1993 2236 2238
30. 13C NMR spectroscopy J. Phys. Chem. C 114 9 2010 4126 4134