Determination of ephedrine and pseudoephedrine by field-amplified sample injection capillary electrophoresis

Journal of Chromatographic Science

Volumn 52, Issue 4, 2014, Pages 357-362

  Deng, Dongli ^a,b   Deng, Hao ^b   Zhang, Lichun ^b   Su, Yingying ^b  

^a CHONGQING INDUSTRY POLYTECHNIC COLLEGE   (China)

^b SICHUAN UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EPHEDRINE; PLANT EXTRACT; PSEUDOEPHEDRINE;

ARTICLE; CAPILLARY ELECTROPHORESIS; CHEMISTRY; EPHEDRA SINICA; LIMIT OF DETECTION; METHODOLOGY; PH; REPRODUCIBILITY; STATISTICAL MODEL;

ELECTROPHORESIS, CAPILLARY; EPHEDRA SINICA; EPHEDRINE; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; LINEAR MODELS; PLANT EXTRACTS; PSEUDOEPHEDRINE; REPRODUCIBILITY OF RESULTS;

EID: 84891486786     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/bmt039     Document Type: Article

References (30)

1. New Medical College of Jiangsu; Dictionary of Chinese traditional medicines. People's Publisher of Shanghai, Shanghai, China, (1977) pp. 2222-2225.
2. Josefson, D.; Herbal stimulant causes US deaths; British Medical Journal, (1996); 312: 1378-1379.
3. Macek, J., Ptacek, P., Klima, J.; Rapid determination of pseudoephe-drine in human plasma by high-performance liquid chromatography; Journal of Chromatography B, (2002); 766: 289-294. (Pubitemid 34142361)
4. Marchei, E., Pellegrini, M., Pacifici, R., Zuccaro, P., Pichini, S.; A rapid and simple procedure for the determination of ephedrine alkaloids in dietary supplements by gas chromatography-mass spectrometry; Journal of Pharmaceutical and Biomedical Analysis, (2006); 41: 1633-1641. (Pubitemid 44247465)
5. Li, H.X., Ding, M.Y., Lv, K., Yu, J.Y.; Separation and determination of ephedrine alkaloids and tetramethylpyrazine in Ephedra sinica Stapf by gas chromatography-mass spectrometry; Journal of Chromatographic Science, (2001); 39: 370-374. (Pubitemid 34984103)
6. Wang, M., Marriott, P.J., Chan, W.H., Lee, A.W.M., Huie, C.W.; Enantiomeric separation and quantification of ephedrine-type alkaloids in herbal materials by comprehensive two-dimensional gas chromatography; Journal of Chromatography A, (2006); 1112: 361-368.
7. Imaz, C., Navajas, R., Carreras, D., Rodriguez, C., Rodriguez, A.F.; Comparison of various reversed-phase columns for the simultaneous determination of ephedrines in urine by high-performance liquid chromatography; Journal of Chromatography A, (2000); 870: 23-28. (Pubitemid 30077405)
8. Pellati, F., Benvenuti, S.; Determination of ephedrine alkaloids in Ephedra natural products using HPLC on a pentafluorophenylpropyl stationary phase; Journal of Pharmaceutical and Biomedical Analysis, (2008); 48: 254-263.
9. Gray, N., Museng, A., Cowan, D.A., Plumb, R., Smith, N.W.; A simple high pH liquid chromatography-tandem mass spectrometry method for basic compounds: Application to ephedrines in doping control analysis; Journal of Chromatography A, (2011); 1218: 2098-2105.
10. Bagheri, H., Khalilian, F., Ahangar, L.E.; Liquid-liquid-liquid microex-traction followed by HPLC with UV detection for quantitation of ephedrine in urine; Journal of Separation Science, (2008); 31: 3212-3217.
11. Chen, H.L., Chen, X.G., Pu, Q.S., Hu, Z.D., Zhao, Z.F., Hooper, M.; Separation and determination of ephedrine and pseudoephedrine by combination of flow injection with capillary electrophoresis; Journal of Chromatographic Science, (2003); 41: 1-5.
12. Li, G.B., Zhang, Z.P., Chen, X.G., Hu, Z.D., Zhao, Z.F., Hooper, M.; Analysis of ephedrine in Ephedra callus by acetonitrile modified capillary zone electrophoresis; Talanta, (1999); 48: 1023-1029.
13. Jiang, T.F., Lv, Z.H., Wang, Y.H.; Chiral separation of ephedrine alkaloids from Ephedra sinica extract and its medicinal preparation using cyclodextrin-modified capillary zone electrophoresis; Journal of Analytical Chemistry, (2007); 62: 85-89.
14. Li, F., Ding, Z.T., Cao, Q.E.; Separation and determination of ephe-drine and pseudoephedrine in Ephedrae Herba by CZE modified with a CUOO-L-lysine complex; Electrophoresis, (2008); 29: 658-664. (Pubitemid 351266756)
15. Huang, H.Y., Hsieh, Y.Z.; Determination of puerarin, daidzein, paeoni-florin, cinnamic acid, glycyrrhizin, ephedrine, and [6]-gingerol in Ge-gen-tang by micellar electrokinetic chromatography; Analytical Chimica Acta, (1997); 351: 49-55.
16. Borst, C., Holzgrabe, U.; Comparison of chiral electrophoretic separation methods for phenethylamines and application on impurity analysis; Journal of Pharmaceutical and Biomedical Analysis, (2010); 53: 1201-1209.
17. Wei, F., Zhang, M., Feng, Y.Q.; Combining poly (methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction and on-line pre-concentration-capillary electrophoresis for analysis of ephedrine and pseudoephedrine; Journal of Chromatography B, (2007); 850: 38-44. (Pubitemid 46618144)
18. Fang, H.F., Liu, M.M., Zeng, Z.R.; Solid-phase microextraction coupled with capillary electrophoresis to determine ephedrine derivatives in water and urine using a sol-gel derived butyl methacrylate/silicone fiber; Talanta, (2006); 68: 979-986.
19. Deng, D.L., Zhang, J.Y., Chen, C., Hou, X.L., Su, Y.Y., Wu, L.; Monolithic molecular imprinted polymer fiber for recognition and solid phase microextraction of ephedrine and pseudoephedrine in biological samples prior to capillary electrophoresis analysis; Journal of Chromatography A, (2012); 1219: 195-200.
20. Zhang, J.Y., Xie, J.P., Chen, X.G., Hu, Z.D.; Sensitive determination of ephedrine and pseudoephedrine by capillary electrophoresis with laser-induced fluorescence detection; Analyst (2003); 128: 369-372.
21. Zhang, J.Y., Xie, J.P., Liu, J.Q., Tian, J.N., Chen, X.G., Hu, Z.D.; Microemulsion electrokinetic chromatography with laser-induced fluorescence detection for sensitive determination of ephedrine and pseudoephedrine; Electrophoresis, (2004); 25: 74-79.
22. Zhou, L., Zhou, X.M., Luo, Z., Wang, W.P., Yan, N., Hu, Z.D.; In-capillary derivatization and analysis of ephedrine and pseudoe-phedrine by micellar electrokinetic chromatography with laser-induced fluorescence detection; Journal of Chromatography A, (2008); 1190: 383-389.
23. Yu, L.S., Xu, X.Q., Huang, L., Lin, J.M., Chen, G.N.; Microemulsion electrokinetic chromatography coupling with field amplified sample injection and electroosmotic flow suppressant for analysis of some quinolizidine alkaloids; Journal of Chromatography A, (2008); 1198-1199: 220-225.
24. Zinellu, A., Sotgia, S., Campesi, I., Franconi, F., Deiana, L., Carru, C.; Measurement of carnosine, homocarnosine and anserine by FASI capillary electrophoresis UV detection: Applications on biological samples; Talanta, (2011); 84: 931-935.
25. Santalad, A., Burakham, R., Srijaranai, S., Grudpan, K.; Field-amplified sample injection and in-capillary derivatization for capillary electrophoretic analysis of metal ions in local wines; Microchemical Journal, (2007); 86: 209-215.
26. Aturki, Z., Fanali, S.; Use of beta-cyclodextrin polymer as a chiral selector in capillary electrophoresis; Journal of Chromatography A, (1994); 680: 137-146. (Pubitemid 24305515)
27. Flurer, C.L., Lin, L.A., Satzger, R.D., Wolnik, K.A.; Determination of ephedrine compounds in nutritional supplements by cyclodextrin-modified capillary electrophoresis; Journal of Chromatography B, (1995); 669: 133-139.
28. Mitnik, L., Salome, L., Viovy, J.L., Heller, C.; Systematic study of field and concentration effects in capillary electrophoresis of DNA in polymer solutions; Journal of Chromatography A, (1995); 710: 309-321.
29. Tilley, M., Bean, S.R., Tilley, K.A.; Capillary electrophoresis for monitoring dityrosine and 3-bromotyrosine synthesis; Journal of Chromatography A, (2006); 1103: 368-371. (Pubitemid 43069419)
30. Chien, R.L., Burgi, D.S.; On-column sample concentration using field amplification in CZE; Analytical Chemistry, (1992); 64: 489A-496A.