Determination of ephedrine alkaloids in Ephedra natural products using HPLC on a pentafluorophenylpropyl stationary phase

Journal of Pharmaceutical and Biomedical Analysis

Volumn 48, Issue 2, 2008, Pages 254-263

  Pellati, Federica ^a   Benvenuti, Stefania ^a  

^a UNIVERSITY OF MODENA AND REGGIO EMILIA   (Italy)

Author keywords

Ephedra; Ephedrine alkaloids; HPLC; Pentafluorophenylpropyl stationary phase; Phytochemical analysis; Synephrine

Indexed keywords

ACETONITRILE; ALKALOID DERIVATIVE; AMMONIUM ACETATE; EPHEDRINE; EPHEDRINE DERIVATIVE; METHYLEPHEDRINE; NOREPHEDRINE; NORPSEUDOEPHEDRINE; OXEDRINE; PENTRAFLUOROPHENYLPROPYL; PHENETHYLAMINE DERIVATIVE; PROPANE; PSEUDOEPHEDRINE; UNCLASSIFIED DRUG; WATER;

ACCURACY; ARTICLE; DRUG DETERMINATION; DRUG STRUCTURE; EPHEDRA; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NONHUMAN; PHYTOCHEMISTRY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; RELIABILITY; SENSITIVITY AND SPECIFICITY; SOUR ORANGE; VALIDATION STUDY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; EPHEDRA; EPHEDRINE;

EID: 50649097934     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2007.10.034     Document Type: Article

References (23)

1. Liu Y.M., Sheu S.J., Chiou S.H., Chang H.C., and Chen Y.P. Planta Med. 59 (1993) 376-378
2. Schaneberg B.T., Crockett S., Badir E., and Khan I.A. Phytochemistry 62 (2003) 911-918
3. Roman M.C. J. AOAC Int. 87 (2004) 1-14
4. Pellati F., and Benvenuti S. J. Chromatogr. A 1161 (2007) 71-88
5. Wang S.M., Lewis R.J., Canfield D., Li T.L., Chen C.Y., and Liu R.H. J. Chromatogr. B 825 (2005) 88-95
6. Wang M., Marriott P.J., Chan W.H., Lee A.W., and Huie C.W. J. Chromatogr. A 1112 (2006) 361-368
7. Hurlbut J.A., Carr J.R., Singleton E.R., Faul K.C., Madson M.R., Storey J.M., and Thomas T.L. J. AOAC Int. 81 (1998) 1121-1127
8. Okamura N., Miki H., Harada T., Yamashita S., Masaoka Y., Nakamoto Y., Tsuguma M., Yoshitomi H., and Yagi A. J. Pharm. Biomed. Anal. 20 (1999) 363-372
9. Niemann R.A., and Gay M.L. J. Agric. Food Chem. 51 (2003) 5630-5638
10. Schaneberg B.T., and Khan I.A. Pharmazie 59 (2004) 819-823
11. Ganzera M., Lanser C., and Stuppner H. Talanta 66 (2005) 889-894
12. Lam J.W.H., Gardner G.J., McCooeye M., Fraser C.A., and Sturgeon R.E. Anal. Bioanal. Chem. 383 (2005) 268-281
13. Sander L.C., Sharpless K.E., Satterfield M.B., Ihara T., Phinney K.W., Yen J.H., Wise S.A., Gay M.L., Lam J.W., McCooeye M., Gardner G., Fraser C., Sturgeon R., and Roman M. Anal. Chem. 77 (2005) 3101-3112
14. Gay M.L., White K.D., Obermeyer W.R., Betz J.M., and Musser S.M. J. AOAC Int. 84 (2001) 761-769
15. Gay M.L., Niemann R.A., and Musser S.M. J. Agric. Food Chem. 54 (2006) 285-291
16. Beyer J., Peters F.T., Kraemer T., and Maurer H.H. J. Mass Spectrom. 42 (2007) 150-160
17. Zhang J., Xie J., Chen X., and Hua Z. Analyst 128 (2003) 369-372
18. Chiang H.Y., and Sheu S.J. Electrophoresis 25 (2004) 670-676
19. Phinney K.W., Ihara T., and Sander L.C. J. Chromatogr. A 1077 (2005) 90-97
20. Sharpless K.E., Anderson D.L., Betz J.M., Butler T.A., Capar S.G., Chen J., Fraser C.A., Gardner G., Gay M.L., Howell D.W., Ihara T., Khan M.A., Lam J.W., Long S.E., McCooeye M., Mackey E.A., Mindak W.R., Mitvalsky S., Murphy K.E., NguyenPho A., Phinney K.W., Porter B.J., Sander L.C., Satterfield M.B., Scriver C., Sturgeon R., Brown Thomas J., Vocke R.D., Wise S.A., Wood L.J., Yang L., Yen J.H., and Ziobro G.C. J. AOAC Int. 89 (2006) 1483-1495
21. International Conference on Harmonization of Technical Requirements for the Registration of Pharmaceuticals for Human Use (ICH), Guideline Q2(R1)-Validation of Analytical Procedures: Text and Methodology, ICH Secretariat, c/o IFPMA, Geneva, Switzerland, 2005, pp. 1-13.
22. Bell D.S., Cramer H.M., and Jones A.D. J. Chromatogr. A 1095 (2005) 113-118
23. Martino E., Ramaiola I., Urbano M., Bracco F., and Collina S. J. Chromatogr. A 1125 (2006) 147-151