메뉴 건너뛰기




Volumn , Issue , 2006, Pages 321-351

Nuclear Magnetic Resonance Spectroscopy in Analysis of Chemicals Related to the Chemical Weapons Convention

Author keywords

Acquired NMR data; Automatic sample changer (ASC); Chemical shift references; Data Systems; Free induction decay (FID); NMR tubes; Nuclear magnetic resonance (NMR) spectroscopy; Probe heads; Quality control

Indexed keywords

CHEMICAL ANALYSIS; CHEMICAL SHIFT; INDICATORS (CHEMICAL); MAGNETIC HEADS; NUCLEAR WEAPONS; QUALITY CONTROL;

EID: 84889366625     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1002/0470012285.ch13     Document Type: Chapter
Times cited : (2)

References (50)
  • 7
    • 84889431544 scopus 로고
    • (1990); F.2 Testing of Procedures on Simulated Industry Samples (1991); F.3 Testing of Procedures on Simulated Military Facility Samples (1992); F.4 Validating of Procedures for Water and Soil Samples (1993); F. International Interlaboratory Comparison (Round-Robin) Test for the Verification of Chemical Disarmament. Methodology and Instrumentation for Sampling and Analysis in the Verification of Chemical Disarmament, The Ministry for Foreign Affairs of Finland, Helsinki
    • Rautio, M. (Ed.), F.1 Testing of Existing Procedures (1990); F.2 Testing of Procedures on Simulated Industry Samples (1991); F.3 Testing of Procedures on Simulated Military Facility Samples (1992); F.4 Validating of Procedures for Water and Soil Samples (1993); F. International Interlaboratory Comparison (Round-Robin) Test for the Verification of Chemical Disarmament. Methodology and Instrumentation for Sampling and Analysis in the Verification of Chemical Disarmament, The Ministry for Foreign Affairs of Finland, Helsinki, 1990-1993.
    • (1990) F.1 Testing of Existing Procedures
    • Rautio, M.1
  • 10
    • 0030180877 scopus 로고    scopus 로고
    • Detection of trace amounts of chemical warfare agents and related compounds in rubber, paint, and soil samples by 1H and 31P NMR spectroscopy
    • Mesilaakso, M. and Tolppa, E.-L., Detection of trace amounts of chemical warfare agents and related compounds in rubber, paint, and soil samples by 1H and 31P NMR spectroscopy, Anal. Chem., 68, 2313-2318 (1996).
    • (1996) Anal. Chem. , vol.68 , pp. 2313-2318
    • Mesilaakso, M.1    Tolppa, E.-L.2
  • 11
    • 0008029312 scopus 로고    scopus 로고
    • Analysis of the 1H and 13C NMR spectral parameters of the tear gases α-chloroacetophenone, dibenz[b,f][1,4]oxazepine, and 2-chlorobenzylidene malononitrile
    • Mesilaakso, M., Analysis of the 1H and 13C NMR spectral parameters of the tear gases α-chloroacetophenone, dibenz[b,f][1,4]oxazepine, and 2-chlorobenzylidene malononitrile, Magn. Reson. Chem., 34, 989-994 (1996).
    • (1996) Magn. Reson. Chem. , vol.34 , pp. 989-994
    • Mesilaakso, M.1
  • 12
    • 0031014562 scopus 로고    scopus 로고
    • Application of NMR spectroscopy to environmental analysis: detection of trace amounts of chemical warfare agents and related compounds in organic extract, water, and sand
    • Mesilaakso, M., Application of NMR spectroscopy to environmental analysis: detection of trace amounts of chemical warfare agents and related compounds in organic extract, water, and sand, Environ. Sci. Technol., 31, 518-522 (1997).
    • (1997) Environ. Sci. Technol. , vol.31 , pp. 518-522
    • Mesilaakso, M.1
  • 13
    • 0042325603 scopus 로고    scopus 로고
    • Application of two-dimensional 1H-31P inverse NMR spectroscopy to the detection of trace amounts of organophosphorus compounds related to the chemical weapons convention
    • Albaret, C., Loeillet, D., Augé, P., Fortier, P.-L., Application of two-dimensional 1H-31P inverse NMR spectroscopy to the detection of trace amounts of organophosphorus compounds related to the chemical weapons convention, Anal. Chem., 69, 2694-2700 (1997).
    • (1997) Anal. Chem. , vol.69 , pp. 2694-2700
    • Albaret, C.1    Loeillet, D.2    Augé, P.3    Fortier, P.-L.4
  • 16
    • 84948811811 scopus 로고
    • Convention on the Prohibition of the Development, Production, Stockpiling and Use of Chemical Weapons and on their Destruction, Signed in January. Printed and distributed by the OPCW/PTS
    • Convention on the Prohibition of the Development, Production, Stockpiling and Use of Chemical Weapons and on their Destruction, Signed in January 1993. Printed and distributed by the OPCW/PTS.
    • (1993)
  • 17
    • 20444382521 scopus 로고
    • Analysis of Two Chemical Weapons Samples from the Iran-Iraq War
    • April
    • Andersson, G., Analysis of Two Chemical Weapons Samples from the Iran-Iraq War, NBC Defence & Technology International, 62-65, April 1986.
    • (1986) NBC Defence & Technology International , pp. 62-65
    • Andersson, G.1
  • 20
    • 0003507907 scopus 로고
    • Two-dimensional NMR Spectroscopy
    • VCH Publishers, New York, Sections 2.4.2, 2.4.5, 2.7.10, 2.8.12
    • Croasmun, W.R. and Carlson, R.M.K. (Eds.), Two-dimensional NMR Spectroscopy. Applications for Chemists and Biochemists, VCH Publishers, New York, Sections 2.4.2, 2.4.5, 2.7.10, 2.8.12, 1994.
    • (1994) Applications for Chemists and Biochemists
    • Croasmun, W.R.1    Carlson, R.M.K.2
  • 21
    • 0001671162 scopus 로고
    • 31P NMR reference standards for aqueous samples
    • Batley, M. and Redmond, J.W., 31P NMR reference standards for aqueous samples, J. Magn. Reson., 49, 172-174 (1982).
    • (1982) J. Magn. Reson. , vol.49 , pp. 172-174
    • Batley, M.1    Redmond, J.W.2
  • 28
    • 0011104033 scopus 로고    scopus 로고
    • Sample Preparation for Analysis of Chemicals Related to the Chemical Weapons Convention
    • Meyers, R.A. (Ed.), John Wiley & Sons, Ltd, Chichester
    • Kuitunen, M.K., Sample Preparation for Analysis of Chemicals Related to the Chemical Weapons Convention, in Encyclopedia of Analytical Chemistry: Instrumentation and Applications, Meyers, R.A. (Ed.), John Wiley & Sons, Ltd, Chichester, 1055-1071, 2000 (ISBN 0-471-97670-9).
    • (2000) Encyclopedia of Analytical Chemistry: Instrumentation and Applications , pp. 1055-1071
    • Kuitunen, M.K.1
  • 29
    • 84889354888 scopus 로고    scopus 로고
    • NMR Spectroscopy in Analysis of Chemicals Related to the Chemical Weapons Convention
    • R.A. (Ed.), John Wiley & Sons, Ltd, Chichester
    • Mesilaakso, M., and Niederhauser, A., NMR Spectroscopy in Analysis of Chemicals Related to the Chemical Weapons Convention, in Encyclopedia of Analytical Chemistry: Instrumentation and Applications; Meyers, R.A. (Ed.), John Wiley & Sons, Ltd, Chichester, 1026-1055, 2000 (ISBN 0-471-97670-9).
    • (2000) Encyclopedia of Analytical Chemistry: Instrumentation and Applications; Meyers , pp. 1026-1055
    • Mesilaakso, M.1    Niederhauser, A.2
  • 35
    • 0004099399 scopus 로고
    • Plenum Press, New York
    • Mason, J. (Ed.), Multinuclear NMR, Plenum Press, New York, 1987.
    • (1987) Multinuclear NMR
    • Mason, J.1
  • 37
    • 0036138810 scopus 로고    scopus 로고
    • Quantitative NMR spectroscopy using coaxial inserts containing a reference standard: purity determinations for military nerve agents
    • Henderson, T.J., Quantitative NMR spectroscopy using coaxial inserts containing a reference standard: purity determinations for military nerve agents, Anal. Chem., 74, 191-198 (2002).
    • (2002) Anal. Chem. , vol.74 , pp. 191-198
    • Henderson, T.J.1
  • 38
    • 0345866727 scopus 로고    scopus 로고
    • Application of nonselective 1-D 1H-31P inverse NMR spectroscopy to the screening of solutions for the presence of organophosphorus compounds related to the chemical weapons convention
    • Meier, U.C., Application of nonselective 1-D 1H-31P inverse NMR spectroscopy to the screening of solutions for the presence of organophosphorus compounds related to the chemical weapons convention, Anal. Chem., 76, 392-398 (2004).
    • (2004) Anal. Chem. , vol.76 , pp. 392-398
    • Meier, U.C.1
  • 39
    • 0031141415 scopus 로고    scopus 로고
    • Analysis of 1H and 13C NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine. Identification of the compounds through reference to simulated spectra
    • Mesilaakso, M., Tolppa, E.-L. and Nousiainen, P., Analysis of 1H and 13C NMR spectral parameters of diphenylchloroarsine, diphenylcyanoarsine, and 10-chloro-5,10-dihydrophenarsazine. Identification of the compounds through reference to simulated spectra, Appl. Spectrosc., 51, 733-737 (1997).
    • (1997) Appl. Spectrosc. , vol.51 , pp. 733-737
    • Mesilaakso, M.1    Tolppa, E.-L.2    Nousiainen, P.3
  • 41
    • 0008169956 scopus 로고
    • Study of the stereochemistry, relaxation mechanisms, and internal motions of natural products utilizing proton relaxation parameters: solution and crystal structures of saxitoxin
    • Niccolai, N., Schnoes, H.K. and Gibbons, W.A. Study of the stereochemistry, relaxation mechanisms, and internal motions of natural products utilizing proton relaxation parameters: solution and crystal structures of saxitoxin, J. Am. Chem. Soc., 102, 1513-1517 (1980).
    • (1980) J. Am. Chem. Soc. , vol.102 , pp. 1513-1517
    • Niccolai, N.1    Schnoes, H.K.2    Gibbons, W.A.3
  • 42
    • 0019415171 scopus 로고
    • Structure of saxitoxin in solutions and stereochemistry of dihydrosaxitoxins
    • Shimizu, Y., Hsu, C.-P. and Genenah, A., Structure of saxitoxin in solutions and stereochemistry of dihydrosaxitoxins, J. Am. Chem. Soc., 103, 605-609 (1981).
    • (1981) J. Am. Chem. Soc. , vol.103 , pp. 605-609
    • Shimizu, Y.1    Hsu, C.-P.2    Genenah, A.3
  • 43
    • 84948811813 scopus 로고    scopus 로고
    • Work Instruction for the Evaluation of the Results of OPCW Proficiency Tests, QDOC/LAB/WI/PT3, OPCW Secretariat, The Hague, 24 March
    • Work Instruction for the Evaluation of the Results of OPCW Proficiency Tests, QDOC/LAB/WI/PT3, OPCW Secretariat, The Hague, 24 March 2004.
    • (2004)
  • 44
    • 84889461271 scopus 로고
    • E.1. Verification Database. Methodology and Instrumentation for Sampling and Analysis in the Verification of Chemical Disarmament, The Ministry for Foreign Affairs of Finland, Helsinki
    • Miettinen, J.K. (Ed.), Computer-Aided Techniques for the Verification of Chemical Disarmament. E.1. Verification Database. Methodology and Instrumentation for Sampling and Analysis in the Verification of Chemical Disarmament, The Ministry for Foreign Affairs of Finland, Helsinki, 1988.
    • (1988) Computer-Aided Techniques for the Verification of Chemical Disarmament
    • Miettinen, J.K.1
  • 45
    • 0031571894 scopus 로고    scopus 로고
    • Application of on-line HPLC-1H NMR to environmental samples: analysis of groundwater near former ammunition plants
    • Godejohann, M., Preiss, A., Mügge, C. and Wünsch, G, Application of on-line HPLC-1H NMR to environmental samples: analysis of groundwater near former ammunition plants, Anal. Chem., 69, 3832-3837 (1997).
    • (1997) Anal. Chem. , vol.69 , pp. 3832-3837
    • Godejohann, M.1    Preiss, A.2    Mügge, C.3    Wünsch, G.4
  • 46
    • 0142138604 scopus 로고    scopus 로고
    • Advantages and disadvantages of nuclear magnetic resonance spectroscopy as a hyphenated technique
    • Elipe, M.V.S., Advantages and disadvantages of nuclear magnetic resonance spectroscopy as a hyphenated technique, Anal. Chim. Acta., 497, 1-25 (2003).
    • (2003) Anal. Chim. Acta. , vol.497 , pp. 1-25
    • Elipe, M.V.S.1
  • 47
    • 0032869207 scopus 로고    scopus 로고
    • Liquid chromatography-nuclear magnetic resonance spectroscopy
    • Albert, K., Liquid chromatography-nuclear magnetic resonance spectroscopy, J. Chromatogr., A856, 199-211 (1999).
    • (1999) J. Chromatogr. , vol.A856 , pp. 199-211
    • Albert, K.1
  • 48
    • 0038439687 scopus 로고    scopus 로고
    • Liquid chromatography with ultraviolet absorbance-mass spectrometric detection and with nuclear magnetic resonance spectroscopy: a powerful combination for the on-line structural investigation of plant metabolites
    • Wolfender, J.-L., Ndjoko, K. and Hostettmann, K., Liquid chromatography with ultraviolet absorbance-mass spectrometric detection and with nuclear magnetic resonance spectroscopy: a powerful combination for the on-line structural investigation of plant metabolites, J. Chromatogr., A1000, 437-455 (2003).
    • (2003) J. Chromatogr. , vol.A1000 , pp. 437-455
    • Wolfender, J.-L.1    Ndjoko, K.2    Hostettmann, K.3
  • 49
    • 84889388945 scopus 로고    scopus 로고
    • TheWorld's First 800MHz Spectrometer installed in a customer's laboratory
    • TheWorld's First 800MHz Spectrometer installed in a customer's laboratory, Bruker Rep., 142, 28-29 (1996).
    • (1996) Bruker Rep. , vol.142 , pp. 28-29
  • 50
    • 84948811814 scopus 로고    scopus 로고
    • 1H Nano.nmr Probe for 500MHz NMR Systems, Varian brochure 814040-001 MAG-7029/874 5/93
    • 1H Nano.nmr Probe for 500MHz NMR Systems, Varian brochure 814040-001 MAG-7029/874 5/93.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.