Semiautomated solid-phase extraction followed by derivatisation and gas chromatography-mass spectrometry for determination of perfluoroalkyl acids in water

Journal of Chromatography A

Volumn 1318, Issue , 2013, Pages 65-71

  Jurado Sánchez, Beatriz ^a   Ballesteros, Evaristo ^b   Gallego, Mercedes ^a  

^a UNIVERSITY OF CÓRDOBA   (Spain)

^b UNIVERSITY OF JAÉN   (Spain)

Author keywords

Derivatisation; Gas chromatography mass spectrometry; Perfluoroalkyl acids; Solid phase extraction; Water

Indexed keywords

AUTOMATIC SOLID-PHASE EXTRACTION; DERIVATISATION; DETECTION AND QUANTIFICATION LIMIT; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PERFLUOROALKYL ACIDS; PERFLUOROALKYL CARBOXYLIC ACIDS; PERFLUOROOCTANE SULFONIC ACIDS; SOLID-PHASE EXTRACTION;

DRUG PRODUCTS; FLOW RATE; GAS CHROMATOGRAPHY; PHASE SEPARATION; SORPTION; WATER;

EXTRACTION;

CHEMICAL COMPOUND; CHLOROFORMIC ACID ETHYL ESTER; DRINKING WATER; ISOBUTANOL; PERFLUOROALKYL ACID; PERFLUORODECANOIC ACID; PERFLUOROHEPTANOIC ACID; PERFLUOROOCTANESULFONIC ACID; PERFLUOROOCTANOIC ACID; PYRIDINE; UNCLASSIFIED DRUG;

ANION EXCHANGE; ARTICLE; AUTOMATION; CATALYST; DERIVATIZATION; ELUTION; ESTERIFICATION; FLOW RATE; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MOISTURE; PARTICLE SIZE; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; REVERSED PHASE LIQUID CHROMATOGRAPHY; SOLID PHASE EXTRACTION; WATER ANALYSIS; WATER TREATMENT;

ALKANESULFONIC ACIDS; DECANOIC ACIDS; FLUOROCARBONS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; SOLID PHASE EXTRACTION; WATER POLLUTANTS, CHEMICAL;

EID: 84887176777     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.10.034     Document Type: Article

References (45)

1. Lindstrom A.B., Strynar M.J., Libelo E.L. Environ. Sci. Technol. 2011, 45:7954.
2. Higgins C.P., Field J.A., Criddle C.S., Luthy R.G. Environ. Sci. Technol. 2005, 39:3946.
3. Hansen K.J., Johnson H.O., Eldridge J.S., Butenhoff J.L., Dick L.A. Environ. Sci. Technol. 2002, 36:1681.
4. Schultz M.M., Barofsky D.F., Field J.A. Environ. Sci. Technol. 2004, 38:1828.
5. Lau C., Anitole K., Hodes C., Lai D., Pfahles-Hutchens A. J. Seed. Toxicol. Sci. 2007, 99:366.
6. Directive 2006/122/EC of the European Parliament and of the Council Official J. Eur. Commun. 2006, L 372:32.
7. EPA (Environmental Protection Agency), 2006, PFOA Stewardship Program, available at (accessed 27.06.13). http://www.epa.gov/oppt/pfoa/pubs/stewardship/index.html.
8. The new POPs under the Stockholm Convention, available at (accessed 27.06.13). http://chm.pops.int/Programmes/New%20POPs/The%209%20new%20POPs/tabid/672/language/en-US/Default.aspx.
9. Directive of the European Parliament and of the Council amending directives 2000/60/EC and 2008/105/EC as regards priority substances in the field of water policy, available at (accessed 27.06.13). http://ec.europa.eu/environment/water/water-dangersub/pdf/com_2011_876.pdf.
10. EPA, 2009, Provisional Health Advisory for perfluorooctanoic acid (PFOA) and perfluorooctane sulfonate (PFOS), available at (accessed 27.06.13). http://water.epa.gov/action/advisories/drinking/upload/2009_01_15_criteria_drinking_pha-PFOA_PFOS.pdf.
11. European Food Safety Authority EFSA J. 2008, 653:1.
12. Mak Y.L., Taniyasu S., Yeung L.W.Y., Lu G., Jin L., Yang Y., Lam P.K.S., Kannan K., Yamashita N. Environ. Sci. Technol. 2009, 43:4824.
13. Ullah S., Alsberg T., Berger U. J. Chromatogr. A 2011, 1218:6388.
14. Eschauzier C., Beerendonk E., Scholte-Veenendaal P., De Voogt P. Environ. Sci. Technol. 2012, 46:1708.
15. Fromme H., Tittlemier S.A., Völkel W., Wilhelm M., Twardella D. Int. J. Hyg. Environ. Health 2009, 212:239.
16. Noorlander C.W., van Leeuwen S.P.J., Biesebeek J.D., Mengelers M.J.B., Zeilmaker M.J. J. Agric. Food Chem. 2011, 59:7496.
17. Llorca M., Farré M., Picó Y., Müller J., Knepper T.P., Barceló D. Sci. Total Environ. 2012, 431:139.
18. EPA Method 537 Determination of selected perfluorinated alkyl acids in drinking water by solid-phase extraction and liquid chromatography/tandem mass spectrometry (LC/MS/MS), EPA/600/R-08/092 2009, National Exposure Research Laboratory, Office of Research and Development, US Environmental Protection Agency, Cincinnati, OH.
19. Furdui V.I., Crozier P.W., Reiner E.J., Mabury S.A. Chemosphere 2008, 73:S24.
20. Luque N., Ballesteros-Gómez A., Van Leeuwen S., Rubio S. J. Chromatogr. A 2010, 1217:3774.
21. Marchetti N., Caciolli L., Laganà A., Gasparrini F., Pasti L., Dondi F., Cavazzini A. Anal. Chem. 2012, 84:7138.
22. Onghena M., Moliner-Martínez Y., Picó Y., Campíns-Falcó P., Barceló D. J. Chromatogr. A 2012, 1244:88.
23. Luque N., Van Leeuwen A., Ballesteros-Gómez S., Rubio S. J. Chromatogr. A 2012, 1235:84.
24. Qiu J., Wu C., Fang Y., Yang C., Li X., Piao X., Li D. J. Chromatogr. A 2012, 1235:132.
25. Alzaga R., Bayona J.M. J. Chromatogr. A 2004, 1042:155.
26. Dufková V., Cabala R., Sevcík V. Chemosphere 2012, 87:463.
27. Liu W.L., Ko Y.C., Hwang B.H., Li Z.G., Yang T.C.C., Lee M.R. Anal. Chim. Acta 2012, 726:28.
28. Monteleone M., Naccarato A., Sindona G., Tagarelli A. J. Chromatogr. A 2012, 1251:160.
29. Moody C.A., Hebert G.N., Strauss S.H., Field J.A. J. Environ. Monitor. 2003, 5:341.
30. Scott B.F., Moody C.A., Spencer C., Small J.M., Muir D.C., Mabury S.A. Environ. Sci. Technol. 2006, 40:6405.
31. Dufková V., Cabala R., Maradová D., Stícha M. J. Chromatogr. A 2009, 1216:8659.
32. Chang Y.C., Chen W.L., Bai F.Y., Chen P.C., Wang G.S., Chen C.Y. Anal. Bioanal. Chem. 2012, 402:1315.
33. Quiñones O., Snyder S.A. Environ. Sci. Technol. 2009, 43:9089.
34. Zhao X., Li J., Shi Y., Cai Y., Mou S., Jiang G. J. Chromatogr. A 2007, 1154:52.
35. Taniyasu S., Kannan K., So M.K., Gulkowska A., Sinclair E., Okazawa T., Yamashit N. J. Chromatogr. A 2005, 1093:89.
36. Takino M., Daishima S., Nakahara T. Rapid Commun. Mass Spectrom. 2003, 17:383.
37. Gosetti F., Chiuminatto U., Zampieri D., Mazzucco E., Robotti E., Calabrese G., Gennaro M.C., Marengo E. J. Chromatogr. A 2010, 1217:7864.
38. Kuklenyik Z., Reich J.A., Tully J.S., Needham L.L., Calafat A.M. Environ. Sci. Technol. 2004, 38:3698.
39. Angelino S., Maurino V., Minero C., Pelizzetti E., Vincenti M. J. Chromatogr. A 1998, 793:307.
40. Armitage J.M., Macleod M., Cousins I.T. Environ. Sci. Technol. 2009, 43:5830.
41. Goss K.U. Environ. Sci. Technol. 2008, 42:456.
42. Cheng J., Psillakis E., Hoffmann M.R., Colussi A.J. J. Phys. Chem. A 2009, 113:8152.
43. Washburn S.T., Bingman T.S., Braithwaite S.K., Buck R.C., Buxton L.W., Clewell H.J., Haroun L.A., Kester J.E., Rickard R.W., Shipp A.M. Environ. Sci. Technol. 2005, 39:3904.
44. Liu X., Krebs K., Guo Z., Roache N. J. Chromatogr. A 2009, 1216:3910.
45. Fiedler S., Pfister G., Schramm K.W. Toxicol. Environ. Chem. 2010, 92:1801.