A rapid and sensitive assay of perfluorocarboxylic acids in aqueous matrices by headspace solid phase microextraction-gas chromatography-triple quadrupole mass spectrometry

Journal of Chromatography A

Volumn 1251, Issue , 2012, Pages 160-168

  Monteleone, Marcello ^a   Naccarato, Attilio ^a   Sindona, Giovanni ^a   Tagarelli, Antonio ^a  

^a UNIVERSITY OF CALABRIA   (Italy)

Author keywords

Experimental design; Gas chromatography; Perfluorocarboxylic acids; Solid phase microextraction; Tandem mass spectrometry

Indexed keywords

ANALYTICAL APPROACH; ANALYTICAL PARAMETERS; AQUEOUS MATRICES; CENTRAL COMPOSITE DESIGNS; DERIVATIZATIONS; EXTRACTION TIME; HEADSPACES; NEGATIVE CHEMICAL IONIZATION MODE; OPTIMUM WORKING CONDITIONS; PERFLUOROCARBOXYLIC ACID; QUADRUPOLE MASS SPECTROMETRY; REAGENT GAS; ROOM TEMPERATURE; SAMPLE VOLUME; SENSITIVE ASSAY; SENSITIVE METHOD; SOLID-PHASE; SOLID-PHASE MICROEXTRACTION; TANDEM MASS SPECTROMETRY;

CARBOXYLATION; DESIGN OF EXPERIMENTS; EXTRACTION; IONIZATION OF GASES; MASS SPECTROMETRY; SODIUM CHLORIDE;

GAS CHROMATOGRAPHY;

AMMONIA; CARBOXYLIC ACID; FORMIC ACID; PERFLUOROCARBOXYLIC ACID; PROPANOL; PROPYLCHLOROFORMATE; SODIUM CHLORIDE; UNCLASSIFIED DRUG;

ACCURACY; ANALYTICAL PARAMETERS; AQUEOUS SOLUTION; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL INTERACTION; DERIVATIZATION; FIBER; GAS CHROMATOGRAPHY; HEADSPACE SOLID PHASE MICROEXTRACTION; IONIZATION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUADRUPOLE MASS SPECTROMETRY; REFERENCE VALUE; ROOM TEMPERATURE; SENSITIVITY ANALYSIS; SOLID PHASE MICROEXTRACTION; TIME; TRIPLE QUADRUPOLE MASS SPECTROMETRY;

FLUOROCARBONS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; ITALY; LIMIT OF DETECTION; REPRODUCIBILITY OF RESULTS; RIVERS; SENSITIVITY AND SPECIFICITY; SODIUM CHLORIDE; SOLID PHASE MICROEXTRACTION; TEMPERATURE; WATER POLLUTANTS, CHEMICAL;

EID: 84864033444     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2012.06.033     Document Type: Article

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