Simultaneous analysis of endosulfan, chlorpyrifos, and their metabolites in natural soil and water samples using gas chromatography-tandem mass spectrometry

Environmental Monitoring and Assessment

Volumn 185, Issue 10, 2013, Pages 8451-8463

  Tiwari, Manoj K ^a   Guha, Saumyen ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY KANPUR   (India)

Author keywords

endosulfan; endosulfan; Chlorpyrifos; Chlorpyrifos oxon; Endodiol; Endosulfan ether; Endosulfan lactone; Endosulfan sulfate; GC MS MS; Quantification; Soil and water

Indexed keywords

CHLORPYRIFOS; CHLORPYRIFOS-OXON; ENDODIOL; ENDOSULFAN LACTONE; ENDOSULFAN SULFATE; ENDOSULFANS; GC-MS/MS; QUANTIFICATION; SOIL AND WATER;

BIOLOGICAL WATER TREATMENT; BIOMOLECULES; COBALT COMPOUNDS; ETHERS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLITES; OPTIMIZATION; SOIL POLLUTION; SOILS;

INSECTICIDES;

CHLORPYRIFOS; CHLORPYRIFOS OXON; ENDODIOL; ENDOSULFAN; ENDOSULFAN ETHER; PESTICIDE RESIDUE; SOIL ORGANIC MATTER; UNCLASSIFIED DRUG;

ACCURACY ASSESSMENT; BIOREACTOR; CHLORPYRIFOS; ENDOSULFAN; EXPERIMENTAL STUDY; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLITE; SOIL ORGANIC MATTER;

ACCURACY; AGRICULTURAL LAND; AGRICULTURAL SLURRY; ARTICLE; BIOREACTOR; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; QUANTITATIVE ANALYSIS; SENSITIVITY AND SPECIFICITY; SOIL ANALYSIS; WATER ANALYSIS;

CHLORPYRIFOS; ENDOSULFAN; ENVIRONMENTAL MONITORING; FRESH WATER; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LIMIT OF DETECTION; MODELS, CHEMICAL; PESTICIDES; SOIL; SOIL POLLUTANTS; TANDEM MASS SPECTROMETRY; WATER POLLUTANTS, CHEMICAL;

EID: 84884357594     PISSN: 01676369     EISSN: 15732959     Source Type: Journal    
DOI: 10.1007/s10661-013-3186-3     Document Type: Article

References (38)

1. Alder, L.; Greulich, K.; Kempe, G.; & Vieth, B. (2006). Residue analysis of 500 high priority pesticides: Better by GC-MS or LC-MS/MS? Mass Spectrometry Reviews, 25(6), 838-865.
2. Armbruster, D. A.; & Pry, T. (2008). Limit of blank, limit of detection and limit of quantitation. Clinical Biochemistry Reviews, 29, 49-52.
3. Arrebola, F. J.; Martínez Vidal, J. L.; & Fernández- Gutiérrez, A. (2001). Analysis of endosulfan and its metabolites in human serum using gas chromatography-tandem mass spectrometry. Journal of Chromatographic Science, 39(5), 177-182.
4. Béguin, S.; Jadas-Hécart, A.; Tabet, J. C.; & Communal, P. Y. (2006). Protocols for optimizing MS/MS parameters with an ion-trap GC-MS instrument. Journal of Mass Spectrometry, 41, 1304-1314.
5. Bempah, C.; & Donkor, A. (2011). Pesticide residues in fruits at the market level in Accra Metropolis, Ghana, a preliminary study. Environmental Monitoring and Assessment, 175(1-4), 551-561.
6. Berthouex, P. M.; & Brown, L. C. (2002). Statistics for environmental engineers. New York: Lewis.
7. Castro, J.; Pérez, R. A.; Miguel, E.; Sánchez-Brunete, C.; & Tadeo, J. L. (2002). Analysis of endosulfan isomers and endosulfan sulfate in air and tomato leaves by gas chromatography with electron-capture detection and confirmation by gas chromatography-mass spectrometry. Journal of Chromatography. A, 947, 119-127.
8. Cho, S. K.; Abd El-Aty, A. M.; Jeon, H. R.; Choi, J. H.; Shin, H. C.; & Shim, J. H. (2008). Comparison of different extraction methods for the simultaneous determination of pesticide residues in kiwi fruit using gas chromatography-mass spectrometry. Biomedical Chromatography, 22, 727-735.
9. Corley, J. (2003). Best practices in establishing detection and quantification limits for pesticide residues in foods (vol. 1, Handbook of residue analytical methods for agrochemicals). Chichester: Wiley.
10. Duirk, S. E.; & Collette, T. W. (2006). Degradation of chlorpyrifos in aqueous chlorine solutions: Pathways, kinetics, and modeling. Environmental Science and Technology, 40(2), 546-551.
11. Fernández Moreno, J. L.; Garrido Frenich, A.; Plaza Bolaños, P.; & Martínez Vidal, J. L. (2008). Multiresidue method for the analysis of more than 140 pesticide residues in fruits and vegetables by gas chromatography coupled to triple quadrupole mass spectrometry. Journal of Mass Spectrometry, 43, 1235-1254.
12. Fialkov, A. B.; Steiner, U.; Lehotay, S. J.; & Amirav, A. (2007). Sensitivity and noise in GC-MS: Achieving low limits of detection for difficult analytes. International Journal of Mass Spectrometry, 260, 31-48.
13. Geerdink, R. B.; Niessen, W. M. A.; & Brinkman, U. A. T. (2002). Trace-level determination of pesticides in water by means of liquid and gas chromatography. Journal of Chromatography. A, 970, 65-93.
14. Khodadoust, A. P.; Suidan, M. T.; Acheson, C. M.; & Brenner, R. C. (1999). Solvent extraction of pentachlorophenol from contaminated soils using water-ethanol mixtures. Chemosphere, 38(11), 2681-2693.
15. Leung, A. M.; McDonough, D. M.; & West, C. D. (1998). Determination of endosulfans in soil/sediment samples from Point Mugu, Oxnard, CA using capillary gas chromatography/mass selective detection (GC/MSD). Environmental Monitoring and Assessment, 50(1), 85-94.
16. Lian, Y.-J.; Pang, G.-F.; Shu, H.-R.; Fan, C.-L.; Liu, Y.-M.; Feng, J.; et al. (2010). Simultaneous determination of 346 multiresidue pesticides in grapes by PSA-MSPD and GC-MS-SIM. Journal of Agricultural and Food Chemistry, 58(17), 9428-9453.
17. Lin, C. H.; Lerch, R. N.; Garrett, H. E.; & George, M. F. (2007). Improved GC-MS/MS method for determination of atrazine and its chlorinated metabolites in forage plants - Laboratory and field experiments. Communications in Soil Science and Plant Analysis, 38, 1753-1773.
18. Lu, J. (2010). Multipesticide residue assessment of agricultural soil and water in major farming areas in Benguet, Philippines. Archives of Environmental Contamination and Toxicology, 59(2), 175-181.
19. Mandalakis, M.; Tsapakis, M.; & Stephanou, E. G. (2001). Optimization and application of high-resolution gas chromatography with ion trap tandem mass spectrometry to the determination of polychlorinated biphenyls in atmospheric aerosols. Journal of Chromatography. A, 925, 183-196.
20. March, R. E. (1997). An introduction to quadrupole ion trap mass spectrometry. Journal of Mass Spectrometry, 32, 351-369.
21. Pinho, G. P.; Neves, A. A.; Queiroz, M. E. L. R.; & Silvério, F. O. (2010). Pesticide determination in tomatoes by solid-liquid extraction with purification at low temperature and gas chromatography. Food Chemistry, 121, 251-256.
22. Pyle, S. M.; Marcus, A. B.; & Robertson, G. L. (1998). ECD-dual-column pesticide method verification by ion trap GC/MS and GC/MS/MS. Environmental Science and Technology, 32, 3213-3217.
23. Racke, K. D. (1993). Environmental fate of chlorpyrifos. Reviews of Environmental Contamination and Toxicology, 131, 1-150.
24. Raina, R. (2011). Chemical analysis of pesticides using GC/MS, GC/MS/MS, and LC/MS/MS. In M. Stoytcheva (Ed.), Pesticides - Strategies for pesticides analysis: InTech, Rijeka.
25. Raina, R.; & Hall, P. (2008). Comparison of gas chromatography-mass spectrometry and gas chromatography-tandem mass spectrometry with electron ionization and negative-ion chemical ionization for analyses of pesticides at trace levels in atmospheric samples. Analytical Chemistry Insights, 3, 111-125.
26. Ramesh, A.; & Ravi, P. E. (2002). A rapid and sensitive analytical method for the quantification of residues of endosulfan in blood. Journal of Environmental Monitoring, 4(2), 190-193.
27. Rashid, A.; Nawaz, S.; Barker, H.; Ahmad, I.; & Ashraf, M. (2010). Development of a simple extraction and clean-up procedure for determination of organochlorine pesticides in soil using gas chromatography-tandem mass spectrometry. Journal of Chromatography. A, 1217, 2933-2939.
28. Sauret, N.; Millet, M.; Herckes, P.; Mirabel, P.; & Wortham, H. (2000). Analytical method using gas chromatography and ion trap tandem mass spectrometry for the determination of S-triazines and their metabolites in the atmosphere. Environmental Pollution, 110, 243-252.
29. Shunthirasingham, C.; Oyiliagu, C. E.; Cao, X.; Gouin, T.; Wania, F.; Lee, S.; et al. (2010). Spatial and temporal pattern of pesticides in the global atmosphere. Journal of Environmental Monitoring, 12(9), 1650-1657.
30. Singh, S. B.; Mukherjee, I.; Maisnam, J.; Kumar, P.; Gopal, M.; & Kulshrestha, G. (2009). Determination of pesticide residues in integrated pest management and nonintegrated pest management samples of apple (Malus pumila Mill.). Journal of Agricultural and Food Chemistry, 57, 11277-11283.
31. Sinha, S. N. (2010). Effect of dissociation energy: Signal to noise ratio on ion formation and sensitivity of analytical method for quantification and confirmation of triazofos in blood samples using gas chromatography-mass spectrometer (GC-MS/MS). International Journal of Mass Spectrometry, 296(1-3), 47-52.
32. Sinha, S. N.; Bhatnagar, V. K.; Doctor, P.; Tuteja, G. S.; Agnihotri, N. P.; & Kalra, R. L. (2011). A novel method for pesticide analysis in refined sugar samples using a gas chromatography-mass spectrometer (GC-MS/MS) and simple solvent extraction method. Food Chemistry, 126, 379-386.
33. Sutherland, T. D.; Horne, I.; Lacey, M. J.; Harcourt, R. L.; Russell, R. J.; & Oakeshott, J. G. (2000). Enrichment of an endosulfan-degrading mixed bacterial culture. Applied and Environmental Microbiology, 66, 2822-2828.
34. Sutherland, T. D.; Horne, I.; Weir, K. M.; Russell, R. J.; & Oakeshott, J. G. (2004). Toxicity and residues of endosulfan isomers. Reviews of Environmental Contamination and Toxicology, 183, 99-113.
35. Tiwari, M. K.; & Guha, S. (2012). Role of soil organic matter on the sorption and cosorption of endosulfan and chlorpyrifos on agricultural soils. Journal of Environmental Engineering ASCE, 138(4), 426-435.
36. Weber, J.; Halsall, C. J.; Muir, D.; Teixeira, C.; Small, J.; Solomon, K.; et al. (2010). Endosulfan, a global pesticide: A review of its fate in the environment and occurrence in the Arctic. Science of the Total Environment, 408, 2966-2984.
37. Wong, J. W.; Zhang, K.; Tech, K.; Hayward, D. G.; Krynitsky, A. J.; Cassias, I.; et al. (2010). Multiresidue pesticide analysis of ginseng powders using acetonitrile- or acetone-based extraction, solid-phase extraction cleanup, and gas chromatography-mass spectrometry/selective ion monitoring (GC-MS/SIM) or -tandem mass spectrometry (GC-MS/MS). Journal of Agricultural and Food Chemistry, 58(10), 5884-5896.
38. Yang, X.; Wang, J.; Xu, D. C.; Qiu, J. W.; Ma, Y.; & Cui, J. (2011). Simultaneous determination of 69 pesticide residues in coffee by gas chromatography-mass spectrometry. Food Analytical Method, 4(2), 186-195.