Quality Control of Drugs

Monolithic Silicas in Separation Science: Concepts, Syntheses, Characterization, Modeling and Applications, First Edition

Volumn , Issue , 2011, Pages 189-205

  Taha, Mohammed ^a   Abed, Abdelkarem ^a   El Deeb, Sami ^a  

^a AL AZHAR UNIVERSITY   (Palestine)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84884050344     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1002/9783527633241.ch10     Document Type: Chapter

References (67)

1. Kobayashi, H., Ikegami, T., Tanaka, N., et al. (2006) Properties of monolithic silica columns for HPLC. J. Anal. Sci., 22, 491-499.
2. Dear, G., Plumb, R., Mallet, D., et al. (2001) Use of monolithic silica columns to increase analytical throughput for metabolite identification by liquid chromatography/tandem mass spectrometry. Rapid Commun. Mass Spectrom., 15 (2), 152-158.
3. Van Nederkassel, A., Aerts, A., Dierick, A., et al. (2003) Fast separations on monolithic silica columns: method transfer, robustness, and column aging for some case studies. J. Pharm. Biomed. Anal., 32 (2), 233-249.
4. Hsieh, Y., Wang, G., Wang, Y., et al. (2002) Simultaneous determination of a drug candidate and its metabolite in rat plasma samples using ultrafast monolithic column high -performance liquid chromatography/tandem mass spectrometry. Rapid Commun. Mass Spectrom., 16 (10), 944-950.
5. Pihlainen, K., Sippola, E., and Kostiainen, R. (2003) Rapid identification and quantitation of compounds with forensic interest using fast liquid chromatography -ion trap mass spectrometry and library searching. J. Chromatogr. A, 994 (1-2), 93-102.
6. Volmer, D.A., Brombacher, S., and Whitehead, B. (2002) Studies on azaspiracid biotoxins. I. Ultrafast high -resolution liquid chromatography/mass spectrometry separations using monolithic columns. Rapid Commun. Mass Spectrom., 16 (24), 2298-2305.
7. Jakab, A., and Forgacs, E. (2002) Characterization of plant oils on a monolithic silica column by high -performance liquid chromatography -atmospheric pressure chemical ionization -mass spectrometry. Chromatographia, 56, S69 -S73.
8. Rostagno, M., Palma, M., and Barroso, C. (2007) Fast analysis of soy isoflavones by high -performance liquid chromatography with monolithic columns. J. Anal. Chim. Acta, 582 (2), 243-249.
9. Xiong, L., Zhang, R., and Regnier, F.E. (2004) Potential of silica monolithic columns in peptide separations. J. Chromatogr. A, 1030 (1-2), 187-194.
10. Shah, A.J., Crespi, F., and Heidbreder, C. (2002) Amino acid neurotransmitters: separation approaches and diagnostic value. J. Chromatogr. B, 781 (1-2), 151-163.
11. Tanaka, N., Kimura, H., Tokuda, D., et al. (2004) Simple and comprehensive two -dimensional reversed -phase HPLC using monolithic silica columns. Anal. Chem., 76 (5), 1273-1281.
12. Merck website (2005) Speed and Performance in Monolithic Form, Chromolith ® HPLC Columns http://www.merck.de/en/index.html (accessed March 7, 2005).
13. Tzanavaras, P.D., Themelis, D.G., Zotou, A., Stratis, J., et al. (2008) Optimization and validation of a dissolution test for selegiline hydrochloride tablets by a novel rapid HPLC assay using a monolithic stationary phase. J. Pharm. Biomed. Anal., 46 (4), 670-675.
14. Liu, Y., Antonucci, V., Shen, Y., Vailaya, A., et al. (2005) Applications of monolithic columns to pharmaceutical process development. J. Liq. Chromatogr. Related Technol., 28 (3), 341-356.
15. Cabrera, K., Lubda, D., Eggenweiler, H., Minakuchi, H., and Nakanishi, K. (2000) A new monolithic -type HPLC column for fast separations. J. High Resolut. Chromatogr., 23 (1), 93-99.
16. Liu, J., Sun, J., Zhang, W., Gao, K., et al. (2008) HPLC determination of rifampicin and related compounds in pharmaceuticals using monolithic column. J. Pharm. Biomed. Anal., 46 (2), 405-409.
17. Mizuguchi, T., Ogasawara, C., and Shimada, K. (2005) Application of monolithic silica column for HPLC separation of estrogens. J. Chromatogr., 3, 101-104.
18. Mc Fadden, K., Gillespie, J., Carney, B., and O ' Driscoll, D. (2006) Development and application of a high -performance liquid chromatography method using monolithic columns for the analysis of ecstasy tablets. J. Chromatogr. A, 1120 (1-2), 54-60.
19. Ali, I., and Aboul -Enein, H.Y. (2005) Fast determination of haloperidol in pharmaceutical preparations using HPLC with a monolithic silica column. J. Liq. Chromatogr. Related Technol., 28 (20), 3169-3179.
20. Pavli, V., and Kmetec, V. (2004) Fast separation of bacitracin on monolithic silica columns. J. Pharm. Biomed. Anal., 36 (2), 257-264.
21. Aboul -Enein, H.Y., Hoenen, H., Ghanem, A., and Koll, M. (2005) Reversed phase liquid chromatographic method for the high -throughput analysis of clopidogrel in pharmaceutical formulations using a monolithic silica column. J. Liq. Chromatogr. Related Technol., 28 (9), 1357-1365.
22. Aboul -Enein, H.Y., and Ali, I. (2005) Determination of tadalafil in pharmaceutical preparation by HPLC using monolithic silica column. Talanta, 65 (1), 276-280.
23. Aboul -Enein, H.Y., and Hefnawy, M.M. (2003) Rapid determination of sildenafil citrate in pharmaceutical preparations using monolithic silica HPLC column. J. Liq. Chromatogr. Related Technol., 26 (17), 2897-2908.
24. Aboul -Enein, H.Y., and Hefnawy, M.M. (2003) High throughput analysis of lamivudine in pharmaceutical preparations using monolithic silica HPLC column. Anal. Lett., 36 (11), 2527-2538.
25. Koelling -Speer, I. (2006) 16 -O -Methylcafestol determination in coffee using different HPLC columns and eluents with diode array and MS detection. J. Computer Optical Disk, 21, 204-208.
26. Shanker, K., Gupta, M.M., Srivastava, S.K., Bawankule, D.U., et al. (2007) Determination of bioactive nitrile glycosides in drumstick (Moringa oleifera) by reverse phase HPLC. Food Chem., 105 (1), 376-382.
27. Gupta, M.M., Singh, D.V., Tripathi, A.K., Pandey, R., et al. (2005) Simultaneous determination of vincristine, vinblastine, catharanthine, and vindoline in leaves of Catharanthus roseus by high -performance liquid chromatography. J. Chromatogr. Sci., 43 (9), 450-453.
28. Schmidt, A.H. (2005) Fast HPLC for quality control of Harpagophytum procumbens by using a monolithic silica column: method transfer from conventional particle -based silica column. J. Chromatogr. A, 1073 (1-2), 377-381.
29. Pan, C., Zhang, H., Chen, S., Xu, Y., and Jiang, S. (2006) Determination of chloramphenicol residues in honey by monolithic column liquid chromatography -mass spectrometry after use of quenchers clean -up. Acta Chromatographica, 17, 320-327.
30. Aboul -Enein, H.Y., Ghanem, A., Hoenen, H., et al. (2005) Determination of vardenafil in pharmaceutical formulation by HPLC using conventional C18 and monolithic silica columns. J. Liq. Chromatogr. Related Technol., 28 (4), 593-604.
31. El Deeb, S., and Watzig, H. (2006) Performance comparison between monolithic C18 and conventional C18 particle -packed columns in the liquid chromatographic determination of propranolol HCl. Turk. J. Chem., 30, 543-552.
32. El Deeb, S., Schepers, U., and Waetzig, H. (2006) Evaluation of monolithic C18 HPLC columns for the fast analysis of pilocarpine hydrochloride in the presence of its degradation products. Pharmazie, 61 (9), 751-756.
33. Novakova, L., Matysova, L., Solichova, D., Koupparis, M.A., et al. (2004) Comparison of performance of C18 monolithic rod columns and conventional C18 particle -packed columns in liquid chromatographic determination of Estrogel and Ketoprofen gel. J. Chromatogr. B, 813 (1-2), 191-197.
34. Karin Cabrera (2008) Recent advances in silica -based monolithic HPLC columns, http://chromatographyonline. findanalytichem.com/lcgc/article/articleDetail.jsp?id=512609 & sk= & date= & pageID=4 (accessed April 20, 2009).
35. El Deeb, S. (2006) High efficiency separation techniques: Fast HPLC using monolithic silica columns and chiral separation using capillary zone electrophoresis.
36. Mistry, K., and Grinberg, N. (2005) Application of monolithic columns in high performance liquid chromatography. J. Liq. Chromatogr. Related Technol., 28 (7-8), 1055-1074.
37. Smith, J.H. (2002) Chromatographic properties of silica -based monolithic HPLC columns, p. 83.
38. Altria, K.D., Marsh, A., and Clark, B. (2006) High performance liquid chromatographic analysis of pharmaceuticals using oil -in -water microemulsion eluent and monolithic column. J. Chromatogr., 63 (7-8), 309-314.
39. El Deeb, S., Schepers, U., and Waetzig, H. (2006) Fast HPLC method for the determination of glimepiride, glibenclamide, and related substances using monolithic column and flow program. J. Sep. Sci., 29 (11), 1571-1577.
40. Kaminiski, L., El Deeb, S., and Wätzig, H. (2008) Repeatability of monolithic HPLC columns while using a flow program. J. Sep. Sci., 31 (10), 1745-1749.
41. Tzanavaras, P.D., and Themelis, D.G. (2007) High -throughput HPLC assay of acyclovir and its major impurity guanine using a monolithic column and a flow gradient approach. J. Pharm. Biomed. Anal., 43 (4), 1526-1530.
42. El Deeb, S., Preu, L., and Waetzig, H. (2004) Evaluation of monolithic HPLC columns for various pharmaceutical separations: Method transfer from conventional phases and batch to batch repeatability. J. Pharm. Biomed. Anal., 44 (1), 85-95.
43. El Deeb, S., Preu, L., and Waetzig, H. (2007) A strategy to develop fast RP -HPLC methods using monolithic silica columns. J. Sep. Sci., 30 (13), 1993-2001.
44. Kimura, H., Tanigawa, T., Morisaka, H., Ikegami, T., et al. (2004) Simple 2D -HPLC using a monolithic silica column for peptide separation. J. Sep. Sci., 27 (10-11), 897-904.
45. Li, F., Wang, L., Yang, G., and Zhao, Y. (2008) Synthesis and evaluation of octadecyl ether -bonded monolithic silica column. Huaxue Tongbao, 71 (3), 220-223.
46. Guo, N., Zhao, Y., Zhang, Y., et al. (2005) Roles of TiO 2 nanoparticles in the formation of monolithic silica -gels via bulk sol -gel process. Zh Neorg Khim, 50 (2), 197-203.
47. Miyazaki, S., Miah, M.Y., Morisato, K., et al. (2005) Titania -coated monolithic silica as separation medium for high performance liquid chromatography of phosphorus -containing compounds. J. Sep. Sci., 28 (1), 39-44.
48. Chankvetadze, B., Kubota, T., Ikai, T., Yamamoto, C., et al. (2006) High -performance liquid chromatographic enantioseparations on capillary columns containing crosslinked polysaccharide phenylcarbamate derivatives attached to monolithic silica. J. Sep. Sci., 29 (13), 1988-1995.
49. Mathias, B., Clarissa, H., and Armin, M. (2006) Enantiomer separation on monolithic silica HPLC columns using chemically bonded methylated and methylated/acetylated 6 -O -tert -butyldimethylsilylated beta -cyclodextrin. J. Sep. Sci., 29 (11), 1561-1570.
50. Xiaoli, D., Jing, D., Junjie, O., et al. (2007) Preparation and evaluation of a vancomycin -immobilized silica monolith as chiral stationary phase for CEC. Electrophoresis, 28 (15), 2606-2612.
51. Ikegami, T., Fujita, H., Horie, K., et al. (2006) HILIC mode separation of polar compounds by monolithic silica capillary columns coated with polyacrylamide. Anal. Bioanal. Chem., 386 (3), 578-585.
52. Chuanhui, X., Jiwei, H., Xiao, H., et al. (2005) Preparation of monolithic silica column with strong cation -exchange stationary phase for capillary electrochromatography. J. Sep. Sci., 28 (8), 751-756.
53. Jiwei, H., Chuanhui, X., Ruijun, T., et al. (2007) Separation of basic and acidic compounds by capillary electrochromatography using monolithic silica capillary columns with zwitterionic stationary phase. J. Sep. Sci., 30 (6), 891-899.
54. Obando, M.A., Estela, J.M., and Cerda, V. (2008) Simultaneous determination of hydrochlorothiazide and losartan potassium in tablets by high -performance low -pressure chromatography using a multi -syringe burette coupled to a monolithic column. Anal. Bioanal. Chem., 391 (6), 2349-2356.
55. Gonzalez -San Miguel, H.M., Alpizar -Lorenzo, J.M., and Cerda, V. (2007) Simultaneous determination of ß -lactamic antibiotics by a new high -performance low -pressure chromatographic system using a multisyringe burette coupled to a monolithic column (MSC). Anal. Bioanal. Chem., 387 (2), 663-671.
56. Satinsky, D., Chocholous, P., Salabova, M., and Solich, P. (2006) Simple determination of betamethasone and chloramphenicol in a pharmaceutical preparation using a short monolithic column coupled to a sequential injection system. J. Sep. Sci., 29 (16), 2494-2499.
57. Waite, S., McGinley, M. (2006) Phenomenex website for Onyx HPLC columns. www.phenomenex.com (accessed April 7, 2009).
58. Plumb, R., Dear, G., Mallett, D., and Ayrton, J. (2001) Direct analysis of pharmaceutical compounds in human plasma with chromatographic resolution using an alkyl -bonded silica rod column. Rapid Commun. Mass Spectrom., 15 (12), 986-993.
59. Zang, X., Luo, R., Song, N., Chen, T., et al. (2005) A novel online solid -phase extraction approach integrated with a monolithic column and tandem mass spectrometry for direct plasma analysis of multiple drugs and metabolites. Rapid Commun. Mass Spectrom., 19 (22), 3259-3268.
60. Aboul -Enein, H.Y., and Hefnawy, M.M. (2005) Liquid chromatographic high -throughput analysis of ketamine and its metabolites in human plasma using a monolithic silica column and solid phase extraction. Talanta, 65 (1), 67-73.
61. Foroutan, S.M., Zarghi, A., Shafaati, A., and Khoddam, A. (2006) Application of monolithic column in quantification of gliclazide in human plasma by liquid chromatography. J. Pharm. Biomed. Anal., 42 (4), 513-516.
62. Zarghi, A., Foroutan, S.M., Shafaati, A., and Khoddam, A. (2006) HPLC determination of omeprazole in human plasma using a monolithic column. Arzneimittelforschung, 56 (6), 382-386.
63. Zarghi, A., Foroutan, S.M., Shafaati, A., and Khoddam, A. (2006) Development an ion -pair liquid chromatographic method for determination of sotalol in plasma using a monolithic column. J. Pharm. Biomed. Anal., 41 (4), 1433-1437.
64. Caufield, W.V., and Stewart, J.T. (2002) Rapid determination of selected drugs of abuse in human plasma using a monolithic silica HPLC column and solid phase extraction. J. Liq. Chromatogr. Related Technol., 25 (19), 2977-2998.
65. Souverain, S., Rudaz, S., and Veuthey, J.L. (2003) Use of monolithic supports for fast analysis of drugs and metabolites in plasma by direct injection. Chromatographia, 57 (9-10), 569-575.
66. Huang, M.Q., Mao, Y., Jemal, M., and Arnold, M. (2006) Increased productivity in quantitative bioanalysis using a monolithic column coupled with high -flow direct -injection liquid chromatography/tandem mass spectrometry. Rapid Commun. Mass Spectrom., 20 (11), 1709-1714.
67. Borges, V., Yang, E., Dunn, J., and Henion, J. (2004) High -throughput liquid chromatography -tandem mass spectrometry determination of bupropion and its metabolites in human, mouse and rat plasma using a monolithic column. J. Chromatogr. B, 804 (2), 277-287.