메뉴 건너뛰기




Volumn 386, Issue 3, 2006, Pages 578-585

HILIC mode separation of polar compounds by monolithic silica capillary columns coated with polyacrylamide

Author keywords

HILIC; Monolithic silica; Nucleosides; PA sugars; Polyacrylamide

Indexed keywords

DERIVATIVES; MECHANICAL PERMEABILITY; NITROGEN COMPOUNDS; POLYACRYLATES; SEPARATION; SILICA;

EID: 33748998166     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-006-0606-z     Document Type: Article
Times cited : (82)

References (42)
  • 1
    • 0000087926 scopus 로고    scopus 로고
    • Majors RE (2000) LC-GC 18:262-285
    • (2000) LC-GC , vol.18 , pp. 262-285
    • Majors, R.E.1
  • 5
  • 34
    • 33749002321 scopus 로고    scopus 로고
    • note
    • N-(3-trimethoxysilylpropyl)methacrylamide was prepared by adding methacryloyl chloride (15.6 ml, 161 mmol) in THF (15 ml) for 1 h to a mixture of APS (25 ml, 107 mmol) and triethylamine (22.5 ml, 161 mmol) in THF (50 ml) at 0°C. The mixture was filtered through PTFE membrane filter to remove any salts, and THF was distilled in vacuo to give the desired product as a brown viscous liquid (28.5 g, 98%)


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.