Supercritical Carbon Dioxide Extraction of Eugenol from Clove Buds: Process Optimization and Packed Bed Characterization

Food and Bioprocess Technology

Volumn 6, Issue 10, 2013, Pages 2587-2599

  Chatterjee, Dipan ^a   Bhattacharjee, Paramita ^a  

^a JADAVPUR UNIVERSITY   (India)

Author keywords

Chrastil equation; Clove buds; Dimensionless numbers; Eugenol; Supercritical carbon dioxide extraction

Indexed keywords

CHRASTIL EQUATION; CLOVE BUDS; DIMENSIONLESS NUMBER; EUGENOL; SUPERCRITICAL CARBON DIOXIDE EXTRACTION;

EFFLUENT TREATMENT; EXTRACTION; OPTIMIZATION; PACKED BEDS; SOLUBILITY; SUPERCRITICAL FLUID EXTRACTION; SUPERCRITICAL FLUIDS;

CARBON DIOXIDE;

SYZYGIUM AROMATICUM;

EID: 84883656997     PISSN: 19355130     EISSN: 19355149     Source Type: Journal    
DOI: 10.1007/s11947-012-0979-2     Document Type: Article

References (37)

1. Bartle, K. D., Clifford, A. A., Hawthorne, S. B., Langenfeld, J. J., Miller, D. J., & Robinson, R. (1990). A model for dynamic extraction using a supercritical fluid. The Journal of Supercritical Fluids, 3, 143-149.
2. Bhattacharjee, P., Chatterjee, D., & Singhal, R. S. (2012). Supercritical carbon dioxide extraction of squalene from Amaranthus paniculatus: experiments and process characterization. Food Bioprocess Technology, 5, 2506-2521.
3. Bhattacharjee, P., Singhal, R. S., & Tiwari, S. R. (2007). Supercritical carbon dioxide extraction of cottonseed oil. Journal of Food Engineering, 79, 892-898.
4. Catchpole, O. J., & Von Kamp, J. C. (1997). Phase equilibrium for the extraction of squalene from shark liver oil using supercritical carbon dioxide. Industrial & Engineering Chemistry Research, 36, 3762-3768.
5. Chaieb, K., Hajlaoui, H., Zmantar, T., Kahla-Nakbi, A. B., Rouabbhia, M., Mahdouani, K., & Bakhrouf, A. (2007). The chemical composition and biological activity of clove essential oil, Eugenia caryophyllata (Syzigium aromaticum L. Myrtaceae): a short review. Phytotherapy Research, 21, 501-506.
6. Chatterjee, D., Bhattacharjee, P., Banerjee, A. (2012). Phytochemical analyses and food applications on clove bud extracts obtained by liquid and supercritical carbon dioxide extraction technologies. Proceedings of 2012 International Conference on Engineering and Applied Science, ISSN 2227-0299, ISBN 978-986-87417-1-3, 392-409.
7. 2 extraction. LWT - Food Science and Technology, 31, 454-460.
8. Ge, Y., Ni, Y., Yan, H., Chen, Y., & Cai, T. (2002). Optimization of the supercritical fluid extraction of natural vitamin E from wheat germ using response surface methodology. Journal of Food Science, 67, 239-243.
9. Gopalakrishnan, N., Shanti, P. P. V., & Narayanan, C. S. (1990). Composition of clove (Syzygium aromaticum) bud oil extracted using carbon dioxide. Journal of the Science of Food and Agriculture, 50, 111-117.
10. Hazra, A., Alexander, K., Dollimore, D., & Riga, A. (2004). Characterization of some essential oils and their key components: thermoanalytical techniques. Journal of Thermal Analysis and Calorimetry, 75, 317-330.
11. Hildebrand, J. H., & Scott, R. L. (1950). The solubility of nonelectrolytes (3rd ed.). New York: Dover.
12. 2 extraction-molecular distillation of essential oil from clove (Eugenia caryophyllata Thunb.) Bud. Chemistry and Industry of Forest Products, 29, 74-78.
13. Ismadji, S., & Bhatia, S. K. (2003). Solubility of selected esters in supercritical carbon dioxide. The Journal of Supercritical Fluids, 27, 1-11.
14. Jafari Nejad, S., Abolghasemi, H., Moosavian, M. A., & Maragheh, M. G. (2010). Prediction of solute solubility in supercritical carbon dioxide: a novel semi-empirical model. Chemical Engineering Research and Design, 88, 893-898.
15. King, J. W. (1995). Determination of the solubility parameter of soybean oil by inverse gas chromatography. LWT - Food Science and Technology, 28, 190-195.
16. 2 extraction of rice bran. Journal of the American Oil Chemists' Society, 75, 623-628.
17. Kwon, K. T., Uddin, M. S., Jung, G. W., Sim, J. E., & Chun, B. S. (2010). Supercritical carbon dioxide extraction of phenolics and tocopherols enriched oil from wheat bran. International Journal of Biological and Life Sciences, 6, 117-122.
18. Lim, G. B., Holder, G. D., & Shah, Y. T. (1989). Solid-fluid mass transfer in a packed bed under supercritical conditions. In: Supercritical fluid science and technology, pp. 379-395. Washington, DC: American Chemical Society.
19. 2 in a countercurrent packed column. The Journal of Supercritical Fluids, 39, 304-314.
20. Montgomery, D. C. (2001a). Experiments with a single factor: the analysis of variance. In: Design and analysis of experiments, pp. 60-125. John Wiley & Sons Inc, New York.
21. Montgomery, D. C. (2001b). Response surface methods and other approaches to process optimization. In: Design and analysis of experiments, pp. 427-510. John Wiley & Sons Inc, New York.
22. Mukhopadhyay, M. (2000). Fundamentals of supercritical fluids and phase equilibria. In: Natural extracts using supercritical carbon dioxide, pp. 13-39. Boca Raton, FL: CRC Press.
23. Norhuda, I., & Mohd Omar, A. K. (2009). Mass transfer modeling in a packed bed of palm kernels under supercritical conditions. International Journal of Chemical and Biological Engineering, 2, 10-13.
24. Peng, D. Y., & Robinson, D. B. (1976). A new two-constant equation of state. Industrial and Engineering Chemistry Fundamentals, 15, 59-64.
25. Perry, R. H., Green, D. W., & Maloney, J. O. (1997). Perry's chemical engineer's handbook (7th ed., pp. 15-22). New York: McGraw-Hill.
26. Reverchon, E. (1997). Supercritical fluid extraction and fractionation of essential oils and related products. Journal of Supercritical Fluids, 10, 1-37.
27. Reverchon, E., Daghero, J., Marrone, C., Mattea, M., & Poletto, M. (1999). Supercritical fractional extraction of fennel seed oil and essential oil: experiments and mathematical modeling. Industrial & Engineering Chemistry Research, 38, 3069-3075.
28. Reverchon, E., & Marrone, C. (1997). Supercritical extraction of clove bud essential oil: isolation and mathematical modeling. Chemical Engineering Science, 20, 3421-3428.
29. 2 separation process. Drying Technology, 25, 335-339.
30. Silva, G. F., Gamarra, F. M. C., Oliveira, A. L., & Cabral, F. A. (2008). Extraction of bixin from annatto seeds. Brazilian Journal of Chemical Engineering, 25, 419-426.
31. 2. Journal of Chemical and Engineering Data, USA, 49, 352-356.
32. Stuber, F., Ma, A., Ma, V., Larrayoz, A., & Recasens, F. (1996). Supercritical fluid extraction of packed beds: external mass transfer in upflow and downflow operation. Industrial and Engineering Chemistry Research, 35, 3618-3628.
33. Tan, C. S., Liang, S. K., & Liou, D. C. (1988). Fluid-solid mass transfer in a supercritical fluid extractor. The Chemical Engineering Journal, 38, 17-22.
34. Tho, F. C., Natova, L., & Ruschev, D. (1991). Thermal analysis of eugenol, isoeugenol and their benzoic acid esters. Journal of Thermal Analysis and Calorimetry, 37, 2723-2727.
35. Wenqiang, G., Shufen, L., Ruixiang, Y., Shaokun, T., & Can, Q. (2007). Comparison of essential oils of clove buds extracted with supercritical carbon dioxide and other three traditional extraction methods. Food Chemistry, 101, 1558-1564.
36. Westerman, D., Santos, R. C. D., Bosley, J. A., Rogers, J. S., & Al-Duri, B. (2006). Extraction of Amaranth seed oil by supercritical carbon dioxide. The Journal of Supercritical Fluids, 37, 38-52.
37. 2 extraction of essential oil from clove bud: effect of operation conditions on the selective Isolation of eugenol and eugenyl acetate. Zeitschrift für Naturforschung. B, A journal of chemical sciences, 60, 1197-1201.