Determination of cocaine in postmortem human liver exposed to overdose. Application of an innovative and efficient extraction/clean up procedure and gas chromatography-mass spectrometry analysis

Journal of Chromatography A

Volumn 1309, Issue , 2013, Pages 15-21

  Magalhães, Elisângela Jaqueline ^a   Queiroz, Maria Eliana Lopes Ribeiro de ^b   Penido, Marcus Luiz de Oliveira ^c   Paiva, Marco Antônio Ribeiro ^c   Teodoro, Janaína Aparecida Reis ^a   Augusti, Rodinei ^a   Nascentes, Clésia Cristina ^a  

^a FEDERAL UNIVERSITY OF MINAS GERAIS   (Brazil)

^b FEDERAL UNIVERSITY OF VIÇOSA   (Brazil)

^c Toxicology Laboratory   (Brazil)

Author keywords

Cocaine; Extraction procedure; GC MS; Liver; Low temperature partitioning; Sample preparation

Indexed keywords

COCAINE; EXTRACTION PROCEDURE; GC-MS; LOW TEMPERATURES; SAMPLE PREPARATION;

CALIBRATION; EXTRACTION; IONIC STRENGTH; LIVER; MAMMALS; MASS SPECTROMETRY; OPTIMIZATION; PH; TEMPERATURE;

GAS CHROMATOGRAPHY;

ACETONITRILE; AMINE; COCAINE; SODIUM CHLORIDE; SOLVENT; SORBENT; WATER;

ACCURACY; ANIMAL TISSUE; ARTICLE; AUTOPSY; CALIBRATION; CHEMICAL COMPOSITION; COW; DRUG ABUSE; DRUG INTOXICATION; DRUG LIVER LEVEL; HUMAN; HUMAN TISSUE; IONIC STRENGTH; LIMIT OF QUANTITATION; LIQUID LIQUID EXTRACTION; LOW TEMPERATURE PARTITIONING; LOW TEMPERATURE PROCEDURES; MASS FRAGMENTOGRAPHY; NONHUMAN; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; PURIFICATION; SOLID PHASE EXTRACTION; VALIDATION PROCESS; VOLUMETRY;

BOVINAE;

EID: 84883246278     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.08.039     Document Type: Article

References (36)

1. Jagerdeo E., Abdel-Rehim M. J. Am. Soc. Mass Spectrom. 2009, 20:891.
2. Drummer O.H. Forensic Sci. Int. 2004, 142:101.
3. Lewis R.J., Johnson R.D., Angier M.K., Ritter R.M. J. Chromatogr. B 2004, 806:141.
4. Musshoff F., Madea B. Forensic Sci. Int. 2010, 200:67.
5. Shimomura E.T., Hodge G.D., Paul B.D. Clin. Chem. 2001, 47:1040.
6. Degenhardt L., Singleton J., Calabria B., McLaren J., Kerr T., Mehta S., Kirk G., Hall W.D. Drug Alcohol Depend. 2011, 113:88.
7. Carvalho V.M., Fukushima A.R., Fontes L.R., Fuzinato D.V., Florio J.C., Chasin A.A.M. J. Forensic Leg. Med. 2012, 10.1016/j.jflm.2012.06.006.
8. Nováková L., Vlcková H. Anal. Chim. Acta 2009, 656:8.
9. Kataoka H., Saito K. J. Pharm. Biomed. Anal. 2011, 54:926.
10. Goulart S.M., Alves R.D., Neves A.A., de Queiroz J.H., de Assis T.C., de Queiroz M.E.L.R. Anal. Chim. Acta 2010, 671:41.
11. de Pinho G.P., Neves A.A., de Queiroz M.E.L.R., Silvério F.O. Food Control 2010, 21:1307.
12. Rübensam G., Barreto F., Hoff R.B., Kist T.L., Pizzolato T.M. Anal. Chim. Acta 2011, 705:24.
13. de Pinho G.P., Neves A.A., Queiroz M.E.L.R.d., Silvério F.O. Food Chem. 2010, 121:251.
14. Goulart S.M., de Queiroz M.E.L.R., Neves A.A., de Queiroz J.H. Talanta 2008, 75:1320.
15. Pichini S., Pacifici R., Pellegrini M., Marchei E., Pérez-Alarcón E., Puig C., Vall O., García-Algar O. J. Chromatogr. B 2003, 794:281.
16. Joya X., Pujadas M., Falcón M., Civit E., Garcia-Algar O., Vall O., Pichini S., Luna A., de la Torre R. Forensic Sci. Int. 2010, 196:38.
17. Marchei E., Escuder D., Pallas C.R., Garcia-Algar O., Gómez A., Friguls B., Pellegrini M., Pichini S. J. Pharm. Biomed. Anal. 2011, 55:309.
18. Pellegrini M., Casá A., Marchei E., Pacifici R., Mayné R., Barbero V., Garcia-Algar O., Pichini S. J. Pharm. Biomed. Anal. 2006, 40:662.
19. Follador M.J.D., Yonamine M., Moreau R.L.d.M., Silva O.A. J. Chromatogr. B 2004, 811:37.
20. Adamowicz P., Kala M. Forensic Sci. Int. 2010, 198:39.
21. Langel K., Gunnar T., Ariniemi K., Rajamäki O., Lillsunde P. J. Chromatogr. B 2011, 879:859.
22. Míguez-Framil M., Moreda-Piñeiro A., Bermejo-Barrera P., Álvarez-Freire I., Tabernero M.J., Bermejo A.M. J. Chromatogr. A 2010, 1217:6342.
23. Mercolini L., Mandrioli R., Gerra G., Raggi M.A. J. Chromatogr. A 2010, 1217:7242.
24. Janicka M., Kot-Wasik A., Namiesnik J. Trends Anal. Chem. 2010, 29:209.
25. Contreras M.T., Hernández A.F., González M., González S., Ventura R., Pla A., Valverde J.L., Segura J., Torre R.d.l. Forensic Sci. Int. 2006, 164:168.
26. Margalho C., Franco J., Corte-Real F., Vieira D.N. J. Forensic Leg. Med. 2011, 18:132.
27. Jones G.R., Singer P.P. Drug Testing in Alternate Biological Specimens 2008, 139-152. Humana Press/Springer, Secaucus, NJ. A. Jenkins (Ed.).
28. Food and Drug Administration Guidance for Industry: Bioanalytical Method Validation. US Department of Health and Human Services, FDA, Center for Drug Evaluation and Research, Rockville, MD, 2001.
29. European Medicines Agency, Committee for Medicinal Products for Human Use Guideline on Bioanalytical Method Validation 2011, European Medicines Agency, London, UK.
30. Stewart D.J., Inaba T., Tang B.K., Kalow W. Life Sci. 1977, 20:1557.
31. Jenkins A.J., Levine B., Titus J., Smialek J.E. Forensic Sci. Int. 1999, 101:17.
32. Roberts S.M., Munson J.W., James R.C., Harbison R.D. Anal. Biochem. 1992, 202:256.
33. Poklis A., Maginn D., Barr J.L. Forensic Sci. Int. 1987, 33:83.
34. Peretti F.J., Isenschmid D.S., Levine B., Caplan Y.H., Smialek J.E. Forensic Sci. Int. 1990, 48:135.
35. Giroud C., Michaud K., Sporkert F., Eap C., Augsburger M., Cardinal P., Mangin P. J. Anal. Toxicol. 2004, 28:464.
36. Burns D.T., Danzer K., Townshend A. Pure Appl. Chem. 2002, 74:2201.