A liquid-liquid extraction procedure followed by a low temperature purification step for the analysis of macrocyclic lactones in milk by liquid chromatography-tandem mass spectrometry and fluorescence detection

Analytica Chimica Acta

Volumn 705, Issue 1-2, 2011, Pages 24-29

  Rübensam, Gabriel ^a,b   Barreto, Fabiano ^b   Hoff, Rodrigo Barcellos ^b   Kist, Tarso Ledur ^a   Pizzolato, Tânia Mara ^a  

^a FEDERAL UNIVERSITY OF RIO GRANDE DO SUL   (Brazil)

^b PECUÁRIA E ABASTECIMENTO   (Brazil)

Author keywords

Avermectins; Extraction; Liquid chromatography fluorescence detection; Liquid chromatography tandem mass spectrometry; Low temperature purification

Indexed keywords

ABAMECTIN; AVERMECTINS; BOVINE MILK; COEFFICIENT OF VARIATION; COMMISSION DECISION 2002/657/EC; DORAMECTIN; EPRINOMECTIN; FLUORESCENCE DETECTION; HIGH-THROUGHPUT ANALYSIS; IVERMECTIN; LC-MS/MS; LIQUID CHROMATOGRAPHY-FLUORESCENCE DETECTION; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; LIQUID-LIQUID EXTRACTION; LIQUID-LIQUID EXTRACTION PROCEDURE; LOW COSTS; LOW TEMPERATURES; MACROCYCLIC LACTONES; MATRIX EFFECTS; NUMBER OF SAMPLES; QUANTIFICATION LIMIT; RECOVERY RATE;

CHROMATOGRAPHY; DRUG PRODUCTS; EXTRACTION; FLUORESCENCE; HIGH PRESSURE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PURIFICATION; SOLVENT EXTRACTION;

LIQUIDS;

ABAMECTIN; DORAMECTIN; EPRINOMECTIN; IVERMECTIN; MACROLIDE; MOXIDECTIN;

ARTICLE; CONTROLLED STUDY; FLUORESCENCE; HIGH THROUGHPUT SCREENING; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; LOW TEMPERATURE; LOW TEMPERATURE PURIFICATION; MILK; PRIORITY JOURNAL; PURIFICATION; QUANTITATIVE ANALYSIS; TANDEM MASS SPECTROMETRY; VALIDATION STUDY;

ANIMALS; CATTLE; CHROMATOGRAPHY, LIQUID; FLUORESCENCE; LACTONES; LIQUID-LIQUID EXTRACTION; MACROCYCLIC COMPOUNDS; MILK; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

BOVINAE;

EID: 80053386044     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2011.02.041     Document Type: Article

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