A new silylation reagent dimethyl(3,3,3-trifluoropropyl)silyldiethylamine for the analysis of estrogenic compounds by gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1301, Issue , 2013, Pages 215-224

  Caban, Magda ^a   Czerwicka, Małgorzata ^a   Łukaszewicz, Paulina ^a   Migowska, Natalia ^a   Stepnowski, Piotr ^a   Kwiatkowski, Marek ^a   Kumirska, Jolanta ^a  

^a UNIVERSITY OF GDA SK   (Poland)

Author keywords

Comparative study; DIMETRIS; Estrogenic compounds; Fragmentation pattern; Mass spectra analysis; Silylation

Indexed keywords

COMPARATIVE STUDIES; DIMETRIS; ESTROGENIC COMPOUNDS; FRAGMENTATION PATTERNS; MASS SPECTRA; SILYLATIONS;

GAS CHROMATOGRAPHY; MASS SPECTROMETRY; MIXTURES;

CHEMICAL ANALYSIS;

CHLOROTRIMETHYLSILANE; DIETHYLSTILBESTROL DERIVATIVE; DIMETHYL (3,3,3 TRIFLUOROPROPYL)SILYLDIETHYLAMINE; ESTRADIOL DERIVATIVE; ESTRIOL; ESTRONE DERIVATIVE; ETHINYLESTRADIOL; N BUTYLDIMETHYLSILYL N METHYLTRIFLUOROACETAMIDE; N,O BIS(TRIMETHYLSILYL)TRIFLUOROACETAMIDE; PYRIDINE; TRIFLUOROACETAMIDE DERIVATIVE; UNCLASSIFIED DRUG;

ANALYTICAL PARAMETERS; ARTICLE; COMPARATIVE STUDY; CONTROLLED STUDY; ELUTION; HIGH TEMPERATURE; LOW TEMPERATURE; MASS FRAGMENTOGRAPHY; NUCLEOPHILICITY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; SILYLATION;

COMPARATIVE STUDY; DIMETRIS; ESTROGENIC COMPOUNDS; FRAGMENTATION PATTERN; MASS SPECTRA ANALYSIS; SILYLATION;

ESTRENES; ESTROGENS; ETHYLAMINES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; REPRODUCIBILITY OF RESULTS; SOLID PHASE EXTRACTION; TRIMETHYLSILYL COMPOUNDS;

EID: 84879887457     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.05.073     Document Type: Article

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