Mass spectrometry as a useful tool for the analysis of stabilizers in polymer materials

TrAC - Trends in Analytical Chemistry

Volumn 50, Issue , 2013, Pages 53-64

  Klampfl, Christian W ^a  

^a JOHANNES KEPLER UNIVERSITY LINZ   (Austria)

Author keywords

Depth profiling; Direct analysis; Hindered amine light stabilizer (HALS); Liquid chromatography (LC); Mass spectrometry (MS); Plastics material; Polymer; Screening; Stabilizer; Surface analysis

Indexed keywords

DEPTH PROFILING; ELASTOMERS; LIQUID CHROMATOGRAPHY; LUNAR SURFACE ANALYSIS; MASS SPECTROMETRY; POLYMERS; SCREENING; STABILIZERS (AGENTS); SURFACE ANALYSIS; TOOLS;

DIRECT ANALYSIS; HINDERED AMINE LIGHT STABILIZER; POLYMER MATERIALS; WEAK POINTS;

PLASTICS;

PLASTIC; POLYMER; STABILIZING AGENT;

CHEMICAL ANALYSIS; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INTERMETHOD COMPARISON; LASER DESORPTION MASS SPECTROMETRY; MASS SPECTROMETRY; PRIORITY JOURNAL; REVIEW; SCREENING TEST; SURFACE PROPERTY; TIME OF FLIGHT SECONDARY ION MASS SPECTROMETRY;

EID: 84879471770     PISSN: 01659936     EISSN: 18793142     Source Type: Journal    
DOI: 10.1016/j.trac.2013.04.012     Document Type: Review

References (68)

1. Jenke D.R. Encyclopedia of Chromatography 2010, CRC Press, Bocca Raton. third ed.
2. Bart J.C.J. Polymer additive analysis at the limits. Polym. Degrad. Stab. 2003, 82:197-205.
3. Jenke D. Chromatographic methods used to identify and quantify organic polymer additives. J. Liquid Chromatogr. Rel. Tech. 2003, 26:2417-2447.
4. Reingruber E., Buchberger W. Analysis of polyolefine stabilizers and their degradation products. J. Sep. Sci. 2010, 33:3463-3475.
5. Barth H.G., Majors R.E. Approaches for extracting and determining additives, contaminants and low-molecular-weight by-products in synthetic polymers. LC-GC (Europe) 2013, 26:23-33.
6. Denberg M., Mosbaek H., Hassager O., Arvin E. Determination of the concentration profile and homogeneity of antioxidants and degradation products in a cross-linked polyethylene type A (PEXa) pipe. Polym. Test. 2009, 28:378-385.
7. Rothenbacher T., Schwack W. Non-targeted multi-component analytical screening of plastic food contact materials using fast interpretation of deliverables via expert structure-activity relationship software. J. AOAC Int. 2009, 92:941-950.
8. Ritter A., Michel E., Schmid M., Affolter S. Interlaboratory test on polymers: determination of antioxidants in polyolefins. Polym. Test. 2005, 24:498-506.
9. Taguchi Y., Ishida Y., Ohtani H., Bekku H., Sera M. Determination of a polymeric hindered amine light stabilizer in polypropylene formulated with magnesium hydroxide flame retardant by reactive thermal desorption-gas chromatography Anal. Science 2004, 20:495-500.
10. Dopico-Garcia M.S., Noguerol-Cal R., Castro-Lopez M.M., Cela-Perez M.C., Pinon-Giz E., Lopez-Vilarino J.M., Gonzalez-Rodriguez M.V. Determination of polyolefin additives by reversed-phase liquid chromatography. Cent. Eur. J. Chem. 2012, 10:585-610.
11. Lavison-Bompard G., Thiebaut D., Beziau J.-F., Carraze B., Valette P., Duteurtre X., Tabet J.-C. Hyphenation of atmospheric pressure chemical ionisation mass spectrometry to supercritical fluid chromatography for polar car lubricant additives analysis. J. Chromatogr. A 2009, 1216:837-844.
12. Vandenburg H.J., Clifford A.A., Bartle K.D., Carroll J., Newton I., Garden L.M., Dean J.R., Costley C.T. Analytical extraction of additives from polymers. Analyst 1997, 122:101R-115R.
13. Aminlashgari N., Hakkarainen M. Emerging mass spectrometric tools for analysis of polymers and polymer additives. Mass Spectrometry of Polymers-New Techniques 2012, Springer, Heidelberg. M. Hakkarainen (Ed.).
14. Jansson K.D., Zawodny C.P., Wampler T.P. Determination of polymer additives using analytical pyrolysis. J. Anal. Appl. Pyrolysis 2007, 79:353-361.
15. Dietrich R. Submonolayer detection of polymer additives at the surface of industrial products. Fresenius J. Anal. Chem. 1998, 361:692-694.
16. Walzak M.J., McIntyre N.S., Prater T., Kaberline S., Graham B.A. Detection and mapping of Chimassorb 944FD antioxidant additive in polyethylene using TOF-SIMS. Anal. Chem. 1999, 71:1428-1430.
17. Stapel D., Benninghoven A. Application of atomic and molecular primary ions for TOF-SIMS analysis of additive containing polymer surfaces. Appl. Surf. Sci. 2001, 174:261-270.
18. Schnöller J., Pittenauer E., Hutter H., Allmaier G. Analysis of antioxidants in insulation cladding of copper wire: a comparison of different mass spectrometric techniques (ESI-MS, MALDI-RTOF and RTOF-SIMS). J. Mass Spectrom. 2009, 44:1724-1732.
19. Medard N., Bennninghoven A., Rading D., Liciardello A., Auditore A., Duc T.M., Montigaud H., Vernerey F., Poleunis C., Bertrand P. Antioxidant seggregation and crystallisation at polyester surfaces studied by TOF-SIMS. Appl. Surf. Sci. 2003, 203-204:571-574.
20. Medard N., Poleunis C., van den Eynde X., Bertrand P. Characterization of additives at polymer surfaces by TOF-SIMS. Surf. Interface Anal. 2002, 34:565-569.
21. Poleunis C., Medard N., Bertrand P. Additive quantification of polymer thin films by TOF-SIMS: aging sample effects. Appl. Surf. Sci. 2004, 231-232:269-273.
22. Medard N., Bertrand P. Additive behavior in ultrathin polymer films investigated by TOF-SIMS. Appl. Surf. Sci. 2004, 231-232:309-313.
23. Bryan S.R., Belu A.M., Hoshi T., Oiwa R. Evaluation of a gold LMIG for detecting small molecules in a polymer matrix by TOF-SIMS. Appl. Surf. Sci. 2004, 231-232:201-206.
24. Ito H., Kono T. Quantitative analysis of organic additive content in apolymer by TOF-SIMS with PCA. Appl. Surf. Sci. 2008, 255:1044-1047.
25. Taguchi Y., Ishida Y., Ohtani H., Matsubara H. Direct analysis of an oligomeric hindered amine light stabilizer in polypropy-lene materials by MALDI-MS using a solid sampling technique to study its photostabilizing action. Anal. Chem. 2004, 76:697-703.
26. Schwarzinger C., Gabriel S., Beißmann S., Buchberger W. Quantitative analysis of polymer additives with MALDI-TOF MS using an internal standard approach. J. Am. Soc. Mass Spectrom. 2012, 23:1120-1125.
27. Pasch H., Schrepp W. MALDI-TOF Mass Spectrometry of Synthetic Polymers 2003, Springer, Heidelberg. first ed.
28. Wright S.J., Dale M.J., Langridge-Smith P.R.R., Zhan Q., Zenobi R. Selective in situ detection of polymer additives using laser mass spectrometry. Anal. Chem. 1996, 68:3585-3594.
29. Zhan Q., Zenobi R., Wright S.J., Langridge-Smith P.R.R. Spatially resolved in-situ analysis of polymer additives by two-step laser mass spectrometry. Macromolecules 1996, 29:7856-7871.
30. Gross J. Mass Spectrometry 2011, Springer, Heidelberg. second ed.
31. Cody R.B., Laramee J.A., Durst H.D. Versatile new ion source for the analysis of materials in open air under ambient conditions. Anal. Chem. 2005, 77:2297-2302.
32. Ackerman L.K., Noonan G.O., Begley T.H. Assessing direct analysis in real-time mass spectrometry (DART) for the rapid identification of additives in food packaging. Food Addit. Contam. 2009, 26:1611-1618.
33. Haunschmidt M., Klampfl C.W., Buchberger W., Hertsens R. Rapid identification of stabilisers in polypropylene using time-of-flight mass spectrometry and DART as ion source. Analyst 2010, 135:80-85.
34. Fouyer K., Lavastre O., Rondeau D. Direct monitoring of the role played by a stabilizer in a solid sample of polymer using direct analysis in real time mass spectrometry: the case of Irgafos 168 in polyethylene. Anal. Chem. 2012, 84:8642-8649.
35. Navare A.T., Mayoral J.G., Nouzova M., Noriega F.G., Fernandez F.M. Rapid direct analysis in real time (DART) mass spectrometric detection of juvenile hormone III and its terpene precursors. Bioanal. Chem. 2010, 398:3005-3013.
36. Wang C., Zhu H., Cai Z., Song F., Liu Z., Liu S. Newborn screening of phenylketonuria using direct analysis in real time (DART) mass spectrometry. Bioanal. Chem. 2013, 405:3159-3164.
37. Takats Z., Wiseman J.M., Gologan B., Cooks R.G. Mass spectrometry sampling under ambient conditions with desorption electrospray ionization. Science 2004, 306:471-473.
38. Reiter S.M., Buchberger W., Klampfl C.W. Rapid identification and semi-quantitative determination of polymer additives by desorption electrospray ionization/time-of-flight mass spectrometry. Anal. Bioanal. Chem. 2011, 400:2317-2322.
39. Paine M.R.L., Barker P.J., Blanksby S.J. Desorption electrospray ionisation mass spectrometry reveals in situ modification of hidered amine light stabiliser resulting from direct N-OR bond cleavage. Analyst 2011, 136:904-912.
40. Paine M.R.L., Barker P.J., Blanksby S.J. Paint spray mass spectrometry for the detection of additives from polymers on conducting surfaces. Mass Spectrom Lett. 2012, 3:25-28.
41. Liu J., Wang H., Cooks R.G., Ouyang Z. Leaf spray: direct chemical analysis of plant material and living plants by mass spectrometry. Anal. Chem. 2011, 83:7608-7613.
42. Wang H., Manicke N.E., Yang Q., Zheng L., Shi R., Cooks R.G., Ouyang Z. Direct analysis of biological tissue by paper spray mass spectrometry. Anal. Chem. 2011, 83:1197-1201.
43. Paine M.R.L., Barker P.J., Maclauglin S.A., Mitchell T.W., Blanksby S.J. Direct detection of additives and degradation products from polymers by liquid extraction surface analysis employing chip-based nanospray mass spectrometry. Rapid Commun. Mass Spectrom. 2012, 26:412-418.
44. Kertesz V., Van Berkel G.J. Fully automated liquid extraction-based surface sampling and ionization using a chip-based robotic nanoelectrospray platform. J. Mass Spectrom. 2010, 45:252-260. 1.
45. Suni N.M., Aalto H., Kauppila T.J., Kotiaho T., Kostiainen R. Analysis of lipids with desorption atmospheric pressure photoionization-mass spectrometry (DAPPI-MS) and desorption electrospray ionization-mass spectrometry (DESI-MS). J. Mass Spectrom. 2012, 47:611-619.
46. McEwen C.N., McKays R.G., Larsen B.S. Analysis of solids, liquids, and biological tissues using solids probe introduction at atmospheric pressure on commercial LC/MS instruments Anal. Chemistry 2005, 77:7826-7831.
47. Barrere C., Maire F., Alfonso C., Giusti P. Atmospheric solid analysis probe-ion mobility mass spectrometry of polypropylene. Anal. Chem. 2012, 84:9349-9354.
48. Whitison S.E., Wesdemiotis C., Lattimer R.P. Characterization of polyurethane formulations by direct probe atmospheric pressure chemical ionization mass spectroemtry. Rubber Chem. Technol. 2010, 83:35-45.
49. Trimpin S., Wijerathne K., McEwen C.N. Rapid methods of polymer and polymer additives identification: multi-sample solvent-free MALDI, pyrolysis at atmospheric pressure, and atmospheric solids analysis probe mass spectrometry. Anal. Chim. Acta 2009, 654:20-25.
50. Lattimer R.P., Polce M.J. Direct probe CI-MS and APCI-MS for direct material analysis. J. Anal. Appl. Pyrol. 2011, 92:355-360.
51. Boutin M., Lesage J., Ostiguy C., Bertrand M.J. Temperature-programmed pyrolysis hyphenated with metastable atom bombardment ionization mass spectrometry (TPPy/MAB-MS) for the identification of additives in polymers. J. Am. Soc. Mass Spectrom. 2004, 15:1315-1319.
52. Buchberger W., Stiftinger M. Analysis of polymer additives and impurities by liquid chromatography/mass spectrometry and capillary electrophoresis/mass spectrometry. Mass Spectrometry of Polymers-New Techniques 2012, Springer, Heidelberg. M. Hakkarainen (Ed.).
53. Lowe T.A., Paine M.R.L., Marshall D.L., Hick L.A., Boge J.A., Barker P.J., Blanksby S.J. Structural identification of hindered amine light stabilisers in coil coatings using electrospray ionisation tandem mass spectrometry. J. Mass Spectrom. 2010, 45:486-495.
54. Hsiao S.T., Tseng M.C., Chen Y.R., Her G.R. Analysis of polymer additives by matrix-assisted laser desorption ionization/time of flight mass spectrometer using delayed extraction and collision induced dissociation. J. Chin. Chem. Soc. 2001, 48:1017-1027.
55. Im S.-H., Choi S.-S. Role of the UV absorber as a matrix in matrix-assisted laser desorption/ionization mass spectrometric analysis of a mixture of a UV absorber and a stabilizer. Rapid Commun. Mass Spectrom. 2010, 24:2753-2758.
56. Pasch H., Meyer-Dulheuer T., Resch M. Zum direkten Nachweis von UV-Stabilisatoren in Kunststoffen durch MALDI-TOF-Massenspektrometrie. KGK 1998, 51:782-788.
57. 2 nanoparticles. J. Mass Spectrom. Soc. Jpn. 2010, 58:123-127.
58. Himmelsbach M., Buchberger W., Reingruber E. Determination of polymer additives by liquid chromatography coupled with mass spectrometry. A comparison of atmospheric pressure photoionization (APPI), atmospheric pressure chemical ionization (APCI) and electrospray ionization (ESI). Polym. Degrad. Stabil. 2009, 94:1213-1219.
59. Duderstadt R.E., Fischer S.M. Effect of organic mobile phase composition on signal responses for selected polyalkene additive compounds by liquid chromatography-mass spectrometry. J. Chromatogr. A 2008, 1193:70-78.
60. Noguerol-Cal R., Lopez-Vilarino J.M., Fernandez-Martinez G., Gonzalez-Rodriguez M.V., Barral-Losada L.F. Liquid chromatographic methods to analyze hindered amines light stabilizers (HALS) levels to improve safety in polyolefines. J. Sep. Sci. 2010, 33:2698-2706.
61. Andersen T., Skuland I.L., Holm A., Trones R., Greibrokk T. Temperature-programmed packed capillary liquid chromatography coupled to evaporative light-scattering detection and electrospray ionization time-of-flight mass spectrometry for characterization of high-molecular-mass hindered amine light stabilizers. J. Chromatogr. A 2004, 1029:49-56.
62. Louden D., Handley A., Lenz E., Sinclair I., Taylor S., Wilson I.D. Reversed-phase HPLC of polymer additives with multiple on-line spectroscopic analysis (UV, IR, (1)H NMR and MS). Anal. Bioanal. Chem. 2002, 373:508-515.
63. Block C., Wynants L., Kelchtermans M., De Boer R., Compernolle F. Identification of polymer additives by liquid chromatography-mass spectrometry. Polym. Degrad. Stab. 2006, 91:3163-3173.
64. Reingruber E., Himmelsbach M., Sauer C., Bucberger W. Identification of degradation products of antioxidants in polyolefins by liquid chromatography combined with atmospheric pressure photoionisation mass spectrometry. Polym. Degrad. Stab. 2010, 95:740-745.
65. Choi S.-S., Jang J.-H. Analysis of UV absorbers and stabilizers in polypropylene by liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry. Polym. Test 2011, 30:673-677.
66. 2 detection. Anal. Bioanal. Chem. 2013, 405:3177-3184.
67. Park I., Yoon K.-H., Namgoong H. Determination of Tinuvin 292 in acrylic resins by reversed-phase high performance liquid chromatography-electrospray ionization-ion trap mass spectrometry. Chem. Lett. 2012, 41:301-303.
68. S. Beißmann, Ph.D. Thesis, Johannes Kepler University Linz/Austria (in preparation).