-
1
-
-
0011779578
-
-
2 nd edn., (Ed.: I. Ojima), Wiley-Interscience, New York
-
T. Ohkuma, M. Kitamura, R. Noyori, in: Catalytic Asymmetric Synthesis, 2 nd edn., (Ed.:, I. Ojima,), Wiley-Interscience, New York, 2000, p 1
-
(2000)
Catalytic Asymmetric Synthesis
, pp. 1
-
-
Ohkuma, T.1
Kitamura, M.2
Noyori, R.3
-
2
-
-
0003616618
-
-
2 nd edn., Wiley-VCH, Weinheim, chap 3.3.1
-
H.-U. Blaser, B. Pugin, F. Spindler, Applied Homogeneous Catalysis with Organometallic Compounds, 2 nd edn., Wiley-VCH, Weinheim, 2000, chap 3.3.1
-
(2000)
Applied Homogeneous Catalysis with Organometallic Compounds
-
-
Blaser, H.-U.1
Pugin, B.2
Spindler, F.3
-
5
-
-
84891564839
-
-
(Ed.: Q.-L. Zhou), Wiley-VCH
-
S.-F. Zhu, Q.-L. Zhou, in: Privileged chiral ligands and catalysts, (Ed.:, Q.-L. Zhou,), Wiley-VCH, 2011, p 137
-
(2011)
Privileged Chiral Ligands and Catalysts
, pp. 137
-
-
Zhu, S.-F.1
Zhou, Q.-L.2
-
6
-
-
33644640381
-
-
(Eds.: J. G. de Vries, C. J. Elsevier), Wiley, New York
-
M. L. Clarke, G. J. Roff, in: The Handbook of Homogeneous Hydrogenation, (Eds.:, J. G. de Vries, C. J. Elsevier,), Wiley, New York, 2007.
-
(2007)
The Handbook of Homogeneous Hydrogenation
-
-
Clarke, M.L.1
Roff, G.J.2
-
7
-
-
84864478361
-
-
B. S. Lucas, B. Fisher, L. R. McGee, S. H. Olson, J. C. Medina, E. Cheung, J. Am. Chem. Soc. 2012, 134, 12855
-
(2012)
J. Am. Chem. Soc.
, vol.134
, pp. 12855
-
-
Lucas, B.S.1
Fisher, B.2
McGee, L.R.3
Olson, S.H.4
Medina, J.C.5
Cheung, E.6
-
8
-
-
77952380086
-
-
K. C. Nicolaou, R. J. Aversa, J. Jin, F. Rivas, J. Am. Chem. Soc. 2010, 132, 6855
-
(2010)
J. Am. Chem. Soc.
, vol.132
, pp. 6855
-
-
Nicolaou, K.C.1
Aversa, R.J.2
Jin, J.3
Rivas, F.4
-
9
-
-
65549116499
-
-
H. Tone, M. Buchotte, C. Mordant, E. Guittet, T. Ayad, V. Ratovelomanana-Vidal, Org. Lett. 2009, 11, 1995.
-
(2009)
Org. Lett.
, vol.11
, pp. 1995
-
-
Tone, H.1
Buchotte, M.2
Mordant, C.3
Guittet, E.4
Ayad, T.5
Ratovelomanana-Vidal, V.6
-
10
-
-
84904098573
-
-
in:, (Ed.: S. Ma), Springer-Verlag, Berlin, Heideberg, p
-
Q.-L. Zhou, J.-H. Xie, in: Asymmetric catalysis from a Chinese perspective, (Ed.:, S. Ma,), Springer-Verlag, Berlin, Heideberg, 2011, p 1
-
(2011)
Asymmetric Catalysis from A Chinese Perspective
, pp. 1
-
-
Zhou, Q.-L.1
Xie, J.-H.2
-
12
-
-
84861838551
-
-
J.-Q. Chen, J.-H. Xie, D.-H. Bao, S. Liu, Q.-L. Zhou, Org. Lett. 2012, 14, 2714.
-
(2012)
Org. Lett.
, vol.14
, pp. 2714
-
-
Chen, J.-Q.1
Xie, J.-H.2
Bao, D.-H.3
Liu, S.4
Zhou, Q.-L.5
-
13
-
-
84871545837
-
-
Q.-Q. Zhang, J.-H. Xie, X.-H. Yang, J.-B. Xie, Q.-L. Zhou, Org. Lett. 2012, 14, 6158.
-
(2012)
Org. Lett.
, vol.14
, pp. 6158
-
-
Zhang, Q.-Q.1
Xie, J.-H.2
Yang, X.-H.3
Xie, J.-B.4
Zhou, Q.-L.5
-
14
-
-
84859963678
-
-
L.-J. Cheng, J.-H. Xie, L.-X. Wang, Q.-L. Zhou, Adv. Synth. Catal. 2012, 354, 1105.
-
(2012)
Adv. Synth. Catal.
, vol.354
, pp. 1105
-
-
Cheng, L.-J.1
Xie, J.-H.2
Wang, L.-X.3
Zhou, Q.-L.4
-
15
-
-
84868248664
-
-
J.-H. Xie, L.-C. Guo, X.-H. Yang, L.-X. Wang, Q.-L. Zhou, Org. Lett. 2012, 14, 4758.
-
(2012)
Org. Lett.
, vol.14
, pp. 4758
-
-
Xie, J.-H.1
Guo, L.-C.2
Yang, X.-H.3
Wang, L.-X.4
Zhou, Q.-L.5
-
16
-
-
84878262375
-
-
C. Liu, J.-H. Xie, Y.-L. Li, J.-Q. Chen, Q.-L. Zhou, Angew. Chem. 2013, 125, 621
-
(2013)
Angew. Chem.
, vol.125
, pp. 621
-
-
Liu, C.1
Xie, J.-H.2
Li, Y.-L.3
Chen, J.-Q.4
Zhou, Q.-L.5
-
19
-
-
38349079974
-
-
H. Pellissier, Tetrahedron 2008, 64, 1563. For selected recent papers on asymmetric hydrogenation of racemic α-substituted ketones via DKR, see
-
(2008)
Tetrahedron
, vol.64
, pp. 1563
-
-
Pellissier, H.1
-
20
-
-
80052019373
-
-
M. Akashi, N. Arai, T. Inoue, T. Ohkuma, Adv. Synth. Catal. 2011, 353, 1955
-
(2011)
Adv. Synth. Catal.
, vol.353
, pp. 1955
-
-
Akashi, M.1
Arai, N.2
Inoue, T.3
Ohkuma, T.4
-
21
-
-
75749154441
-
-
W.-J. Bai, J.-H. Xie, Y.-L. Li, S. Liu, Q.-L. Zhou, Adv. Synth. Catal. 2010, 352, 81
-
(2010)
Adv. Synth. Catal.
, vol.352
, pp. 81
-
-
Bai, W.-J.1
Xie, J.-H.2
Li, Y.-L.3
Liu, S.4
Zhou, Q.-L.5
-
22
-
-
78249259179
-
-
T. Hibino, K. Makino, T. Sugiyama, H. Takaya, ChemCatChem 2009, 1, 237
-
(2009)
ChemCatChem
, vol.1
, pp. 237
-
-
Hibino, T.1
Makino, K.2
Sugiyama, T.3
Takaya, H.4
-
23
-
-
70350635784
-
-
S. Liu, J.-H. Xie, W. Li, W.-L. Kong, L.-X. Wang, Q.-L. Zhou, Org. Lett. 2009, 11, 4994
-
(2009)
Org. Lett.
, vol.11
, pp. 4994
-
-
Liu, S.1
Xie, J.-H.2
Li, W.3
Kong, W.-L.4
Wang, L.-X.5
Zhou, Q.-L.6
-
24
-
-
67849103989
-
-
J.-H. Xie, S. Liu, W.-L. Kong, X.-C. Wang, L.-X. Wang, Q.-L. Zhou, J. Am. Chem. Soc. 2009, 131, 4222.
-
(2009)
J. Am. Chem. Soc.
, vol.131
, pp. 4222
-
-
Xie, J.-H.1
Liu, S.2
Kong, W.-L.3
Wang, X.-C.4
Wang, L.-X.5
Zhou, Q.-L.6
-
25
-
-
4444287706
-
-
The cyclohexanone with an ethylene ketal group at its 3 position is sensitive under base conditions, forming 3-alkoxycyclohex-2-enone. See, T. K. M. Shing, C. M. Lee, H. Y. Ho, Tetrahedron 2004, 60, 9179. The poor solubility of 1a in i-PrOH is also a major reason for the formation of by-product 4a. The poor solubility of compound 1a in i-PrOH slows down the reaction rate of the hydrogenation. At the same time, the base-sensitive compound 1a is converted to by-product 4a. When toluene is added as a co-solvent, the solubility of compound 1a increases remarkably and the hydrogenation reaction speeds up. As a result, the formation of by-product 4a is suppressed.
-
(2004)
Tetrahedron
, vol.60
, pp. 9179
-
-
Shing, T.K.M.1
Lee, C.M.2
Ho, H.Y.3
-
28
-
-
77957083775
-
-
in:; (Eds.: R. H. F. Manske, H. L. Holmes), Academic Press, New York, p 331
-
J. W. Cook, J. D. Loudon, in: The Alkaloids; (Eds.:, R. H. F. Manske, H. L. Holmes,), Academic Press, New York, 1952, Vol. 2, p 331
-
(1952)
The Alkaloids
, pp. 2
-
-
Cook, J.W.1
Loudon, J.D.2
-
29
-
-
0000427207
-
-
S. Ghosal, K. S. Saini, S. Razdan, Phytochemistry 1985, 24, 2141.
-
(1985)
Phytochemistry
, vol.24
, pp. 2141
-
-
Ghosal, S.1
Saini, K.S.2
Razdan, S.3
-
30
-
-
84943915564
-
-
K. Takeda, K. Kotera, S. Mizukami, M. Kobayashi, Chem. Pharm. Bull. 1960, 8, 483
-
(1960)
Chem. Pharm. Bull.
, vol.8
, pp. 483
-
-
Takeda, K.1
Kotera, K.2
Mizukami, S.3
Kobayashi, M.4
-
33
-
-
0042730091
-
-
K. Tomioka, K. Nishimura, M. Yamashita, N. Fukuyama, K.-I. Yamada, O. Muraoka, K. Tomioka, Org. Lett. 2003, 5, 1123
-
(2003)
Org. Lett.
, vol.5
, pp. 1123
-
-
Tomioka, K.1
Nishimura, K.2
Yamashita, M.3
Fukuyama, N.4
Yamada, K.-I.5
Muraoka, O.6
Tomioka, K.7
-
36
-
-
0028225158
-
-
W. Oppolzer, A. C. Spivey, C. G. Bochet, J. Am. Chem. Soc. 1994, 116, 3139
-
(1994)
J. Am. Chem. Soc.
, vol.116
, pp. 3139
-
-
Oppolzer, W.1
Spivey, A.C.2
Bochet, C.G.3
-
37
-
-
0025908071
-
-
J.-E. Backvall, P. G. Andersson, G. B. Stone, A. GoZoll, J. Org. Chem. 1991, 56, 2988
-
(1991)
J. Org. Chem.
, vol.56
, pp. 2988
-
-
Backvall, J.-E.1
Andersson, P.G.2
Stone, G.B.3
Gozoll, A.4
-
38
-
-
0021135994
-
-
C.-L. Wang, W. C. Ripka, P. N. Confalon, Tetrahedron Lett. 1984, 25, 4613
-
(1984)
Tetrahedron Lett.
, vol.25
, pp. 4613
-
-
Wang, C.-L.1
Ripka, W.C.2
Confalon, P.N.3
-
39
-
-
0000292841
-
-
B. Umezawa, O. Hoshino, S. Sawaki, H. Sashida, K. Mori, Tetrahedron 1984, 40, 1783
-
(1984)
Tetrahedron
, vol.40
, pp. 1783
-
-
Umezawa, B.1
Hoshino, O.2
Sawaki, S.3
Sashida, H.4
Mori, K.5
-
40
-
-
0017588899
-
-
B. Umezawa, O. Hoshino, S. Sawaki, S. Sato, N. Numao, J. Org. Chem. 1977, 42, 4272.
-
(1977)
J. Org. Chem.
, vol.42
, pp. 4272
-
-
Umezawa, B.1
Hoshino, O.2
Sawaki, S.3
Sato, S.4
Numao, N.5
-
41
-
-
84867250820
-
-
Y. Wang, Y.-C. Luo, H.-B. Zhang, P.-F. Xu, Org. Biomol. Chem. 2012, 10, 8211.
-
(2012)
Org. Biomol. Chem.
, vol.10
, pp. 8211
-
-
Wang, Y.1
Luo, Y.-C.2
Zhang, H.-B.3
Xu, P.-F.4
-
42
-
-
33947086608
-
-
R. O. Hutchins, C. A. Milewski, B. E. Maryanoff, J. Am. Chem. Soc. 1973, 95, 3662.
-
(1973)
J. Am. Chem. Soc.
, vol.95
, pp. 3662
-
-
Hutchins, R.O.1
Milewski, C.A.2
Maryanoff, B.E.3
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