Evaluation of different derivatisation approaches for gas chromatographic-mass spectrometric analysis of carbohydrates in complex matrices of biological and synthetic origin

Journal of Chromatography A

Volumn 1281, Issue , 2013, Pages 115-126

  Becker, M ^a   Zweckmair, T ^a   Forneck, A ^a   Rosenau, T ^a   Potthast, A ^a   Liebner, F ^a  

^a UNIVERSITY OF NATURAL RESOURCES AND LIFE SCIENCES   (Austria)

Author keywords

Carbohydrate analysis; GC MS; O isopropylidenation; Oximation; Trifluoroacetylation; Trimethylsilylation

Indexed keywords

CARBOHYDRATE ANALYSIS; GC/MS; O-ISOPROPYLIDENATION; OXIMATION; TRIFLUOROACETYLATION; TRIMETHYL SILYLATION;

ALDEHYDES; CHEMICAL ANALYSIS; GAS CHROMATOGRAPHY; GLUCOSE; MASS SPECTROMETERS; MASS SPECTROMETRY; SEPARATION; TRIFLUOROACETIC ACID;

CARBOHYDRATES;

CARBOHYDRATE;

ACETYLATION; ARTICLE; BENZOXIMATION; CALIBRATION; CARBOHYDRATE ANALYSIS; CHEMICAL REACTION; CONTROLLED STUDY; DECOMPOSITION; DERIVATIZATION; ETHOXIMATION; ISOPROPYLIDENATION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MASS SPECTROMETRY; MOLECULAR WEIGHT; NONHUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SEPARATION TECHNIQUE; SILYLATION; STEREOCHEMISTRY; TRIFLUOROACETYLATION; TRIMETHYLSILYLATION;

ACETALDEHYDE; CARBOHYDRATES; CLUSTER ANALYSIS; DIHYDROXYACETONE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; LINEAR MODELS; MULTIVARIATE ANALYSIS;

EID: 84873990572     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.01.053     Document Type: Article

References (40)

1. Rudnik E. Compostable Polymer Materials 2008, Elsevier, Oxford, Boston.
2. Decker P., Schweer H., Pohlmann R. J. Chromatogr. A 1982, 244:281.
3. Sanz M.L., Martinez-Castro I. J. Chromatogr. A 2007, 1153:74.
4. Koek M.M., Muilwijk B., van der Werf M.J., Hankemeier T. Anal. Chem. 2006, 78:1272.
5. Blau K., Halket J.M. Handbook of Derivatives for Chromatography 1993, Wiley, New York.
6. Zaikin V., Halket J. A Handbook of Derivatives for Mass Spectrometry 2009, IM Publications, Chichester.
7. Knapp D.R. Handbook of Analytical Derivatization Reactions 1979, Wiley, New York.
8. Andrews M.A. Carbohydr. Res. 1989, 194:1.
9. García-Raso A., Fernández-Díaz M., Páez M.I., Sanz J., Martínez-Castro I. J. Chromatogr. A 1989, 471:205.
10. Ruiz-Matute A.I., Hernandez-Hernandez O., Rodriguez-Sanchez S., Sanz M.L., Martinez-Castro I. J. Chromatogr. B: Analyt. Technol. Biomed. Life Sci. 2011, 879:1226.
11. Black G.E., Fox A. J. Chromatogr. A 1996, 720:51.
12. M. Becker, F., Liebner, T., Rosenau, A. Potthast, submitted to Talanta.
13. Mason B.S., Slover H.T. J. Agr. Food Chem. 1958, 6:551.
14. Fiehn O., Kopka J., Trethewey R.N., Willmitzer L. Anal. Chem. 2000, 72:3573.
15. Morgenlie S. Carbohydr. Res. 1975, 41:285.
16. Funcke W., von Sonntag C. Carbohydr. Res. 1979, 69:247.
17. Snyder J.R. Carbohydr. Res. 1990, 198:1.
18. Chemische Analytik, Nachweis-, Erfassungs- und Bestimmungsgrenze, Normenausschuss Materialprüfung, DIN 32645:2008-11.
19. De Jongh D.C., Biemann K. J. Am. Chem. Soc. 1964, 86:67.
20. Morgenlie S. Carbohydr. Res. 1980, 80:215.
21. Zaikin V.G., Halket J.M. Eur. J. Mass Spectrom. 2004, 10:555.
22. García-Raso A., Martínez-Castro I., Páez M.I., Sanz J., García-Raso J., Saura-Calixto F. J. Chromatogr. A 1987, 398:9.
23. Paez M., Martínez-Castro I., Sanz J., Olano A., Garcia-Raso A., Saura-Calixto F. Chromatographia 1987, 23:43.
24. Englmaier P. Carbohydr. Res. 1985, 144:177.
25. König W.A., Bauer H., Voelter W., Bayer E. Chem. Ber. 1973, 106:1905.
26. Zanetta J.P., Breckenridge W.C., Vincendon G. J. Chromatogr. A 1972, 69:291.
27. Lakszner K., Szepesy L., Vida L. Chromatographia 1984, 19:304.
28. Moldoveanu S., David V. J. Chromatogr. Libr. 2002, 930.
29. Kalsi P.S. Spectroscopy of Organic Compounds 2004, New Age International, New Delhi.
30. Hajslova J., Zrostlikova J. J. Chromatogr. A 2003, 1000:181.
31. Katona Z.F., Sass P., Molnar-Perl I. J. Chromatogr. A 1999, 847:91.
32. Fuzfai Z., Molnarperl I. J. Chromatogr. A 2007, 1149:88.
33. Fuzfai Z., Katona Z.F., Kovacs E., Molnar-Perl I. J. Agr. Food Chem. 2004, 52:7444.
34. Molnar-Perl I. J. Chromatogr. A 1999, 845:181.
35. Mastovska K., Lehotay S.J., Anastassiades M. Anal. Chem. 2005, 77:8129.
36. Dixon R.W., Baltzell G. J. Chromatogr. A 2006, 1109:214.
37. Snyder L.R., Kirkland J.J., Dolan J.W. Introduction to Modern Liquid Chromatography 2010, Wiley, Hoboken, NJ.
38. Grob R.L., Barry E.F. Modern Practice of Gas Chromatography 2004, Wiley-Interscience, Hoboken, NJ.
39. Brady R.F. Adv. Carbohydr. Chem. Biochem. 1971, 26:197.
40. Lehrfeld J. J. Chromatogr. A 1976, 120:141.