Simultaneous analysis of 17 diuretics in dietary supplements by HPLC and LC-MS/MS

Food Additives and Contaminants - Part A

Volumn 30, Issue 2, 2013, Pages 209-217

  Woo, H ^a   Kim, J W ^a   Han, K M ^a   Lee, J H ^a   Hwang, I S ^a   Kim, J ^a,a   Kweon, S J ^a   Cho, S ^a   Chae, K R ^a   Han, S Y ^a  

^a Korea Food and Drug Administration   (South Korea)

Author keywords

adulterant; dietary supplements; diuretics; HPLC; LC MS MS; simultaneous analysis

Indexed keywords

EXTRACTION; FOOD ADDITIVES; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NUTRITION; RECOVERY; SILICON COMPOUNDS; VITAMINS;

ADULTERANT; DIURETICS; HPLC; LC-MS/MS; SIMULTANEOUS ANALYSIS;

DIETARY SUPPLEMENTS;

ACETAZOLAMIDE; BENDROFLUMETHIAZIDE; BUMETANIDE; CHLOROTHIAZIDE; CYCLOTHIAZIDE; DIURETIC AGENT; ETACRYNIC ACID; FUROSEMIDE; HYDROCHLOROTHIAZIDE; HYDROFLUMETHIAZIDE; ILLICIT DRUG; INDAPAMIDE; METHYCLOTHIAZIDE; METOLAZONE; SPIRONOLACTONE; TORASEMIDE; TRIAMTERENE; TRICHLORMETHIAZIDE;

ARTICLE; BIOLOGICAL MONITORING; DIET SUPPLEMENTATION; DRUG DETERMINATION; EXTRACTION; LIQUID CHROMATOGRAPHY; MULTIPLE REACTION MONITORING; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SCREENING TEST; TANDEM MASS SPECTROMETRY; ULTRAVIOLET SPECTROSCOPY; WEIGHT REDUCTION;

EID: 84872588457     PISSN: 19440049     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/19440049.2012.738939     Document Type: Article

References (17)

1. Amendola, L, Colamonici, C, Mazzarino, M and Botre, F. 2003. Rapid determination of diuretics in human urine by gas chromatography-mass spectrometry following microwave assisted derivatization. Anal Chim Acta, 475: 125-136.
2. Barroso, MB, Meiring, HD, de Jong, A, Alonso, RM and Jimenez, RM. 1997. Gas chromatographic-mass spectrometric analysis of the loop diuretic torasemide in human urine. J Chromatogr B, 690: 105-113.
3. Bogusz, MJ, Hassan, H, Al-Enazi, E, Ibrahim, Z and Al-Tufail, M. 2006. Application of LC-ESI-MS-MS for detection of synthetic adulterants in herbal remedies. J Pharmaceut Biomed Anal, 41: 554-564.
4. Deventer, K, Delbeke, FT, Roels, K and van Eenoo, P. 2002. Screening for 18 diuretics and probenecide in doping analysis by liquid chromatography-tandem mass spectrometry. Biomed Chromatogr, 16: 529-535.
5. European Commission Decision No. 657/2002. 2002. Implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Commun. L221: 8-36
6. Food and Drug Administration (FDA). 2009. FDA uncovers additional tainted weight loss products. Agency alerts consumers to the finding of new undeclared drug ingredients; [cited 2009 Mar 20]. Available from:http://www.fda.gov/NewsEvents/Newsroom/PressAnnouncements/2009/ucm149547/
7. Gonzalez, E, Becerra, A and Laserna, JJ. 1996. Direct determination of diuretic drugs in urine by capillary zone electrophoresis using fluorescence detection. J Chromatogr B, 687: 145-150.
8. Goto, T, Mikami, E, Ohno, T and Matsumoto, H. 2002. Simultaneous analysis of four diuretic drugs by HPLC and its application to health food supplements advertising weight reduction. J Food Hyg Soc Jpn., 43: 95-98.
9. Guchelaar, HJ, Chandi, L, Schouten, O and van den Brand, WA. 1999. A high performance liquid chromatographic method for the screening of 17 diuretics in human urine. Fresenius J Anal Chem, 363: 700-705.
10. Kim, SH, Lee, J, Yoon, T, Choi, J, Choi, D, Kim, D and Kwon, SW. 2009. Simultaneous determination of anti-diabetes/anti-obesity drugs by LC/PDA, and targeted analysis of sibutramine analog in dietary supplements by LC/MS/MS. Biomed Chromatogr, 23: 1259-1265.
11. Reddy, IM, Beotra, A, Jain, S and Ahi, S. 2009. A simple and rapid ESI-LC-MS/MS method for simultaneous screening of doping agents in urine samples. Ind J Pharmacol, 41: 80-86.
12. Shao, B, Zhang, J, Yang, Y, Meng, J, Wu, Y and Duan, H. 2008. Simultaneous analysis of thirteen diuretics residues in bovine milk by ultra-performance liquid chromatography/tandem mass spectrometry. Rapid Comm Mass Spectrom, 22: 3427-3433.
13. Sora, DI, Udrescu, S, Albu, F, David, V and Medvedovici, A. 2010. Analytical issues in HPLC/MS/MS simultaneous assay of furosemide, spironolactone and canrenone in human plasma samples. J Pharmaceut Biomed Anal, 52: 734-740.
14. Thevis, M, Schmickler, H and Schanzer, W. 2002. Mass spectrometric behavior of thiazide-based diuretics after electrospray ionization and collision-induced dissociation. Anal Chem, 74: 3802-3808.
15. Thieme, D, Grosse, J, Lang, R, Mueller, RK and Wahl, A. 2001. Screening, confirmation and quantitation of diuretics in urine doping control analysis by high-performance liquid chromatography-atmospheric pressure ionisation tandem mass spectrometry. J Chromatogr B, 757: 49-57.
16. Tisdall, PA, Moyer, TP and Anhalt, JP. 1980. Liquid-chromatographic detection of thiazide diuretics in urine. Clin Chem, 26(6): 702-706.
17. Weiner, IM, Goodman Gilman, A, Rall, TW, Nies, AS and Taylor, P. 1990. Goodman and Gilman's pharmacological basis of therapeutics, New York (NY): Pergamon.