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Polymer synthesis by the SuzukiMiyaura cross-coupling reaction is accompanied by formation of boronic acids, which tend to precipitate in organic phase and hamper the formation of high-molecular-weight polymers. Thus polymer synthesis by this cross-coupling reaction is carried out often in an organicaqueous biphase system to let boronic acid residue move to aqueous phase. However, the presence of water often is apt to trigger protodeborylation. In sharp contrast, HOMSi-based cross-coupling reaction coproduces cyclic silyl ether 4 which acts like an organic solvent, and water cosolvent is not necessary. Therefore, HOMSi-based cross-coupling reaction is free of salt precipitation and protodesilylation
-
Polymer synthesis by the SuzukiMiyaura cross-coupling reaction is accompanied by formation of boronic acids, which tend to precipitate in organic phase and hamper the formation of high-molecular-weight polymers. Thus polymer synthesis by this cross-coupling reaction is carried out often in an organicaqueous biphase system to let boronic acid residue move to aqueous phase. However, the presence of water often is apt to trigger protodeborylation. In sharp contrast, HOMSi-based cross-coupling reaction coproduces cyclic silyl ether 4 which acts like an organic solvent, and water cosolvent is not necessary. Therefore, HOMSi-based cross-coupling reaction is free of salt precipitation and protodesilylation.
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In order to dissolve 4,7-dibromobenzothiadiazole, the reaction was carried out at 85 °C
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In order to dissolve 4,7-dibromobenzothiadiazole, the reaction was carried out at 85 °C.
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Supporting Information is available electronically on the CSJ-Journal Web site
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Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/ index.html.
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