Comparative study of sample decomposition methods for the determination of total Hg in crude oil and related products

Fuel Processing Technology

Volumn 106, Issue , 2013, Pages 122-126

  Pontes, Fernanda Veronesi M ^a,b   Carneiro, Manuel C ^a   Vaitsman, Delmo S ^b   Monteiro, Maria Inês C ^a   Neto, Arnaldo A ^a   Tristão, Maria Luíza B ^c   Guerrante, Maurício De F ^c  

^a CENTRO DE TECNOLOGIA MINERAL   (Brazil)

^b FEDERAL UNIVERSITY OF RIO DE JANEIRO   (Brazil)

^c PETROBRAS   (Brazil)

Author keywords

Crude oil; CV AAS; Mercury; Oil sludge; Sample decomposition

Indexed keywords

ACCURACY TEST; CERTIFIED REFERENCE MATERIALS; COLD VAPOR ATOMIC ABSORPTION SPECTROMETRY; COMPARATIVE STUDIES; CV-AAS; DECOMPOSITION METHODS; DIGESTION TIME; LOW COSTS; OIL SAMPLES; OIL SLUDGE; RELATED PRODUCTS; REPRODUCIBILITIES; SAMPLE DECOMPOSITION;

BOATS; MERCURY (METAL); QUARTZ; SPECTROSCOPIC ANALYSIS; WEIGHING;

CRUDE OIL;

EID: 84870565490     PISSN: 03783820     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.fuproc.2012.07.011     Document Type: Article

References (24)

1. C. Duyck, N. Miekeley, C.L.P. Da Silveira, R.Q. Aucélio, R.C. Campos, P. Grinberg, and G.P. Brandão The determination of trace elements in crude oil and its heavy fractions by atomic spectrometry Spectrochimica Acta Part B 62 2007 939 951 (Pubitemid 47407799)
2. A.V. Soin, T.A. Maryutina, T.V. Arbuzova, and B.Ya. Spivakov Sample preparation in the determination of metals in oil and petroleum products by ICP MS Journal of Analytical Chemistry 65 6 2010 571 576
3. S.M. Wilhelm, and N. Bloom Mercury in petroleum Fuel Processing Technology 63 2000 1 27 (Pubitemid 30561029)
4. N.S. Bloom Analysis and stability of mercury speciation in petroleum hydrocarbons Fresenius' Journal of Analytical Chemistry 366 2000 438 443
5. L. Liang, M. Horvat, V. Fajon, N. Prosenc, H. Li, and P. Pang Comparison of improved combustion/trap technique to wet extraction methods for determination of mercury in crude oil and related products by atomic fluorescence Energy Fuel 17 2003 1175 1179
6. R.A.A. Munoz, P.R.M. Correia, A.N. Nascimento, C.S. Silva, P.V. Oliveira, and L. Angnes Electroanalysis of crude oil and petroleum-based fuel for trace metals: evaluation of different microwave-assisted sample decompositions and stripping techniques Energy Fuel 21 2007 295 302
7. L. Liang, S. Lazoff, M. Horvat, and E. Swain Determination of mercury in crude oil by in-situ thermal decomposition using a simple lab built system Fresenius' Journal of Analytical Chemistry 367 2000 8 11
8. W.R. Kelly, S.E. Long, and J.L. Mann Determination of mercury in SRM crude oils and refined products by isotope dilution cold vapor ICP-MS using closed-system combustion Analytical and Bioanalytical Chemistry 376 2003 753 758 (Pubitemid 40877991)
9. R.A.K. Nadkarni, and J.D. Hwang Determination of mercury in crude oil by atomic spectroscopy Journal of ASTM International 8 5 2011 (Paper ID JAI103559.)
10. ASTM D7622-10 Standard Test Method for Total Mercury in Crude Oil using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction 2010
11. ASTM D7623-10 Standard Test Method for Total Mercury in Crude Oil using Combustion-Gold Amalgamation and Cold Vapor Atomic Absorption Method 2010
12. B.S. Fox, K.J. Mason, and F.C. McElroy Determination of total mercury in crude oil by combustion cold vapor atomic absorption spectrometry (CVAAS) Journal of ASTM International 2 6 2005 (Paper ID JAI13089.)
13. T. Wondimu, and W. Goessler Comparison of closed-pressurized and open-refluxed vessel digestion systems for trace elements in the residual fuel oil reference material (SRM 1634c) Bulletin of the Chemical Society of Ethiopia 14 2 2000 99 113 (Pubitemid 32464765)
14. S. Bloom, J. Parker, E.V.D. Geest, and C. Howard Comparison of high pressure wet ashing and hot acid extraction for the determination of Hg and other trace metals in crude oil 7th International Conference on Mercury as a Global Pollutant, Ljubljana, Slovenia 2004
15. M. Ostermann, P. Kettisch, and D. Becker Measurements of sulfur in oil using a pressurized wet digestion technique in open vessels and isotope dilution mass spectrometry Analytical and Bioanalytical Chemistry 2003 779 783 (Pubitemid 40890298)
16. R.M. de Jesus, A.M.P. dos Santos, S.L.C. Ferreira, M.M.S. Junior, and G.D. Matos Validation of a digestion system using a digester block/cold finger system for the determination of lead in vegetable foods by electrothermal atomic absorption spectrometry Journal of AOAC International 2011 942 946
17. L.D. Lacerda, H.H.M. Paraquetti, R.V. Marins, C.E. Rezende, I.R. Zalmon, M.P. Gomes, and V. Farias Mercury content in shark species from the south-eastern Brazilian coast Revista Brasileira de Biologia 60 4 2000 571 576
18. D. Gibicar, V. Jereb, R. Jacimovic, T. Dizdarevic, E.C. Paiva, R. Melamed, L.G.S. Sobral, Z. Spiric, and M. Horvat Optimisation of cold vapour atomic absorption spectrometry for determination of high levels of total mercury in activated carbon 7th International Conference on Mercury as a Global Pollutant, Ljubljana, Slovenia 2004
19. E.V. Silva-Filho, S.M. Sella, E.C. Spinola, I.R. Santos, W. Machado, and L.D. Lacerda Mercury, zinc, manganese, and iron accumulation in leachate pond sediments from a refuse tip in southeastern Brazil Microchemical Journal 82 2006 196 200
20. M.M. Molisani, R. Rocha, W. Machado, R.C. Barreto, and L.D. Lacerda Mercury contents in aquatic macrophytes from two reservoirs in the Paraíba do Sul: Guandú river system, SE Brasil Brazilian Journal of Biology 66 1A 2006 101 107
21. A.V. Zmozinski, A. De Jesus, M.G.R. Vale, and M.M. Silva Determination of calcium, magnesium and zinc in lubricating oils by flame atomic absorption spectrometry using a three-component solution Talanta 83 2 2010 637 643
22. S. Sholupov, S. Pogarev, V. Ryzhov, N. Mashyanov, and A. Stroganov Zeeman atomic absorption spectrometer RA-915+ for direct determination of mercury in air and complex matrix samples Fuel Processing Technology 85 2004 473 485
23. ASTM C1234-98, Standard practice for preparation of oils and oily waste samples by high pressure, high temperature digestion for trace element determinations, 2004.
24. Occupational Safety & Health Administration (OSHA) ID-145 Particulate Mercury in Workplace Atmospheres 1989