Validation of a Direct Analysis in Real Time Mass Spectrometry (DART-MS) method for the quantitation of six carbon sugars in a saccharification matrix

Analytical Methods

Volumn 4, Issue 10, 2012, Pages 3460-3465

  Saang'Onyo, Daudi ^a,b   Selby, Gary ^a   Smith, Darrin L ^a  

^a EASTERN KENTUCKY UNIVERSITY   (United States)

^b UNIVERSITY OF KENTUCKY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CALIBRATION CURVES; CORRELATION COEFFICIENT; DIRECT ANALYSIS IN REAL TIME; ENZYME HYDROLYSIS; INTERNAL STANDARDS; LIMITS OF DETECTION AND QUANTITATION; LINEAR ION TRAP; LINEAR RANGE; MATRIX EFFECTS; MOLECULAR IONS; SIX-CARBON SUGARS; SWITCHGRASS;

AMMONIUM COMPOUNDS; CALIBRATION; CARBON; GLUCOSE; ION SOURCES; MASS SPECTROMETRY;

SACCHARIFICATION;

EID: 84866985458     PISSN: 17599660     EISSN: 17599679     Source Type: Journal    
DOI: 10.1039/c2ay25337b     Document Type: Article

References (26)

1. G. A. Harris A. S. Galhena F. M. Fernandez Ambient sampling/ionization mass spectrometry: applications and current trends Anal. Chem. 2011 83 4508 4538
2. R. M. Alberici R. C. Simas G. B. Sanvido W. Romao P. M. Lalli M. Benassi I. B. S. Cunha M. N. Eberlin Ambient mass spectrometry: bringing MS into the "Real World" Anal. Bioanal. Chem. 2010 398 265 294
3. M. Z. Huang C. H. Yuan S. Y. Cheng Y. T. Cho J. Shiea Ambient ionization mass spectrometry Annu. Rev. Anal. Chem. 2010 3 43 65
4. S. Yu E. Crawford J. Tice B. Musselman J. T. Wu Bioanalysis without sample cleanup or chromatography: the evaluation and initial implementation of direct analysis in real time ionization mass spectrometry for the quantification of drugs in biological matrixes Anal. Chem. 2009 81 193 202
5. L. Nyadong G. A. Harris S. Balayssac A. S. Galhena M. Malet-Martino R. Martino R. M. Parry M. D. Wang F. M. Fernandez V. Gilard Combining two-dimensional diffusion-ordered nuclear magnetic resonance spectroscopy, imaging desorption electrospray ionization mass spectrometry, and direct analysis in real-time mass spectrometry for the Integral investigation of counterfeit pharmaceuticals Anal. Chem. 2009 81 4803 4812
6. R. Helmy W. Schafer L. Buhler S. Marcinko B. Musselman E. Guidry H. Jenkins F. Fleitz C. J. Welch Ambient pressure desorption ionization mass spectrometry in support of preclinical pharmaceutical development Org. Process Res. Dev. 2010 14 386 392
7. C. Y. Pierce J. R. Barr R. B. Cody R. F. Massung A. R. Woolfitt H. Moura H. A. Thompson F. M. Fernandez Ambient generation of fatty acid methyl ester ions from bacterial whole cells by direct analysis in real time (DART) mass spectrometry Chem. Commun. 2007 807 809
8. K. Kpegba T. Spadaro R. B. Cody N. Nesnas J. A. Olson Analysis of self-assembled monolayers on gold surfaces using direct analysis in real time mass spectrometry Anal. Chem. 2007 79 5479 5483 (Pubitemid 47121070)
9. E. Jagerdeo M. Abdel-Rehim Screening of cocaine and its metabolites in human urine samples by direct analysis in real-time source coupled to time-of-flight mass spectrometry after online preconcentration utilizing microextraction by packed sorbent J. Am. Soc. Mass Spectrom. 2009 20 891 899
10. R. R. Steiner R. L. Larson Validation of the direct analysis in real time source for use in forensic drug screening J. Forensic Sci. 2009 54 617 622
11. R. W. Jones R. B. Cody J. F. McClelland Differentiating writing inks using direct analysis in real time mass spectrometry J. Forensic Sci. 2006 51 915 918 (Pubitemid 44015203)
12. C. Petucci J. Diffendal D. Kaufman B. Mekonnen G. Terefenko B. Musselman Direct analysis in real time for reaction monitoring in drug discovery Anal. Chem. 2007 79 5064 5070 (Pubitemid 47051463)
13. P. Kumar D. M. Barrett M. J. Delwiche P. Stroeve Methods for pretreatment of lignocellulosic biomass for efficient hydrolysis and biofuel production Ind. Eng. Chem. Res. 2009 48 3713
14. J. D. McMillan, in Enzymatic Conversion of Biomass for Fuel Production, ed., M. E. Himmel, J. O. Baker, and, R. P. Overend, American Chemical Society (ACS), Washington DC, 1994, pp. 292-293
15. D. R. Keshwani J. J. Cheng Switchgrass for bioethanol and other value-added applications: a review Bioresour. Technol. 2009 100 1515 1523 (Pubitemid 50315293)
16. K. David A. J. Ragauskas Switchgrass as an energy crop for biofuel production: a review of its lingo-cellulosic chemical properties Energy Environ. Sci. 2010 3 1182 1190
17. A. Fox P. Y. Lau A. Brown S. L. Morgan Z.-T. Zhu M. Lema M. D. Walla Capillary gas chromatographic analysis of carbohydrates of Legionella pneumophila and other members of the family Legionellaceae J. Clin. Microbiol. 1984 19 326 332 (Pubitemid 14187582)
18. J. H. Ko H. Huang G. W. Kang W. J. Cheong Simultaneous quantitative determination of monosaccharides including fructose in hydrolysates of yoghurt and orange juice products by derivatization of monnossacharides with p-aminobenzoic acid ethyl ester followed by HPLC Bull. Korean Chem. Soc. 2005 26 1533 1538 (Pubitemid 41653263)
19. P. Luo M. Z. Luo R. P. Baldwin Determination of sugars in food products: using HPLC and electrochemical detection at a Cu electrode J. Chem. Educ. 1993 70 679 681
20. X. Zhu T. Sato The distinction of underivatized monosaccharides using electrospray ion trap mass spectrometry Rapid Commun. Mass Spectrom. 2007 21 191 198 (Pubitemid 46095477)
21. C. R. Taormina J. T. Baca S. A. Asher J. J. Grabowski Analysis of tear glucose concentration with electrospray ionization mass spectrometry J. Am. Soc. Mass Spectrom. 2007 18 332 336 (Pubitemid 46150104)
22. S.-S. Choi J.-C. Kim Deuterium effect on ionization and fragmentation patterns of monosaccharides ionized by atmospheric pressure chemical ionization Carbohydr. Res. 2010 345 408 413
23. M. S. Bereman T. I. Williams D. C. Muddiman Carbohydrate analysis by desorption electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry Anal. Chem. 2007 79 8812 8815 (Pubitemid 350171398)
24. D. Saang'onyo D. L. Smith Optimization of direct analysis in real time (DART) linear ion trap parameters for the detection and quantitation of glucose Rapid Commun. Mass Spectrom. 2012 26 385 391
25. J. H. Zar, in Biostatistical Analysis, Prentice Hall, Upper Saddle River, New Jersey, 5th edn, 2010
26. L. Huber, in Validation and Qualification in Analytical Laboratories, Interpharm Press, East Englewood, Colorado, 1998