Online coupling of size-exclusion chromatography and low-field 1H NMR spectroscopy

Macromolecular Chemistry and Physics

Volumn 213, Issue 18, 2012, Pages 1933-1943

  Cudaj, Markus ^a   Guthausen, Gisela ^a   Hofe, Thorsten ^b   Wilhelm, Manfred ^a  

^a KARLSRUHE INSTITUTE OF TECHNOLOGY   (Germany)

^b Polymer Standards Service GmbH   (Germany)

Author keywords

detectors; low field NMR; medium resolution NMR; SEC

Indexed keywords

COLUMN DIMENSIONS; DEUTERATED SOLVENTS; H NMR SPECTROSCOPY; LOW-FIELD NMR; NMR SPECTROMETER; ON-LINE COUPLING; POLYMER FRACTIONS; PROTONATED; SEC; SIGNAL TO NOISE (S/N) RATIOS; SOLVENT SUPPRESSION; TIME DOMAIN; VOLUME FLOW;

DETECTORS; DEUTERIUM; DIGITAL FILTERS; SOLVENTS; SPECTROMETERS;

SIZE EXCLUSION CHROMATOGRAPHY;

EID: 84866245581     PISSN: 10221352     EISSN: 15213935     Source Type: Journal    
DOI: 10.1002/macp.201200290     Document Type: Article

References (32)

1. J. W. Gilman, Appl. Clay Sci. 1999, 15, 31.
2. J. E. Weston, B. C. H. Steele, Solid State Ionics 1982, 7, 75.
3. D. Needham, T. J. McIntosh, D. D. Lasic, Biochimica et Biophysica (BBA)-Biomembranes 1992, 1, 40.
4. W. W. Yau, J. J. Kirkland, D. D. Bly, Modern Size Exclusion Chromatography, Wiley-Interscience, New York 1979.
5. H. G. Barth, Modern Methods of Particle Size Analysis, Wiley-Interscience, New York 1984.
6. R. R. Ryan, Biochem.-Us 1969, 8, 495.
7. E. G. Bartick, J. F. Johnson, Abstr. Pap. Am. Chem. S. 1976, 172, 94.
8. Y. Brun, J. Liq. Chromatogr. Rel. Technol. 1998, 21, 1979.
9. G. Marko-Vargas, D. Barcelo, Anal. Chim. Acta 1992, 270, 63.
10. F. Gores, P. Montag, C. Schall, J. Vienken, S. K. Bowry, Biomaterials 2002, 23, 3131.
11. P. Montag, Lc.Gc.Eur, 2006, Supplement S, 42.
12. A. Bandis, W.-Y. Wen, E. B. Jones, P. Kaskan, Y. Zhu, A. A. Jones, P. T. Inglefield, J. T. Bendler, J. Polym. Sci., B: Polym. Phys. 1994, 32, 1707.
13. J. Falkenhagen, T. Gruendling, S. Weidner, C. Barner-Kowollik, Polym. Chem.-Uk 2010, 1, 599.
14. C. Barner-Kowollik, T. Gruendling, D. Voll, M. Guilhaus, Macromol. Chem. Phys. 2010, 211, 80.
15. M. Buback, A. Feldermann, C. Barner-Kowollik, I. Lacik, Macromolecules 2001, 34, 5439.
16. W. Hiller, M. Hehn, T. Hofe, K. Oleschko, Anal. Chem. 2010, 82, 8244.
17. W. Hiller, H. Pasch, T. Macko, M. Hofmann, J. Ganz, M. Spraul, U. Braumann, R. Streck, J. Mason, F. van Damme, J. Magn. Reson. 2006, 183, 290.
18. M. Cudaj, G. Guthausen, A. Kamlowski, D. Maier, T. Hofe, M. Wilhelm, Nachr. Chem. 2010, 58, 1155.
19. F. Dalitz, M. Maiwald, G. Guthausen, Chem. Eng. Sci. 2012, 75, 318.
20. S. Berger, S. Braun, 200 and More NMR Experiments, Wiley-VCH, Weinheim Germany 2004.
21. R. R. Ernst, G. Bodenhausen, A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions, Clarendon Press, Oxford 1994.
22. H. Brouwer, J. Magn. Reson. 2009, 201, 230.
23. J. C. Moore, Separ. Sci. 1970, 5, 723.
24. J. J. van Deemter, F. J. Zuiderweg, A. Klinkenberg, Chem. Eng. Sci. 1956, 5, 271.
25. G. Meira, M. Netopilik, M. Potschka, I. Schnoll-Bitai, J. Vega, Macromol. Symp. 2007, 258, 186.
26. M. Cudaj, G. Guthausen, T. Hofe, M. Wilhelm, Macromol. Rapid Comm. 2011, 32, 665.
27. ACT, "act mobile NMR solutions", ACT Aachen, Aachen, 2011.
28. M. A. Vargas, M. Cudaj, K. Hailu, K. Sachsenheimer, G. Guthausen, Macromolecules 2010, 43, 5561.
29. T. F. Beskers, T. Hofe, M. Wilhelm, Macromol. Rapid Comm. 2012, DOI: 10.1002/marc.20120040.
30. G. Guthausen, A. Garnier, R. Reimert, Appl. Spectrosc. 2009, 63, 1121.
31. G. Guthausen, A. Kamlowski, Developments in time domain and single sided NMR, in Magnetic Resonance in Food Science: Challenges in a Changing World, (Eds:, M. Guojonsdottir, P. Belton, G. A. Webb,), RSC Publisher, Nordic House, Reykjavik, Iceland 2009, p. 293/46.
32. M. Cudaj, T. Hofe, M. Wilhelm, M. A. Vargas, G. Guthausen, Medium resolution NMR at 20 MHz: Possibilities and challenges, in Magnetic Resonance in Food Science: An Exciting Future, (Eds:, J.-P. Renou, P. S. Belton, G. A. Webb,), RSC Publishing, Cambridge 2011, p. 332/84.