Online size exclusion chromatography-NMR for the determination of molar mass distributions of copolymers

Analytical Chemistry

Volumn 82, Issue 19, 2010, Pages 8244-8250

  Hiller, Wolf ^a   Hehn, Mathias ^a   Hofe, Thorsten ^b   Oleschko, Kirsten ^b  

^a TU DORTMUND UNIVERSITY   (Germany)

^b Polymer Standards Service GmbH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL COMPOSITION DISTRIBUTIONS; CHEMICAL COMPOSITIONS; CHROMATOGRAPHIC CONDITIONS; CONCENTRATION DETECTORS; ELUTION VOLUMES; GENERAL APPROACH; HOMOPOLYMERS; MASS CALIBRATIONS; MASS PARAMETER; MOLAR MASS DISTRIBUTION; MONOMER UNITS; MULTI-DETECTORS; POLYSTYRENE-B-POLY(METHYL METHACRYLATE); SAMPLE CONCENTRATION;

BLOCK COPOLYMERS; CALIBRATION; COPOLYMERIZATION; ESTERS; GEL PERMEATION CHROMATOGRAPHY; MOLAR MASS; PLASTIC PRODUCTS; POLYMETHYL METHACRYLATES; POLYSTYRENES;

SIZE EXCLUSION CHROMATOGRAPHY;

EID: 77957313223     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac1013095     Document Type: Article

References (33)

1. Watanabe, N. and Niki, E. Proc. Jpn. Acad., Ser. B 1978, 54, 194-199
2. Korhammer, S. A. and Bernreuther, A. Fresenius J. Anal. Chem. 1996, 354, 131-135
3. Albert, K. On-line LC-NMR and Related Techniques; John Wiley & Sons Ltd.: Chichester, U.K., 2002.
4. Pasch, H. and Hiller, W. Macromolecules 1996, 29, 6556-6559
5. Pasch, H., Hiller, W., and Haner, R. Polymer 1998, 39, 1515-1523
6. Krämer, I., Hiller, W., and Pasch, H. Macromol. Chem. Phys. 2000, 201, 1662-1666
7. Kitayama, T., Janco, M., Ute, K., Niimi, R., Hatada, K., and Berek, D. Anal. Chem. 2000, 72, 1518-1522
8. Hiller, W., Brüll, A., Argyropoulos, D., Hoffmann, E., and Pasch, H. Magn. Reson. Chem. 2005, 43, 729
9. Hiller, W., Sinha, P., and Pasch, H. Macromol. Chem. Phys. 2007, 208, 1965-1978
10. Hiller, W., Sinha, P., and Pasch, H. Macromol. Chem. Phys. 2009, 210, 605-613
11. Hiller, W., Pasch, H., Sinha, P., Wagner, T., Thiel, J., Wagner, M., and Müllen, K. Macromolecules 2010, 43, 4853-4863
12. Hatada, K., Ute, K., Okamoto, Y., Imanari, M., and Fujii, N. Polym. Bull. 1988, 20, 317-321
13. Ute, K. and Hatada, K. Anal. Sci. 1991, 7, 1629-1632
14. Hatada, K., Ute, K., Kitayama, T., Nishimura, T., Kashiyama, M., and Fujimoto, N. Polym. Bull. 1990, 23, 549-554
15. Hatada, K., Ute, K., Kitayama, T., Yamamoto, M., Nishimura, T., and Kashiyama, M. Polym. Bull. 1989, 21, 489-495
16. Krämer, I., Pasch, H., Händel, H., and Albert, K. Macromol. Chem. Phys. 1999, 200, 1734-1744
17. Ute, K., Niimi, R., Matsunaga, M., Hatada, K., and Kitayama, T. Macromol. Chem. Phys. 2001, 202, 3081-3086
18. Hiller, W., Pasch, H., Macko, T., Hofmann, M., Ganz, J., Spraul, M., Braumann, U., Streck, R., Mason, J., and van Damme, F. J. Magn. Reson. 2006, 183, 290-302
19. Ute, K., Niimi, R., Hongo, S.-Y., and Hatada, K. Polym. J. 1998, 30, 439-443
20. Hatada, K., Ute, K., Kashiyama, M., and Imanari, M. Polym. J. 1990, 22, 218-222
21. Smallcombe, S. H., Patt, S. L., and Keifer, P. A. J. Magn. Res. A 1995, 117, 295-303
22. Yau, W. W., Kirkland, J. J., and Bly, D. D. Modern Size-Exclusion Liquid Chromatography; John Wiley & Sons: New York, 1979.
23. Fyfe, C. A., Cocivera, M., Damji, S. W. H., Hostetter, T. A., Sproat, D., and O'Brien, J. J. Magn. Reson. 1976, 23, 377-384
24. Laude, D. A., Jr., Lee, R. W.-K., and Wilkins, C. L. J. Magn. Reson. 1984, 60, 453-459
25. Laude, D. A., Jr., Lee, R. W.-K., and Wilkins, C. L. Anal. Chem. 1985, 57, 1281-1286
26. Laude, D. A., Jr., Lee, R. W.-K., and Wilkins, C. L. Anal. Chem. 1985, 57, 1286-1290
27. Griffiths, L. Anal. Chem. 1995, 67, 4091-4095
28. Sudmeier, J. L., Günther, U. L., Albert, K., and Bachovchin, W. W. J. Magn. Res. A 1996, 118, 145-156
29. Griffiths, L. Magn. Reson. Chem. 1997, 35, 257-261
30. Striegel, A. M., Yau, W. W., Kirkland, J. J., and Bly, D. D. Modern Size-Exclusion Liquid Chromatography: Practice of Gel Permeation and Gel Filtration Chromatography, 2 nd ed.; Wiley: Hoboken, NJ, 2009.
31. Kilz, P. and Pasch, H. Coupled LC Techniques in Molecular Characterization. In Encyclopedia of Analytical Chemistry; Myers, R. A., Ed.; Wiley: Chichester, U.K., 2000.
32. Haidar Ahmad, I. A. and Striegel, A. M. Anal. Bioanal. Chem. 2010, 396, 1589-1598
33. Hsieh, H. L. and Quirk, R. P. Anionic Polymerization: Principles and Practical Applications; Marcel Dekker Inc.: New York, 1996; p 671.